Indexed by:
Abstract:
本文建立了液相色谱安培检测鳗鱼中常用8种磺胺检测方法,采用甲醇:磷酸盐缓冲液(pH=3)梯度淋洗,反相C18分离.样品采用乙腈提取后,正己烷脱脂,用Oasis MCX、MAX小柱净化后,采用玻碳电极直流安培1.3V检测.线性范围为0.05-100μg/mL,分别做3个浓度的添加回收,方法回收率在52.8~102.0%之间,方法精密度在0.8~4.6%之间,方法定量限为0.5-4μg/kg.
Keyword:
Reprint 's Address:
Email:
Version:
Source :
福建分析测试
ISSN: 1009-8143
CN: 35-1246/T
Year: 2007
Issue: 2
Volume: 16
Page: 19-24
Cited Count:
WoS CC Cited Count: 0
SCOPUS Cited Count:
ESI Highly Cited Papers on the List: 0 Unfold All
WanFang Cited Count:
Chinese Cited Count:
30 Days PV: 0
Affiliated Colleges: