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In this paper tantalum oxide arrays with eximious dielectric films were fabricated on the surface of a pure tantalum sheet by direct electrochemical anodic oxidation. Essential mechanism of preparaing Ta2O5by anodic oxidation was analysed. The parameters of the anodic oxidation such as different electrolyte, oxidation voltage and heat treatment influenced on properties of tantalum oxide were discussed. XRD, EDS, AFM and current testing instrument with high resistance techniques have been used to characterize the Ta2O5dielectric film. It shows that crystallization is effectively prevented when glycol is appened in the H3PO4electrolyte. The resisitant breakdown voltage is strong as oxidation voltage is between 125 and 150V in which Ta2O5dielectric films are fabricated. The intestine structure of Ta2O5films is more compact at 350°C/60 min in air atmosphere, by which the resisitant breakdown voltage of dielectric films availably enhances.
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Journal of Functional Materials
ISSN: 1001-9731
CN: 50-1099/TH
Year: 2009
Issue: 6
Volume: 40
Page: 977-980
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ESI Highly Cited Papers on the List: 0 Unfold All
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30 Days PV: 1
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