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author:

Guo, Longhua (Guo, Longhua.) [1] | Liu, Meihua (Liu, Meihua.) [2] | Yin, Yuechun (Yin, Yuechun.) [3] | Chen, Lifen (Chen, Lifen.) [4] | Chen, Zhitao (Chen, Zhitao.) [5] | Liu, Jingjing (Liu, Jingjing.) [6] | Qiu, Bin (Qiu, Bin.) [7] (Scholars:邱彬)

Indexed by:

EI Scopus SCIE

Abstract:

In this work, a novel method based on gold nanoparticle preconcentration coupled with CE for electrochemiluminescence detection of ciprofloxacin, enrofloxacin, ofloxacin, and norfloxacin in European eels was developed. The addition of gold nanoparticles induced the rapid enrichment of fluoroquinolones, which was simpler than the conventional enrichment approaches such as solid phase extraction and solid-phase microextraction. More than 100 times enrichment was observed after gold nanoparticle aggregation-based preconcentration. The CE-electrochemiluminescence parameters that affected the separation and detection were optimized. Under the optimized conditions, the linear ranges for the four fluoroquinolones were 0.090-8.0 mu mol L-1 with the detection limits between 0.020 and 0.050 mu mol L-1. The proposed approach showed the advantages of high sensitivity, high selectivity, a wide linear range, and a low detection limit. It was used to analyze fluoroquinolones in European eel, and the results showed that the developed method can satisfy the detection requirements for fluoroquinolone determination in aquatic products set by China and the European Union.

Keyword:

Community:

  • [ 1 ] [Guo, Longhua]Fujian Normal Univ, Fuqing Branch, Fuqing 350300, Fujian, Peoples R China
  • [ 2 ] [Chen, Zhitao]Fujian Normal Univ, Fuqing Branch, Fuqing 350300, Fujian, Peoples R China
  • [ 3 ] [Liu, Jingjing]Fujian Normal Univ, Fuqing Branch, Fuqing 350300, Fujian, Peoples R China
  • [ 4 ] [Liu, Meihua]Jiaxing Univ, Coll Biol Chem Sci & Engn, Jiaxing 314001, Peoples R China
  • [ 5 ] [Chen, Lifen]Jiaxing Univ, Coll Biol Chem Sci & Engn, Jiaxing 314001, Peoples R China
  • [ 6 ] [Liu, Meihua]Fuzhou Univ, Coll Chem, Minist Educ, Key Lab Anal & Detect Technol Food Safety, Fuzhou 350116, Peoples R China
  • [ 7 ] [Yin, Yuechun]Fuzhou Univ, Coll Chem, Minist Educ, Key Lab Anal & Detect Technol Food Safety, Fuzhou 350116, Peoples R China
  • [ 8 ] [Qiu, Bin]Fuzhou Univ, Coll Chem, Minist Educ, Key Lab Anal & Detect Technol Food Safety, Fuzhou 350116, Peoples R China

Reprint 's Address:

  • 郭隆华

    [Liu, Meihua]Jiaxing Univ, Coll Biol Chem Sci & Engn, Jiaxing 314001, Peoples R China;;[Chen, Lifen]Jiaxing Univ, Coll Biol Chem Sci & Engn, Jiaxing 314001, Peoples R China;;[Liu, Meihua]Fuzhou Univ, Coll Chem, Minist Educ, Key Lab Anal & Detect Technol Food Safety, Fuzhou 350116, Peoples R China

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Source :

ANALYTICAL METHODS

ISSN: 1759-9660

Year: 2020

Issue: 21

Volume: 12

Page: 2693-2702

2 . 8 9 6

JCR@2020

2 . 7 0 0

JCR@2023

ESI Discipline: CHEMISTRY;

ESI HC Threshold:160

JCR Journal Grade:2

CAS Journal Grade:3

Cited Count:

WoS CC Cited Count: 4

SCOPUS Cited Count: 4

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 1

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