Development of Multigram Scale Synthesis of Trifluoromethylthiolating Reagent: (bpy)CuSCF3 - Details

author：

Zhang, Yunxiao (Zhang, Yunxiao.) ^[1] | Gan, Kangji (Gan, Kangji.) ^[2] | Weng, Zhiqiang (Weng, Zhiqiang.) ^[3]

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Abstract：

A　practical　and　reproducible　procedure　for　the　efficient　preparation　of　(bpy)CuSCF3　(1),　a　copper　reagent　for　trifluoromethylthiolation　reaction,　is　reported.　All　reaction　parameters　were　optimized,　and　reagent　1　was　synthesized　in　26　g　scale.　Finally,　the　utility　of　the　reagent　1　was　highlighted　in　the　synthesis　of　a　Toltrazuril　intermediate　on　a　preparative　scale.　©　2016　American　Chemical　Society.

Keyword：

Chemical reactions Chemistry

Community：

[ 1 ] [Zhang, Yunxiao]State Key Laboratory of Photocatalysis on Energy and Environment, College of Chemistry, Fuzhou University, Fuzhou; 350108, China
[ 2 ] [Gan, Kangji]State Key Laboratory of Photocatalysis on Energy and Environment, College of Chemistry, Fuzhou University, Fuzhou; 350108, China
[ 3 ] [Weng, Zhiqiang]State Key Laboratory of Photocatalysis on Energy and Environment, College of Chemistry, Fuzhou University, Fuzhou; 350108, China

Reprint 's Address：

[weng, zhiqiang]state key laboratory of photocatalysis on energy and environment, college of chemistry, fuzhou university, fuzhou; 350108, china

Email：

zweng@fzu.edu.cn

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Source ：

Organic Process Research and Development

ISSN： 1083-6160

Year： 2016

Issue： 4

Volume： 20

Page： 799-802

2 . 8 5 7

JCR@2016

3 . 1 0 0

JCR@2023

ESI HC Threshold：235

JCR Journal Grade：1

CAS Journal Grade：2

Cited Count：

WoS CC Cited Count：

SCOPUS Cited Count： 9

ESI Highly Cited Papers on the List： 0 Unfold All

WanFang Cited Count：

Chinese Cited Count：

30 Days PV： 0

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