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author:

Liu, Xi (Liu, Xi.) [1] (Scholars:刘曦) | Zhuang, Kunyu (Zhuang, Kunyu.) [2] | Lin, Shi (Lin, Shi.) [3] | Zhang, Zheng (Zhang, Zheng.) [4] | Li, Xuelai (Li, Xuelai.) [5] (Scholars:李学来)

Indexed by:

Scopus SCIE

Abstract:

Understanding the crystallization behavior of ice slurry under vacuum condition is important to the wide application of the vacuum method. In this study, we first measured the supercooling degree of the initiation of ice slurry formation under different stirring rates, cooling rates and ethylene glycol concentrations. Results indicate that the supercooling crystallization pressure difference increases with increasing cooling rate, while it decreases with increasing ethylene glycol concentration. The stirring rate has little influence on supercooling crystallization pressure difference. Second, the crystallization kinetics of ice crystals was conducted through batch cooling crystallization experiments based on the population balance equation. The equations of nucleation rate and growth rate were established in terms of power law kinetic expressions. Meanwhile, the influences of suspension density, stirring rate and supercooling degree on the process of nucleation and growth were studied. Third, the morphology of ice crystals in ice slurry was obtained using a microscopic observation system. It is found that the effect of stirring rate on ice crystal size is very small and the addition of ethylene glycoleffectively inhibits the growth of ice crystals. The results in this paper can provide theoretical guidance and technical support for the development of vacuum icemakers.

Keyword:

growth rate ice slurry nucleation rate particle size supercooling degree

Community:

  • [ 1 ] [Liu, Xi]Fuzhou Univ, Sch Chem Engn, Fuzhou 350116, Peoples R China
  • [ 2 ] [Zhuang, Kunyu]Fuzhou Univ, Sch Chem Engn, Fuzhou 350116, Peoples R China
  • [ 3 ] [Lin, Shi]Fuzhou Univ, Sch Chem Engn, Fuzhou 350116, Peoples R China
  • [ 4 ] [Zhang, Zheng]Fuzhou Univ, Sch Chem Engn, Fuzhou 350116, Peoples R China
  • [ 5 ] [Li, Xuelai]Fuzhou Univ, Sch Chem Engn, Fuzhou 350116, Peoples R China

Reprint 's Address:

  • 李学来

    [Li, Xuelai]Fuzhou Univ, Sch Chem Engn, Fuzhou 350116, Peoples R China

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Source :

CRYSTALS

ISSN: 2073-4352

Year: 2017

Issue: 5

Volume: 7

2 . 1 4 4

JCR@2017

2 . 4 0 0

JCR@2023

ESI Discipline: MATERIALS SCIENCE;

ESI HC Threshold:306

JCR Journal Grade:2

CAS Journal Grade:4

Cited Count:

WoS CC Cited Count: 29

SCOPUS Cited Count: 33

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 0

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