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[期刊论文]

Identification and quantitation of pyrethroid pesticide residues in vegetables by solid-phase extraction and liquid chromatography/electrospray ionization ion trap mass spectrometry

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author:

Chen, Tianwen (Chen, Tianwen.) [1] (Scholars:陈天文) | Chen, Guonan (Chen, Guonan.) [2] (Scholars:陈国南)

Indexed by:

Scopus SCIE

Abstract:

A quantitative method consisting of solid-phase extraction (SPE) followed by liquid chromatography/electrospray ionization ion trap mass spectrometry (LC/ESI-ITMS) analysis was developed for the identification and quantitation of ten pyrethroid pesticides commonly used in vegetables. The best HPLC separation was achieved using a gradient program of methanol/water mixture. For the vegetable samples, an SPE procedure to clean up the matrices was carried out prior to LC/MS analysis. Under the optimum conditions, the limits of quantification of the pyrethroid pesticides (tetramethrin, allethrin, fenpropathrin, lambda-cyhalothrin, cypermethrin, deltamethrin, fenvalerate, bioresmethrin, permethrin and bifenthrin) ranged from 0.03 to 0.1 mg kg(-1) with relative standard deviations <20%, and the mean recoveries ranged from 69.5 to 102.5%. The proposed method has been successfully applied to the determination of pyrethroids in six vegetables with satisfactory results. Copyright (C) 2007 John Wiley & Sons, Ltd.

Community:

  • [ 1 ] Fuzhou Univ, Minist Educ, Key Lab Anal & Detect Technol Food Safety, Fujian 350002, Peoples R China
  • [ 2 ] Fuzhou Univ, Dept Chem, Fujian 350002, Peoples R China
  • [ 3 ] Fuzhou Univ, Analyt & Testing Ctr, Fujian 350002, Peoples R China

Reprint 's Address:

  • 陈国南

    [Chen, Guonan]Fuzhou Univ, Minist Educ, Key Lab Anal & Detect Technol Food Safety, Fujian 350002, Peoples R China

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Source :

RAPID COMMUNICATIONS IN MASS SPECTROMETRY

ISSN: 0951-4198

Year: 2007

Issue: 12

Volume: 21

Page: 1848-1854

2 . 9 7 1

JCR@2007

1 . 8 0 0

JCR@2023

ESI Discipline: CHEMISTRY;

JCR Journal Grade:1

Cited Count:

WoS CC Cited Count: 36

SCOPUS Cited Count: 35

30 Days PV: 1

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