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author:

Li, Xiaojing (Li, Xiaojing.) [1] | Xiong, Wenming (Xiong, Wenming.) [2] | Lin, Hua (Lin, Hua.) [3] | Zhuo, Liyang (Zhuo, Liyang.) [4] | Lv, Shuiyuan (Lv, Shuiyuan.) [5] | Tang, Xi (Tang, Xi.) [6] | Chen, Minshi (Chen, Minshi.) [7] | Zou, Zhexiang (Zou, Zhexiang.) [8] | Lin, Zhenyu (Lin, Zhenyu.) [9] | Qiu, Bin (Qiu, Bin.) [10] | Chen, Guonan (Chen, Guonan.) [11]

Indexed by:

EI

Abstract:

An RP LC-ESI-MS/MS method for the determination of the migration of 16 primary phthalic acid esters from plastic samples has been developed using distilled water, 3% acetic acid, 10% alcohol, and olive oil as food simulants. Detection limits were 1.6-18.5 μg/kg in distilled water, 1.4-17.3 μg/kg in 3% acetic acid, 1.4-19.2 μg/kg in 10% alcohol, and 31.9-390.8 μg/kg in olive oil. The RSDs were in the range of 0.07-11.28%. The real plastic products inspection showed that only few analyzed samples were phthalates contaminated. Bis-2-ethylhexyl ester and dibutyl phthalate were the common items migrated from the plastic products into food and feeds, but the migration concentrations were far below the limits set by European Union (1.5 mg/kg for bis-2-ethylhexyl ester and 0.3 mg/kg for dibutyl phthalate). © 2013 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Keyword:

Acetic acid Chemical contamination Esters Olive oil pH Plastic products

Community:

  • [ 1 ] [Li, Xiaojing]Technical Centre of Fujian Entry-Exit Inspection and Quarantine Bureau, Fuzhou, China
  • [ 2 ] [Xiong, Wenming]Department of Chemistry, MOE Key Laboratory of Analysis and Detection for Food Safety, Fuzhou University, Fujian, Fuzhou, China
  • [ 3 ] [Lin, Hua]Technical Centre of Fujian Entry-Exit Inspection and Quarantine Bureau, Fuzhou, China
  • [ 4 ] [Zhuo, Liyang]Department of Chemistry, MOE Key Laboratory of Analysis and Detection for Food Safety, Fuzhou University, Fujian, Fuzhou, China
  • [ 5 ] [Lv, Shuiyuan]Technical Centre of Fujian Entry-Exit Inspection and Quarantine Bureau, Fuzhou, China
  • [ 6 ] [Tang, Xi]Technical Centre of Fujian Entry-Exit Inspection and Quarantine Bureau, Fuzhou, China
  • [ 7 ] [Chen, Minshi]Technical Centre of Fujian Entry-Exit Inspection and Quarantine Bureau, Fuzhou, China
  • [ 8 ] [Zou, Zhexiang]Technical Centre of Fujian Entry-Exit Inspection and Quarantine Bureau, Fuzhou, China
  • [ 9 ] [Lin, Zhenyu]Department of Chemistry, MOE Key Laboratory of Analysis and Detection for Food Safety, Fuzhou University, Fujian, Fuzhou, China
  • [ 10 ] [Qiu, Bin]Department of Chemistry, MOE Key Laboratory of Analysis and Detection for Food Safety, Fuzhou University, Fujian, Fuzhou, China
  • [ 11 ] [Chen, Guonan]Department of Chemistry, MOE Key Laboratory of Analysis and Detection for Food Safety, Fuzhou University, Fujian, Fuzhou, China

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Source :

Journal of Separation Science

ISSN: 1615-9306

Year: 2013

Issue: 3

Volume: 36

Page: 477-484

2 . 5 9 4

JCR@2013

2 . 8 0 0

JCR@2023

JCR Journal Grade:2

CAS Journal Grade:3

Cited Count:

WoS CC Cited Count:

SCOPUS Cited Count: 29

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 2

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