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author:

谢福荣 (谢福荣.) [1] | 涂貌贞 (涂貌贞.) [2] | 谢增鸿 (谢增鸿.) [3]

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CQVIP CSCD

Abstract:

基于碱性介质中敌百虫增强鲁米诺-H2O2体系发光的研究,建立了测定敌百虫的流动注射化学发光分析方法.该法测定敌百虫的线性范围为1.0×10^-8-1.0×10^-5g/mL,根据IUPAC建议计算出检出限为3.2×10^-9g/mL,相对标准偏差为1.10%(1.0×10^-7g/mL的敌百虫,n=11).对蔬菜中的敌百虫进行固相萃取,有效地除去蔬菜中的干扰物质,并对蔬菜样进行加标测定,回收率范围在88.5%-92.6%之间,结果令人满意.

Keyword:

化学发光法 敌百虫 流动注射

Community:

  • [ 1 ] 福州大学化学化工学院,福州市350002
  • [ 2 ] 福建林业职业技术学院,福建省南平市金山路353000

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Source :

光谱实验室

ISSN: 1004-8138

Year: 2006

Issue: 3

Volume: 23

Page: 644-647

Cited Count:

WoS CC Cited Count:

SCOPUS Cited Count:

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count: -1

30 Days PV: 5

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