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author:

Li, Xiaojing (Li, Xiaojing.) [1] | Xiong, Wenming (Xiong, Wenming.) [2] | Lin, Hua (Lin, Hua.) [3] | Zhuo, Liyang (Zhuo, Liyang.) [4] | Lv, Shuiyuan (Lv, Shuiyuan.) [5] | Tang, Xi (Tang, Xi.) [6] | Chen, Minshi (Chen, Minshi.) [7] | Zou, Zhexiang (Zou, Zhexiang.) [8] | Lin, Zhenyu (Lin, Zhenyu.) [9] (Scholars:林振宇) | Qiu, Bin (Qiu, Bin.) [10] (Scholars:邱彬) | Chen, Guonan (Chen, Guonan.) [11] (Scholars:陈国南)

Indexed by:

EI Scopus SCIE

Abstract:

An RP LC-ESI-MS/MS method for the determination of the migration of 16 primary phthalic acid esters from plastic samples has been developed using distilled water, 3% acetic acid, 10% alcohol, and olive oil as food simulants. Detection limits were 1.6-18.5 mu g/kg in distilled water, 1.4-17.3 mu g/kg in 3% acetic acid, 1.4-19.2 mu g/kg in 10% alcohol, and 31.9-390.8 mu g/kg in olive oil. The RSDs were in the range of 0.07-11.28%. The real plastic products inspection showed that only few analyzed samples were phthalates contaminated. Bis-2-ethylhexyl ester and dibutyl phthalate were the common items migrated from the plastic products into food and feeds, but the migration concentrations were far below the limits set by European Union (1.5 mg/kg for bis-2-ethylhexyl ester and 0.3 mg/kg for dibutyl phthalate).

Keyword:

Food simulant LC-MS/MS Migration Phthalic acid ester

Community:

  • [ 1 ] [Li, Xiaojing]Fujian Entry Exit Inspect & Quarantine Bur, Ctr Tech, Fuzhou, Peoples R China
  • [ 2 ] [Lin, Hua]Fujian Entry Exit Inspect & Quarantine Bur, Ctr Tech, Fuzhou, Peoples R China
  • [ 3 ] [Lv, Shuiyuan]Fujian Entry Exit Inspect & Quarantine Bur, Ctr Tech, Fuzhou, Peoples R China
  • [ 4 ] [Tang, Xi]Fujian Entry Exit Inspect & Quarantine Bur, Ctr Tech, Fuzhou, Peoples R China
  • [ 5 ] [Chen, Minshi]Fujian Entry Exit Inspect & Quarantine Bur, Ctr Tech, Fuzhou, Peoples R China
  • [ 6 ] [Zou, Zhexiang]Fujian Entry Exit Inspect & Quarantine Bur, Ctr Tech, Fuzhou, Peoples R China
  • [ 7 ] [Xiong, Wenming]Fuzhou Univ, Dept Chem, Fujian Prov Key Lab Anal & Detect Technol Food Sa, MOE Key Lab Anal & Detect Food Safety, Fuzhou 350002, Fujian, Peoples R China
  • [ 8 ] [Zhuo, Liyang]Fuzhou Univ, Dept Chem, Fujian Prov Key Lab Anal & Detect Technol Food Sa, MOE Key Lab Anal & Detect Food Safety, Fuzhou 350002, Fujian, Peoples R China
  • [ 9 ] [Lin, Zhenyu]Fuzhou Univ, Dept Chem, Fujian Prov Key Lab Anal & Detect Technol Food Sa, MOE Key Lab Anal & Detect Food Safety, Fuzhou 350002, Fujian, Peoples R China
  • [ 10 ] [Qiu, Bin]Fuzhou Univ, Dept Chem, Fujian Prov Key Lab Anal & Detect Technol Food Sa, MOE Key Lab Anal & Detect Food Safety, Fuzhou 350002, Fujian, Peoples R China
  • [ 11 ] [Chen, Guonan]Fuzhou Univ, Dept Chem, Fujian Prov Key Lab Anal & Detect Technol Food Sa, MOE Key Lab Anal & Detect Food Safety, Fuzhou 350002, Fujian, Peoples R China

Reprint 's Address:

  • [Li, Xiaojing]B-816 312 Hudong Rd, Fuzhou 350002, Fujian, Peoples R China

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Source :

JOURNAL OF SEPARATION SCIENCE

ISSN: 1615-9306

Year: 2013

Issue: 3

Volume: 36

Page: 477-484

2 . 5 9 4

JCR@2013

2 . 8 0 0

JCR@2023

ESI Discipline: CHEMISTRY;

JCR Journal Grade:2

CAS Journal Grade:3

Cited Count:

WoS CC Cited Count: 29

SCOPUS Cited Count: 29

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 2

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