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Abstract:
Nanocrystalline nickel was synthesized by direct current electrodeposition from a modified Watts-type bath. X-ray diffraction and transmission electron microscopy were used to characterize the microstructure of nickel deposits. The results show that nanocrytalline nickel with grain sizes in the range of 20-50 nm can be synthesized from saccharin-containing Watts-type baths with the current density range of 5-30 A/dm2. There existed preferred orientation in the deposits and it changed progressively from a (200) fibre texture to a (111) (200) double fibre texture as saccharin concentration increased. The hardness of the deposits increased prominently as grain size decreased to nanometer range.
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Transactions of Materials and Heat Treatment
ISSN: 1009-6264
CN: 11-4545/TG
Year: 2004
Issue: 5
Volume: 25
Page: 1283-1286
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ESI Highly Cited Papers on the List: 0 Unfold All
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30 Days PV: 0
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