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Abstract：
A biased bimetallic Fe-Fe complex Cp*Fe(dppe)(C ≡ CFc) (1) was synthesized from FcC ≡ CH (Fc=C5H4FeC5H5)and Cp*Fe(dppe)C1 (Cp*=C5Me5). Its one-electron oxidation species [Cp*Te(dppe)(C≡ CFc)][PF6] (1a) was also prepared and the spectroscopic properties of 1a was studied. The single-crystal X-ray diffraction analysis of 1 shows that ferrocenylacetylene is bonded at the terminal carbon to the iron center in the Cp*Fe(dppe) part. Crystallographic data for 1: monoclinic, space group C2/c, with a=4.067 65(14) nm, b=1.26074(4) nm, c=1.649 89(5) nm,fined to R1=0.038 4, wR2=0, 1000. CCDC: 234893.
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无机化学学报
ISSN： 1001-4861
Year： 2004
Issue： 9
Volume： 20
Page： 1061-1066
0 . 6
JCR@2004
0 . 8 0 0
JCR@2023
JCR Journal Grade：4
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ESI Highly Cited Papers on the List： 0 Unfold All
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Chinese Cited Count： -1
30 Days PV： 0
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