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Abstract:
A practical and reproducible procedure for the efficient preparation of (bpy)CuSCF3 (1), a copper reagent for trifluoromethylthiolation reaction, is reported. All reaction parameters were optimized, and reagent 1 was synthesized in 26 g scale. Finally, the utility of the reagent 1 was highlighted in the synthesis of a Toltrazuril intermediate on a preparative scale.
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ORGANIC PROCESS RESEARCH & DEVELOPMENT
ISSN: 1083-6160
Year: 2016
Issue: 4
Volume: 20
Page: 799-802
2 . 8 5 7
JCR@2016
3 . 1 0 0
JCR@2023
ESI Discipline: CHEMISTRY;
ESI HC Threshold:235
JCR Journal Grade:1
CAS Journal Grade:2
Cited Count:
WoS CC Cited Count: 0
SCOPUS Cited Count: 9
ESI Highly Cited Papers on the List: 0 Unfold All
WanFang Cited Count:
Chinese Cited Count:
30 Days PV: 0
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