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Abstract:
Nanocrystalline nickel was synthesized by direct current electrodeposition from a modified Watts-type bath. X-ray diffraction and transmission electron microscope were used to characterize the microstructure of nickel deposits. The results show that nanocrytalline nickel with grain sizes in the range 20 similar to 50nm can be synthesized from saccharin-containing Watts-type baths with current density range 5 similar to 30A/dm(2). There existed preferred orientation in the deposits and it changed progressively from a (200) fibre texture to a (111) (200) double fibre texture as saccharin concentration increased. The hardness of the deposits increased prominently as grain size decreased to nanometer range.
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14TH CONGRESS OF INTERNATIONAL FEDERATION FOR HEAT TREATMENT AND SURFACE ENGINEERING, VOLS 1 AND 2, PROCEEDINGS
Year: 2004
Page: 1283-1286
Language: English
Cited Count:
WoS CC Cited Count: 5
SCOPUS Cited Count:
ESI Highly Cited Papers on the List: 0 Unfold All
WanFang Cited Count:
Chinese Cited Count:
30 Days PV: 1
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