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author:

Wang, Ran (Wang, Ran.) [1] | Tong, Wei (Tong, Wei.) [2] | Wu, Yijing (Wu, Yijing.) [3] | Chen, Zhuling (Chen, Zhuling.) [4] (Scholars:陈珠灵) | Lin, Zian (Lin, Zian.) [5] (Scholars:林子俺) | Cai, Zongwei (Cai, Zongwei.) [6]

Indexed by:

EI Scopus SCIE

Abstract:

A hollow microtubular covalent organic framework (denoted as TatDha-COF) was synthesized by solvothermal method for the enrichment and determination of quinones. The TatDha-COF showed large specific surface area (2057 m(2) g(-1)), good crystal structure, ordered pore size distribution (2.3 nm), stable chemical properties and good reusability. Accordingly, a simple and efficient method based on dispersive solid-phase extraction (d-SPE) and atmospheric pressure gas chromatography tandem mass spectrometry (APGC-MS/MS) was developed for the determination of quinones in complex samples. The established method demonstrated a wide liner range, good linearity (r > 0.9990), high enrichment factors (EFs, 24-69-folds) and low detection limits (LODs, 0.200-30.0 pg L-1, S/N >= 3). On this basis, the suggested method was successfully applied to sensitively detect the eight ultratrace quinones in mice plasma. Overall, the established method has provided a powerful tool for the enrichment and detection of ultratrace quinones in complex samples, presenting the promising application of TatDha-COF in sample pretreatment.

Keyword:

APGC-MS/MS Dispersive solid-phase extraction Hollow microtubular covalent organic frameworks Plasma analysis Quinones

Community:

  • [ 1 ] [Wang, Ran]Fuzhou Univ, Coll Chem, Fujian Prov Key Lab Anal & Detect Technol Food Saf, Minist Educ,Key Lab Analyt Sci Food Safety & Biol, Fuzhou 350116, Fujian, Peoples R China
  • [ 2 ] [Tong, Wei]Fuzhou Univ, Coll Chem, Fujian Prov Key Lab Anal & Detect Technol Food Saf, Minist Educ,Key Lab Analyt Sci Food Safety & Biol, Fuzhou 350116, Fujian, Peoples R China
  • [ 3 ] [Wu, Yijing]Fuzhou Univ, Coll Chem, Fujian Prov Key Lab Anal & Detect Technol Food Saf, Minist Educ,Key Lab Analyt Sci Food Safety & Biol, Fuzhou 350116, Fujian, Peoples R China
  • [ 4 ] [Chen, Zhuling]Fuzhou Univ, Coll Chem, Fujian Prov Key Lab Anal & Detect Technol Food Saf, Minist Educ,Key Lab Analyt Sci Food Safety & Biol, Fuzhou 350116, Fujian, Peoples R China
  • [ 5 ] [Lin, Zian]Fuzhou Univ, Coll Chem, Fujian Prov Key Lab Anal & Detect Technol Food Saf, Minist Educ,Key Lab Analyt Sci Food Safety & Biol, Fuzhou 350116, Fujian, Peoples R China
  • [ 6 ] [Cai, Zongwei]Hong Kong Baptist Univ, Dept Chem, State Key Lab Environm & Biol Anal, Kowloon Tong, 224 Waterloo Rd, Hong Kong 999077, Peoples R China

Reprint 's Address:

  • [Lin, Zian]Fuzhou Univ, Coll Chem, Fujian Prov Key Lab Anal & Detect Technol Food Saf, Minist Educ,Key Lab Analyt Sci Food Safety & Biol, Fuzhou 350116, Fujian, Peoples R China;;[Cai, Zongwei]Hong Kong Baptist Univ, Dept Chem, State Key Lab Environm & Biol Anal, Kowloon Tong, 224 Waterloo Rd, Hong Kong 999077, Peoples R China;;

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Source :

MICROCHIMICA ACTA

ISSN: 0026-3672

Year: 2023

Issue: 2

Volume: 190

5 . 4

JCR@2023

5 . 4 0 0

JCR@2023

ESI Discipline: CHEMISTRY;

ESI HC Threshold:39

JCR Journal Grade:1

CAS Journal Grade:2

Cited Count:

WoS CC Cited Count: 3

SCOPUS Cited Count: 3

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 4

Online/Total:116/10011557
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