In　order　to　improve　the　comprehensive　recovery　of　the　beneficial　metal　in　the　high-sulfur　copper　and　gold　ore　from　Yunnan　province,　the　concentration　experiments　were　conducted.　The　grade　of　copper,　sulfur　and　gold　are　5.14%,　16.96%　and　0.3　g/t　in　this　ore,　respectively.　Based　on　the　property　of　the　high-sulfur　cooper,　mixed　floatation　was　performed　to　recovery　copper　and　pyrrhotite　firstly,　then　magnetic　separation　was　used　to　separate　the　chalcopyrite　and　pyrrhotite,　at　last　gravity　separation　was　used　to　enrich　the　gold　in　the　copper　concentrate.　Three　concentrate　products　were　got　using　the　joint　process　of　flotation-magnetic　separation-gravity　separation.　With　the　process　we　can　obtain　good　results　in　the　closed　circuit　experiment,　the　results　were　as　below:　in　copper　concentrate　I　the　grades　of　Cu　and　Au　were　28.64%　and　1.21　g/t,　in　copper　concentrate　II　the　grades　of　Cu　and　Au　were　25.31%　and　0.64　g/t,　respectively.　The　total　recovery　rate　of　Cu　was　up　to　98.53%.　The　grade　of　S　in　sulfur　concentrate　was　39.93%　with　the　recovery　rate　of　46.08%.　The　recovery　rate　of　gold　was　30.43%.　In　this　process,　without　the　addition　of　lime,　it　not　only　realized　the　efficient　separation　of　copper　and　sulfur,　but　also　enhanced　the　comprehensive　recovery　of　mineral　products　and　the　maximal　value　of　the　ore.　It　has　particular　means　of　innovative　and　practical　application.　©　2016,　Science　Press.　All　right　reserved.