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学者姓名：李浩宏
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Abstract ：
The design of highly stable and active bifunctional catalysts for electrolytic water remains a significant challenge. In this study, self-supported CoP/CNT/Ni2P bifunctional catalysts with three-phase heterojunction nano- structures were constructed by a multi-step electrodeposition and phosphorylation strategy. X-ray diffraction analysis and transmission electron microscope showed that CoP/CNT/Ni2P was a three-phase heterojunction nanostructure, and scanning electron microscope results of CoP/CNT/Ni2P suggested the successful introduction of carbon nanotube (CNT). The X-ray photoelectron spectroscopy results indicate a shift in the elemental binding energy in CoP/CNT/Ni2P, which is believed to contribute to the electrocatalytic reaction. The incorporation of CNT enhances charge transfer within the multiphase catalyst and maximizes the exposure of catalytically active sites, achieving an increase in catalyst performance. As anticipated, the CoP/CNT/Ni2P catalyst displays high catalytic activity for both the hydrogen evolution reaction (61 mV at 10 mA cm_ 2 ) and the oxygen evolution reaction (342 mV at 100 mA cm_ 2 ), in addition to exhibiting long-term stability at a current density of 10 mA cm_ 2 over 40 h. The electrolyzer comprising CoP/CNT/Ni2P(+,_) necessitates a modest operating voltage of 1.52 V to attain 10 mA cm_ 2 during alkaline water splitting, thereby outperforming the commercial catalyst Pt/C|| IrO2 and earlier reports. This study provides guidance for the development of ultra-high activity and durability catalysts for water splitting.
Keyword ：
Bifunctional electrocatalysts Bifunctional electrocatalysts CNT CNT Hydrogen evolution reaction Hydrogen evolution reaction Overall water splitting Overall water splitting
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| GB/T 7714 | Yu, Guo , Zhao, Jiaxiang , Hou, Songjia et al. Mutual promotion of CoP/CNT/Ni2P by heterojunction structural design and intrinsic activity coupling for water splitting [J]. | FUEL , 2025 , 382 . |
| MLA | Yu, Guo et al. "Mutual promotion of CoP/CNT/Ni2P by heterojunction structural design and intrinsic activity coupling for water splitting" . | FUEL 382 (2025) . |
| APA | Yu, Guo , Zhao, Jiaxiang , Hou, Songjia , Han, Haoyang , Zhou, Qing , Yan, Zuoyi et al. Mutual promotion of CoP/CNT/Ni2P by heterojunction structural design and intrinsic activity coupling for water splitting . | FUEL , 2025 , 382 . |
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A multi-level memristor, implemented with inexpensive precursors and well-defined mechanisms, will be significant for the development of high-density memory in the coming big data era. Sulfur, a cheap element extracted from petroleum and natural gas, holds fascinating potential for use in information memory. In this work, a three-component hybrid, [Cu(Phen)2I]2Cu2I4S8 (Phen = 1,10-phenanthroline), was synthesized. In this structure, strong pi-pi stacking interactions among Phen ligands, cuprophilic interactions in (Cu2I4)2- anions, and C-H & ctdot;I/S hydrogen bonds contributed to the formation of a quasi-3D network. A FTO/hybrid/Ag memristor was fabricated, exhibiting ternary memory performance with a high ON2/ON1/OFF current ratio (104.50/101.47/1) and a ternary yield of 68%. The memristor could operate at a high temperature of 185 degrees C. Based on the structural characteristics of the hybrid, FIB-SEM measurements on the Ag/hybrid/Ag model device, double logarithm analysis of the I-V curve, memory performance of the three individual precursors, and external voltage-dependent PXRD, its ternary resistive switching performance could be explained as follows: upon continuous external voltages, the transition OFF -> ON1 was driven by enhanced pi-pi stacking interactions among the Phen ligands, and the current jump ON1 -> ON2 resulted from the formation of a conductive S8/(Cu2I4)2- layer bearing cuprophilic interactions via S8 relaxation. This works extends the strategy of sulfur relaxation in multi-level memories from coordinated polysulfides to uncoordinated ones. The use of inexpensive precursors, combined with the distinct structure-property correlation, provides a promising avenue for implementing novel high-density memristors.
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| GB/T 7714 | Li, Huifang , Gao, Yiqun , Lin, Xi et al. Ternary resistive switching memory of copper-organic complex/iodocuprate/sulfur hybrid enabled by π-π interactions and S8 relaxation [J]. | CRYSTENGCOMM , 2025 , 27 (10) : 1439-1445 . |
| MLA | Li, Huifang et al. "Ternary resistive switching memory of copper-organic complex/iodocuprate/sulfur hybrid enabled by π-π interactions and S8 relaxation" . | CRYSTENGCOMM 27 . 10 (2025) : 1439-1445 . |
| APA | Li, Huifang , Gao, Yiqun , Lin, Xi , Li, Ke , Lin, Xiaoli , Li, Haohong et al. Ternary resistive switching memory of copper-organic complex/iodocuprate/sulfur hybrid enabled by π-π interactions and S8 relaxation . | CRYSTENGCOMM , 2025 , 27 (10) , 1439-1445 . |
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Multifunctional memristors with a high memory density, low power consumption, flexibility, programmability, and environmental robustness are essential for next-generation memories. In this work, a titanocene-polysulfide complex (Cp2TiS5) with strong SS interactions and hydrogen bonds was synthesized and integrated with TiO2 to create a novel Cu/TiO2/Cp2TiS5/Ag memristor. This device shows bipolar nonvolatile memory performance with a remarkable ON/OFF ratio (104.8), low switching voltages (V SET, -0.16 V; V RESET, +0.15 V), and low power consumption (2.7 x 10-4 mu W). It exhibits multilevel memory behavior, flexibility, optical modulation (V SET decreases from -1.35 to -0.17 V with decreasing irradiation wavelength), and thermal tolerance (up to 200 degrees C). The electron-rich Cp2TiS5 layer protects the Ag-CFs, while TiO2's oxygen vacancies and unsaturated Ti atoms interact with sulfur from Cp2TiS5, lowering the Schottky barrier and facilitating charge transport. This work offers promising opportunities in flexible memristive devices for neuromorphic computing under extreme conditions.
Keyword ：
flexible memory flexible memory interfacial engineering interfacial engineering memristor memristor multilevel memory multilevel memory titanocene-polysulfide titanocene-polysulfide
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| GB/T 7714 | Zhou, Panke , Lin, Xi , Gao, Yiqun et al. Engineering Titanium Dioxide/Titanocene-Polysulfide Interface for Flexible, Optical-Modulated, and Thermal-Tolerant Multilevel Memristor [J]. | NANO LETTERS , 2025 , 25 (7) : 2741-2748 . |
| MLA | Zhou, Panke et al. "Engineering Titanium Dioxide/Titanocene-Polysulfide Interface for Flexible, Optical-Modulated, and Thermal-Tolerant Multilevel Memristor" . | NANO LETTERS 25 . 7 (2025) : 2741-2748 . |
| APA | Zhou, Panke , Lin, Xi , Gao, Yiqun , Lin, Xiaoli , Zeng, Tao , Li, Haohong et al. Engineering Titanium Dioxide/Titanocene-Polysulfide Interface for Flexible, Optical-Modulated, and Thermal-Tolerant Multilevel Memristor . | NANO LETTERS , 2025 , 25 (7) , 2741-2748 . |
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Among individuals who wear removable dentures, there is a significant likelihood, reaching up to 70 %, of experiencing a condition known as denture-induced stomatitis. To address this issue, a commonly used method involves soaking dentures in denture cleansers to eliminate microorganisms. However, the prolonged use of this cleaning method has resulted in the emergence of drug resistance. Composite antibacterial nanomaterials possess excellent chemical, physical, and antibacterial properties, not only allowing the individual components to function but sometimes also leading to synergistic effects that enhance antibacterial performance. In this study, we have successfully synthesized a new benzpyrole derivant/iodocuprate bio-nanomaterial, (TMBI)2(Cu2I4) (TMBI = 1,1,2,3-Tetramethyl-1H-benzo[e]indolium cation), that demonstrates remarkable resistance to Candida albicans, Streptococcus mutans, and dental plaque biofilm. It can effectively clean the surfaces of denture bases by removing Candida albicans, Streptococcus mutans, and dental plaque biofilm. Prolonged immersion in this material does not significantly affect the common mechanical properties of polymethyl methacrylate (PMMA) denture bases. At effective antibacterial concentrations, this nanomaterial (TMBI)2(Cu2I4) demonstrates no residual cytotoxicity on PMMA denture bases after immersion and maintains excellent hemocompatibility. These findings indicate that (TMBI)2(Cu2I4) has the potential to be a promising denture cleanser.
Keyword ：
Benzpyrole/iodocuprate hybrid Benzpyrole/iodocuprate hybrid Candida albicans Candida albicans Dental plaque Dental plaque Denture cleaner Denture cleaner Mechanical properties Mechanical properties PMMA PMMA Streptococcus mutans Streptococcus mutans
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| GB/T 7714 | Ruan, Chenglu , Huang, Xuanhao , Li, Ke et al. Antimicrobial activity and applications in PMMA of a novel benzpyrole derivant/iodocuprate hybrid (TMBI)2(Cu2I4) [J]. | BIOORGANIC CHEMISTRY , 2025 , 156 . |
| MLA | Ruan, Chenglu et al. "Antimicrobial activity and applications in PMMA of a novel benzpyrole derivant/iodocuprate hybrid (TMBI)2(Cu2I4)" . | BIOORGANIC CHEMISTRY 156 (2025) . |
| APA | Ruan, Chenglu , Huang, Xuanhao , Li, Ke , Fang, Lijuan , Li, Haohong , Zheng, Dali et al. Antimicrobial activity and applications in PMMA of a novel benzpyrole derivant/iodocuprate hybrid (TMBI)2(Cu2I4) . | BIOORGANIC CHEMISTRY , 2025 , 156 . |
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In the burgeoning sucralose (TGS) production, the separation bottleneck has hindered its further technology upgrading. In this work, the crystal structural of sucrose-6-acetate chlorination product 4,1 ',6 '-trichlorosucrose-6- acetate hydrate (TSA-6.2H2O) from multi-step recrystallization has been determined, thus the bad separation efficiency of the chlorination process was assigned to the easy incorporation of by-products into the cavities or local defects of the respirable TSA-6.2H2O network. Based on this mechanism, the second cheap organic solvents have been pre-embedded into TSA-6.2H2O to generate stable ternary solvates, i. e. TSA-6.H2Osecond solvent (second solvent = DMF (N,N'-dimethylformamide), DMAc (N, N'-dimethylacetamide), and NMP (N-methyl-2pyrrolidone)). Their cellular-type compacted arrangements were constructed from strong hydrogen bonding interactions between H2O.second solvent guests and TSA-6 networks. Consequently, the free space or local defects for the encapsulation of impurities could be inhibited completely. Upon the optimization of the crystallized process (H2O: NMP = 7: 3, solvent: TSA-6 = 12: 1, operating temperature: 288.2 K), high TSA-6 purity (99.74 % wt) and low sum of alpha x (0.023) can be achieved. Furthermore, under the guidance of ternary phase diagrams (TPD), the second solvents could be facilely removed by modulating the H2O/second solvent ratio (TSA-6 purity: 99.91 % wt in 0.5 h). In all, the clarification on the obscure mechanism and the strategy of pre-embedding second solvents have broken the separation bottleneck in TGS production, which can also be applied in other relative glycosyl halides industries.
Keyword ：
1 ' 1 ' 6 ' -trichlorosucrose-6-acetate 6 ' -trichlorosucrose-6-acetate Hydrogen bond framework Hydrogen bond framework Selective separation by solvation-induced Selective separation by solvation-induced Separation mechanism Separation mechanism Ternary phase diagrams Ternary phase diagrams
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| GB/T 7714 | Chen, Xiaoping , Lei, Jiayan , Lv, Zhoulin et al. Breaking separation bottleneck in sucralose production: Clarifying the obscure mechanism and pre-embedding second solvents for highly selective separation of chlorinated product [J]. | CHEMICAL ENGINEERING JOURNAL , 2025 , 504 . |
| MLA | Chen, Xiaoping et al. "Breaking separation bottleneck in sucralose production: Clarifying the obscure mechanism and pre-embedding second solvents for highly selective separation of chlorinated product" . | CHEMICAL ENGINEERING JOURNAL 504 (2025) . |
| APA | Chen, Xiaoping , Lei, Jiayan , Lv, Zhoulin , Chen, Zi'ang , Lin, Shitong , Guo, Zhenming et al. Breaking separation bottleneck in sucralose production: Clarifying the obscure mechanism and pre-embedding second solvents for highly selective separation of chlorinated product . | CHEMICAL ENGINEERING JOURNAL , 2025 , 504 . |
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The development of green memorizers with distinct mechanism is significant. In this work, renewable polyphenol ellagic acid (EA) and environmentally friendly calcium were used to construct a unique 3D interpenetrated bio-metal-organic framework (BioMOF), i.e. {[Ca2(EA)3(4H2O)]2H2O}n. Its high chemical stability stems from the twofold interpenetrated (6,3) bi-layers and versatile strong pi-pi stacking interactions. The memorizer FTO/{[Ca2(EA)3(4H2O)]2H2O}n/Ag exhibits good bipolar resistive switching performance with an ON/OFF ratio of 5.40 x 103 and a tolerant temperature of 300 degrees C. In particular, the local conjugated EA ligand and strong pi-pi stacking interactions in the interpenetrated 3D network are responsible for a carrier trapping/de-trapping process, rendering the excellent binary resistive switching performance. This work demonstrates a new way for the construction of green electrons by adopting renewable natural products as organic linkers. Natural product ellagic acid was used to construct a stable 3D BioMOF with twofold interpenetrated (6,3) bi-layers, which was fabricated as a biomemorizer with an ON/OFF ratio of 5.40 x 103 bearing a high working temperature of 300 degrees C.
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| GB/T 7714 | Liu, Ting-Bo , Deng, Jing-Wen , Li, Yi et al. Stable calcium ellagate metal-organic frameworks as high-performance green memorizers bearing high working temperatures [J]. | INORGANIC CHEMISTRY FRONTIERS , 2024 , 11 (10) : 3056-3062 . |
| MLA | Liu, Ting-Bo et al. "Stable calcium ellagate metal-organic frameworks as high-performance green memorizers bearing high working temperatures" . | INORGANIC CHEMISTRY FRONTIERS 11 . 10 (2024) : 3056-3062 . |
| APA | Liu, Ting-Bo , Deng, Jing-Wen , Li, Yi , Fu, Hai-Ying , Shi, Liang-Wen , Lin, Shi-Ying et al. Stable calcium ellagate metal-organic frameworks as high-performance green memorizers bearing high working temperatures . | INORGANIC CHEMISTRY FRONTIERS , 2024 , 11 (10) , 3056-3062 . |
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Purpose: To investigate the inhibition of Streptococcus mutans (S.mutans) and its biofilm by AgBr-nanoparticles (NP) @CTMAB (cetyltrimethyl-ammonium bromide) and evaluate the changes in Polymethyl methacrylate (PMMA)'s surface roughness (Ra), microhardness, and flexural strength during prolonged immersion in AgBr-NP@CTMAB for application in the denture cleaning industry. Patients and Methods: The antibacterial activity of AgBr-NP@CTMAB against S.mutans was measured colony formation assay, OD600 and laser confocal microscopy. Changes in the specimens' values for surface roughness, microhardness, and flexural strength (MPa) were measured after immersion solutions for 180 or 360 days. Results: The AgBr-NP@CTMAB solution exhibited a robust antibacterial effect on planktonic S. mutans, with a minimum bactericidal concentration of 5 mu g/mL. The 10 mu g/mL AgBr-NP@CTMAB solution efficiently inhibited S. mutans biofilm formation. (2) No significant difference in surface roughness after immersion in AgBr-NP@CTMAB (10 mu g/mL and 20 mu g/mL) comparing with distilled water (P > 0.05) and Polident had significantly higher than distilled water (P < 0.05). There was a significant decrease in the surface hardness of the PMMA specimens that were immersed in the Polident compared with those in distilled water (P < 0.05). While, no significant differences in surface hardness after immersion in the AgBr-NP@CTMAB (P > 0.05). The result of flexural strength suggested that there was no statistically significant difference (P < 0.05) between AgBr-NP@CTMAB as well as Polident and water. Conclusion: AgBrNP@CTMAB can efficiently inhibit the growth of plankton S.mutans and biofilm formation, without affecting the flexural strength, microhardness, or surface roughness of PMMA. Therefore, AgBrNP@CTMAB holds promise as a new denture cleaning agent.
Keyword ：
AgBr-NP@CTMAB AgBr-NP@CTMAB biofilm biofilm denture cleanser denture cleanser polymethyl methacrylate polymethyl methacrylate S.mutans S.mutans
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| GB/T 7714 | Huang, Jing-Jing , Jia, Lin , Zhang, Qiao-Jun et al. Anti-Microbial Effect of AgBr-NP@CTMAB on Streptococcus Mutans and Assessment of Surface Roughness Hardness and Flexural Strength of PMMA [J]. | INTERNATIONAL JOURNAL OF NANOMEDICINE , 2024 , 19 : 1273-1285 . |
| MLA | Huang, Jing-Jing et al. "Anti-Microbial Effect of AgBr-NP@CTMAB on Streptococcus Mutans and Assessment of Surface Roughness Hardness and Flexural Strength of PMMA" . | INTERNATIONAL JOURNAL OF NANOMEDICINE 19 (2024) : 1273-1285 . |
| APA | Huang, Jing-Jing , Jia, Lin , Zhang, Qiao-Jun , Li, Hao-Hong , Zheng, Da-Li , Zheng, Ming . Anti-Microbial Effect of AgBr-NP@CTMAB on Streptococcus Mutans and Assessment of Surface Roughness Hardness and Flexural Strength of PMMA . | INTERNATIONAL JOURNAL OF NANOMEDICINE , 2024 , 19 , 1273-1285 . |
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Covalent organic polymers (COPs) memristors with multilevel memory behavior in harsh environments and photoelectric regulation are crucial for high-density storage and high-efficiency neuromorphic computing. Here, a donor-acceptor (D-A)-type COP film (Py-COP-3), which is initiated by keto-enol tautomerism, is proposed for high-performance memristors. Satisfactorily, the indium tin oxide (ITO)/Py-COP-3/Ag device demonstrates multilevel memory performance, even in high temperatures, acid-base corrosion, and various organic solvents. Moreover, the performance can be modulated by the photoelectric effect to maintain a great switching behavior. By contrast, Py-COP-0, with similar structure and chemical composition to Py-COP-3 but without keto-enol tautomerism, exhibits binary storage performance. Further studies unravel that both the formation of conductive filaments and charge transfer within D-A Py-COP-3 film contribute to the resistive switching behavior of memory devices. Py-COP-n (n = 0, 3) films are rationally designed for realizing efficient multilevel memory devices in harsh environments by adjusting the content of & beta;-ketoenamine moieties readily. Moreover, the fabricated indium tin oxide/Py-COP-3/Ag memory device can be modulated by the photoelectric effect to maintain a great switching behavior.image
Keyword ：
covalent organic polymers covalent organic polymers harsh environments harsh environments keto-enol tautomerism keto-enol tautomerism memristors memristors resistive random access memory resistive random access memory
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| GB/T 7714 | Zhou, Pan-Ke , Yu, Hongling , Huang, Weiguo et al. Photoelectric Multilevel Memory Device based on Covalent Organic Polymer Film with Keto-Enol Tautomerism for Harsh Environments Applications [J]. | ADVANCED FUNCTIONAL MATERIALS , 2024 , 34 (1) . |
| MLA | Zhou, Pan-Ke et al. "Photoelectric Multilevel Memory Device based on Covalent Organic Polymer Film with Keto-Enol Tautomerism for Harsh Environments Applications" . | ADVANCED FUNCTIONAL MATERIALS 34 . 1 (2024) . |
| APA | Zhou, Pan-Ke , Yu, Hongling , Huang, Weiguo , Chee, Mun Yin , Wu, Shuo , Zeng, Tao et al. Photoelectric Multilevel Memory Device based on Covalent Organic Polymer Film with Keto-Enol Tautomerism for Harsh Environments Applications . | ADVANCED FUNCTIONAL MATERIALS , 2024 , 34 (1) . |
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Dehydroxylation of biomass-based platform molecules is critical for obtaining building blocks for use in the chemical industry. Acid catalytic dehydration has provided a feasible route. However, simultaneously pursuing high product-selective and ultra-stable catalysts for the dehydroxylation of polyols remains an open challenge. In this study, a strategy for in-situ Bronsted acid sites (BAS) with chemo-adsorption selectivity is proposed. The construction of defect sites B[3] and P[4] species has been proved to be a prerequisite for the dynamic acid site formation at hydrothermal conditions. The BPO4 catalyst with in-situ BAS can achieve the high selectivity of acrolein (similar to 80%) and robust stability of catalyst (over 425 h) using glycerol dehydration as a model reaction. In addition, in-situ BAS is highly selective for secondary hydroxyl groups and has been extended to other substrate applications. This catalytic strategy provides a green, efficient, and economical approach for converting biomassderived polyols to high-value-added chemicals.
Keyword ：
Acrolein Acrolein Biomass Biomass Dehydration Dehydration Glycerol Glycerol In -situ Br onsted acid In -situ Br onsted acid
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| GB/T 7714 | Su, Chenxin , Zhou, Shouquan , Wu, Shaoyun et al. Highly efficient dehydration of polyols: In-situ Brempty setnsted acid from boron phosphate catalyst [J]. | CHEMICAL ENGINEERING JOURNAL , 2024 , 483 . |
| MLA | Su, Chenxin et al. "Highly efficient dehydration of polyols: In-situ Brempty setnsted acid from boron phosphate catalyst" . | CHEMICAL ENGINEERING JOURNAL 483 (2024) . |
| APA | Su, Chenxin , Zhou, Shouquan , Wu, Shaoyun , Gao, Mingbin , Zhang, Weiling , Ma, Zhuang et al. Highly efficient dehydration of polyols: In-situ Brempty setnsted acid from boron phosphate catalyst . | CHEMICAL ENGINEERING JOURNAL , 2024 , 483 . |
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Dealing with multiphase systems containing solid particles in microreactor is a great challenge. Herein, microreactor with coupled oscillation technology was designed to explore clogging mechanism. The simulation revealed that no vortex was generated in the straight-tube microreactor. In the helical microreactor, the vortex could be generated and destroyed periodically. Second, the deposition clogging mechanism was explored. Solid particles were deposited and agglomerated without oscillation. After coupled oscillation, agglomerations were reduced, but deposition still existed in the straight microreactor. In the helical microreactor, the deposition phenomenon could be eliminated. Finally, the bridging clogging mechanism was explored. Solid particles were deposited first and then bridged without oscillation, forming a local high viscosity zone, and eventually completely clogging the reactor. After coupled oscillation, it was difficult to destroy the bridging behavior in the straight microreactor. In the helical microreactor, the periodic vortex could effectively destroy the bridging structure and the particles flowed uniformly.
Keyword ：
Bridging clogging Bridging clogging CFD CFD Deposition clogging Deposition clogging Liquid-solid system Liquid-solid system Microscale oscillatory flow reactor Microscale oscillatory flow reactor
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| GB/T 7714 | Liu, Jianchen , Zheng, Meiqin , Ma, Yanli et al. Microreactor with coupled oscillatory flow: Research on liquid-solid two-phase characteristics and clogging mechanism [J]. | CHEMICAL ENGINEERING SCIENCE , 2024 , 302 . |
| MLA | Liu, Jianchen et al. "Microreactor with coupled oscillatory flow: Research on liquid-solid two-phase characteristics and clogging mechanism" . | CHEMICAL ENGINEERING SCIENCE 302 (2024) . |
| APA | Liu, Jianchen , Zheng, Meiqin , Ma, Yanli , Wang, Jiawei , Li, HaoHong , Zheng, Huidong et al. Microreactor with coupled oscillatory flow: Research on liquid-solid two-phase characteristics and clogging mechanism . | CHEMICAL ENGINEERING SCIENCE , 2024 , 302 . |
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