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author:

Liu, Ming (Liu, Ming.) [1] (Scholars:刘明) | Chen, Shuai (Chen, Shuai.) [2]

Indexed by:

EI Scopus SCIE

Abstract:

Micromechanical characterization of brittle ceramics remains challenging due to the difficulty in sample preparation required by conventional tests. The micromechanical properties (e.g., elastic modulus E IT , indentation hardness H IT , and fracture toughness K IC ) of ZrO2 2 and Si3N4 3 N 4 were investigated by indentation and scratch tests with different indenters (e.g., Vickers, Knoop, and Berkovich indenters) under various loads. The ratio of the true hardness by the Vickers indenter over that by the Knoop indenter is approximately a constant of 1.13 and independent of material. Elastic recovery of residual imprint by the Knoop indenter was also used to assess elastic modulus of ZrO2 2 and Si3N4, 3 N 4 , and modified equations were proposed. The length of Vickers indenter-induced cracking was found to be proportional to the applied load under large loads, and a modified formula for calculating fracture toughness was proposed for ZrO2 2 and Si3N4, 3 N 4 , which have relatively large fracture toughness of about 9 MPa & sdot;m1/2. & sdot; m 1/2 . The critical void volume fraction f * in the nanoindentation energy-based methods was found to linearly decrease with the exponent m f of the power-law equation used for curve fitting of the degradation of H IT or E IT with h max . The determination of fracture toughness by scratch methodology was found to be affected by mechanical properties of material, indenter geometry, and data range.

Keyword:

Brittle ceramics Fracture toughness Instrumented indentation Micromechanical properties Scratch testing

Community:

  • [ 1 ] [Liu, Ming]Fuzhou Univ, Sch Mech Engn & Automat, Fujian Prov Key Lab Terahertz Funct Devices & Inte, Fuzhou 350108, Peoples R China
  • [ 2 ] [Chen, Shuai]Fuzhou Univ, Sch Mech Engn & Automat, Fujian Prov Key Lab Terahertz Funct Devices & Inte, Fuzhou 350108, Peoples R China

Reprint 's Address:

  • [Liu, Ming]Fuzhou Univ, Sch Mech Engn & Automat, Fujian Prov Key Lab Terahertz Funct Devices & Inte, Fuzhou 350108, Peoples R China;;

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Source :

CERAMICS INTERNATIONAL

ISSN: 0272-8842

Year: 2024

Issue: 11

Volume: 50

Page: 19982-20010

5 . 1 0 0

JCR@2023

Cited Count:

WoS CC Cited Count:

SCOPUS Cited Count:

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 2

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