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Abstract:
The lead iodide adduct [(Pb2I5)(L-H +)·2DMF]n (L=piperazine) has been prepared by self-assembly and structurally characterized. It presents one dimensional structure and crystallizes in Triclinic, P1 space group with the crystal cell parameter: a=0.922 06(18) nm, b=1.237 5(3) nm, c=1.297 2(3) nm, α=99.05(3)°, β=102.98(3)°, γ= 105.30(3)°, and V=1.353 8(6) nm3, Z=2, Dc=3.078 Mg·m-3, μ(Mo Kα)=18.127 mm-1, F(000)=1 085, chemical formula C 16H43N8O4Pb4I 10 and Mr=2 509.39, the final R=0.053 3 and wR=0.146 4 for 3 889 observed reflections with I>2σ(I). CCDC: 250760.
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Chinese Journal of Inorganic Chemistry
ISSN: 1001-4861
CN: 32-1185/O6
Year: 2005
Issue: 1
Volume: 21
Page: 83-86
0 . 6 9 7
JCR@2005
0 . 8 0 0
JCR@2023
ESI Discipline: CHEMISTRY;
JCR Journal Grade:4
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ESI Highly Cited Papers on the List: 0 Unfold All
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30 Days PV: 2
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