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Abstract：
Two palladium complexes of isonitrosoacetylacetoneimine, Pd (o-BrC6H4-IAI)(2) (1) and Pd (C6H5CH2-IAI)(2) (2), were synthesized and characterized by IR and Raman spectra. Complex 1 crystallizes in monoclinic system, space group P2(1)/c, with parameters: a = 0.8013 (2) nm, b = 1.8775 (4) nm, c = 0.7905(2) nm, beta = 98.22(3)degrees, V = 1.1770(5) nm(3), Z = 2, D-c = 1. 892 g.cm(-3) and F(000) = 656. The final R value is 0.0663 for 1742 observed reflections with Igreater than or equal to2sigma(I). The Pd(II) atoms have trans distorted square-planar PdN4 coordination composed of imino-nitrogen atoms and oximo-nitrogen atoms from the two Schiff base ligands.
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ACTA CHIMICA SINICA
ISSN： 0567-7351
CN： 31-1320/O6
Year： 2002
Issue： 5
Volume： 60
Page： 947-949
0 . 5 3 6
JCR@2002
1 . 7 0 0
JCR@2023
ESI Discipline： CHEMISTRY;
JCR Journal Grade：3
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WoS CC Cited Count： 1
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ESI Highly Cited Papers on the List： 0 Unfold All
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30 Days PV： 3
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