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Abstract:
本文建立了液相色谱安培检测鳗鱼中常用8种磺胺检测方法,采用甲醇:磷酸盐缓冲液(pH=3)梯度淋洗,反相C18分离。样品采用乙腈提取后,正己烷脱脂,用OasisMCX、MAX小柱净化后,采用玻碳电极直流安培1.3V检测。线性范围为0.05-100μg/mL,分别做3个浓度的添加回收,方法回收率在52.8~102.0%之间,方法精密度在0.8~4.6%之间,方法定量限为0.5-4μg/kg。
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福建分析测试
ISSN: 1009-8143
Year: 2007
Issue: 2
Volume: 16
Page: 19-24
Cited Count:
WoS CC Cited Count: 0
SCOPUS Cited Count:
ESI Highly Cited Papers on the List: 0 Unfold All
WanFang Cited Count:
Chinese Cited Count: -1
30 Days PV: 1
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