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author:

Dai, Pin-Qiang (Dai, Pin-Qiang.) [1] | Yu, Hui (Yu, Hui.) [2] | Li, Qiang (Li, Qiang.) [3] (Scholars:李强)

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Abstract:

Nanocrystalline nickel was synthesized by direct current electrodeposition from a modified Watts-type bath. X-ray diffraction and transmission electron microscopy were used to characterize the microstructure of nickel deposits. The results show that nanocrytalline nickel with grain sizes in the range of 20-50 nm can be synthesized from saccharin-containing Watts-type baths with the current density range of 5-30 A/dm2. There existed preferred orientation in the deposits and it changed progressively from a (200) fibre texture to a (111) (200) double fibre texture as saccharin concentration increased. The hardness of the deposits increased prominently as grain size decreased to nanometer range.

Keyword:

Current density Electrodeposition Grain size and shape Hardness Microstructure Nanostructured materials Nickel deposits Synthesis (chemical)

Community:

  • [ 1 ] [Dai, Pin-Qiang]Coll. of Mat. Sci. and Eng., Fuzhou Univ., Fuzhou, China
  • [ 2 ] [Yu, Hui]Coll. of Mat. Sci. and Eng., Fuzhou Univ., Fuzhou, China
  • [ 3 ] [Li, Qiang]Coll. of Mat. Sci. and Eng., Fuzhou Univ., Fuzhou, China

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Source :

Transactions of Materials and Heat Treatment

ISSN: 1009-6264

CN: 11-4545/TG

Year: 2004

Issue: 5

Volume: 25

Page: 1283-1286

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ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

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30 Days PV: 0

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