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学者姓名：叶炳火
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Abstract ：
本发明涉及一种以改性铝土矿为载体制备钌基水煤气变换催化剂的方法，将改性铝土矿与RuCl3溶液分三次进行等体积浸渍，每次浸渍后进行过滤、烘干，第三次烘干后制成以改性铝土矿为载体的钌基水煤气变换催化剂。本发明制备过程简单，可以充分利用我国具有丰富的铝土矿资源，可大幅度降低催化剂的生产成本，且制备的催化剂负载量低，催化活性高，使用寿命长，具有广阔的应用前景。
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| GB/T 7714 | 江莉龙 , 杨阳 , 叶炳火 et al. 一种以改性铝土矿为载体制备钌基水煤气变换催化剂的方法 : CN201010301121.1[P]. | 2010/2/3 . |
| MLA | 江莉龙 et al. "一种以改性铝土矿为载体制备钌基水煤气变换催化剂的方法" : CN201010301121.1. | 2010/2/3 . |
| APA | 江莉龙 , 杨阳 , 叶炳火 , 魏明灯 , 魏可镁 . 一种以改性铝土矿为载体制备钌基水煤气变换催化剂的方法 : CN201010301121.1. | 2010/2/3 . |
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以改性铝土矿为载体, 采用等体积浸渍法, 制备了Ni-Mn-Ce-k体系水煤气变换催化剂. 通过TG、 DTA 、 TPR和活性表征等方法, 系统考察了制备和还原条件对催化剂水煤气变换性能的影响. 结果表明: 催化剂的优化制备工艺为: 第一步浸渍组分Ni、 Mn、 Ce的盐溶液(其摩尔配比为8:7:4), 焙烧温度500 ℃, 第二步浸渍K的加入量为5%(W), 还原最高温度为500 ℃, 还原过程添加适量的水蒸气, 制得的催化剂具有良好的催化性能和热稳定性能, 优于国内外现行工业产品.
Keyword ：
Ni-Mn-Ce Ni-Mn-Ce 制备参数 制备参数 水煤气变换催化剂 水煤气变换催化剂 还原条件 还原条件 铝土矿 铝土矿
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| GB/T 7714 | 江莉龙 , 杨阳 , 叶炳火 et al. Ni-Mn-Ce-K/铝土矿催化剂的制备和还原条件对水煤气变换性能的影响 [J]. | 分子催化 , 2010 , 24 (2) : 147-152 . |
| MLA | 江莉龙 et al. "Ni-Mn-Ce-K/铝土矿催化剂的制备和还原条件对水煤气变换性能的影响" . | 分子催化 24 . 2 (2010) : 147-152 . |
| APA | 江莉龙 , 杨阳 , 叶炳火 , 魏可镁 . Ni-Mn-Ce-K/铝土矿催化剂的制备和还原条件对水煤气变换性能的影响 . | 分子催化 , 2010 , 24 (2) , 147-152 . |
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Abstract ：
以福建漳浦铝土矿为原料,采用水热法,制备具有高比表面积的铝土矿载体;并以其为载体,通过浸渍法获得不同Pt含量的催化剂,应用于一氧化碳氧化反应。采用XRF、低温N2吸附、XRD,和活性评价对铝土矿载体和催化剂的活性进行了表征,并对比表面积增大的原因进行了探讨。结果表明:原矿经130℃温度下水热反应72h,550℃焙烧4h后,所制得的铝土矿比表面积比原矿增大了2.7倍,为153m2·g-1,孔容量为0.20mL·g-1,最可几孔主要在3nm左右。其原因为原矿中的主要成分高岭石在水热作用下,转化为水铝氧(Gibbsite,Al(OH)3),再经焙烧转化为氧化铝.CO氧化反应研究结果表明该催化剂有较好...
Keyword ：
CO氧化 CO氧化 水热法 水热法 载体 载体 铝土矿 铝土矿
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| GB/T 7714 | 江莉龙 , 杨阳 , 叶炳火 et al. 高比表面积的铝土矿载体制备及其在CO氧化反应中的应用 [J]. | 化工进展 , 2009 , 28 (S2) : 417 . |
| MLA | 江莉龙 et al. "高比表面积的铝土矿载体制备及其在CO氧化反应中的应用" . | 化工进展 28 . S2 (2009) : 417 . |
| APA | 江莉龙 , 杨阳 , 叶炳火 , 魏可镁 . 高比表面积的铝土矿载体制备及其在CO氧化反应中的应用 . | 化工进展 , 2009 , 28 (S2) , 417 . |
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| GB/T 7714 | 江莉龙 , 杨阳 , 叶炳火 et al. 高比表面积的铝土矿载体制备及其在CO氧化反应中的应用 [C] //中国化工学会2009年年会暨第三届全国石油和化工行业节能节水减排技术论坛会议论文集(下) . 2009 . |
| MLA | 江莉龙 et al. "高比表面积的铝土矿载体制备及其在CO氧化反应中的应用" 中国化工学会2009年年会暨第三届全国石油和化工行业节能节水减排技术论坛会议论文集(下) . (2009) . |
| APA | 江莉龙 , 杨阳 , 叶炳火 , 魏可镁 . 高比表面积的铝土矿载体制备及其在CO氧化反应中的应用 中国化工学会2009年年会暨第三届全国石油和化工行业节能节水减排技术论坛会议论文集(下) . (2009) . |
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In this study, VO2 rods with a rectangular cross-section have successfully been synthesized using a simple hydrothermal route in the absence of templates or catalysts. The synthesized rods were characterized by the X-ray diffraction (XRD), scanning electron microscope (SEM) and transmission electron micrographs (TEM) measurements. It was found that the rods are single crystal and the size ranges from several tens nanometers to several micrometers. Furthermore, a possible model, nucleating-growing-splitting, was proposed for the formation of rods with a rectangular cross-section. (C) 2008 Elsevier B.V. All rights reserved.
Keyword ：
Growth models Growth models Hydrothermal crystal growth Hydrothermal crystal growth Nucleation Nucleation
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| GB/T 7714 | Jiang, Lilong , Wei, Mingdeng , Ye, Binghuo et al. VO2 rods with a rectangular cross-section [J]. | JOURNAL OF CRYSTAL GROWTH , 2008 , 310 (19) : 4301-4304 . |
| MLA | Jiang, Lilong et al. "VO2 rods with a rectangular cross-section" . | JOURNAL OF CRYSTAL GROWTH 310 . 19 (2008) : 4301-4304 . |
| APA | Jiang, Lilong , Wei, Mingdeng , Ye, Binghuo , Wei, Kemei . VO2 rods with a rectangular cross-section . | JOURNAL OF CRYSTAL GROWTH , 2008 , 310 (19) , 4301-4304 . |
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Single-crystal V2O5 nanowires were successfully synthesized from the starting materials V6O13 powder and water. The experimental results indicate that high purity nanowires can be obtained using this simple synthetic route in absence of templates or catalysts. The diameter of the nanowires was found to be ca. 20 similar to 60 nm and the length up to several tens of micrometers, and the phases of nanowires were determined by XRD and TEM measurements.
Keyword ：
Nanowires Nanowires Single-Crystal Single-Crystal V2O5 V2O5
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| GB/T 7714 | Gao, Shaokang , Chen, Yuzhen , Luo, Haiyan et al. Single-Crystal Vanadium Pentoxide Nanowires [J]. | JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY , 2008 , 8 (7) : 3500-3503 . |
| MLA | Gao, Shaokang et al. "Single-Crystal Vanadium Pentoxide Nanowires" . | JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY 8 . 7 (2008) : 3500-3503 . |
| APA | Gao, Shaokang , Chen, Yuzhen , Luo, Haiyan , Jiang, Lilong , Ye, Binghuo , Wei, Mingdeng et al. Single-Crystal Vanadium Pentoxide Nanowires . | JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY , 2008 , 8 (7) , 3500-3503 . |
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A multiple-metal (Ni-Cu-Mn-K/Al2O3) catalyst was prepared by impregnated method. The effects of technology parameters and global kinetics on the water gas shift reaction using this catalyst were investigated. The results of technology parameters showed that the increase of the vapor/gas (v/g) radio enhanced CO conversion, the optimum v/g radio for was gas shift reaction was from 0.8 to 1.5. The space velocity had only a negligible effect on the CO conversion, revealing a good operating flexibility for the catalyst in the water gas shift reaction process. With the reaction temperature rising, there was an extreme operating temperature for CO conversion around 400°C. Its global kinetics was also investigated in an internal-circulation gradientless reactor, and a power law type global kinetics model for the water gas shift reaction using this catalyst was regressed by the non-linear square method. The results based on the global kinetics model were in very good agreement with the experimental data. It is demonstrated that the model is liable and suitable.
Keyword ：
Alumina Alumina Carbon monoxide Carbon monoxide Catalysts Catalysts Chemical reactions Chemical reactions Coal gas Coal gas Impregnation Impregnation Regression analysis Regression analysis Water Water
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| GB/T 7714 | Jiang, Lilong , Ye, Binghuo , Wei, Kemei et al. Study on the technology parameters and the global kinetics of Ni-Cu-Mn-K/Al2O3 catalyst for high-temperature water gas shift reaction [J]. | Journal of Basic Science and Engineering , 2008 , 16 (2) : 270-279 . |
| MLA | Jiang, Lilong et al. "Study on the technology parameters and the global kinetics of Ni-Cu-Mn-K/Al2O3 catalyst for high-temperature water gas shift reaction" . | Journal of Basic Science and Engineering 16 . 2 (2008) : 270-279 . |
| APA | Jiang, Lilong , Ye, Binghuo , Wei, Kemei , Lin, Cheng . Study on the technology parameters and the global kinetics of Ni-Cu-Mn-K/Al2O3 catalyst for high-temperature water gas shift reaction . | Journal of Basic Science and Engineering , 2008 , 16 (2) , 270-279 . |
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Multiple-metal catalysts (Ni-Mn-Ce-K/bauxite) for Water-Gas Shift (WGS) reaction were prepared by impregnation, and the catalytic structure and properties were investigated by N-2 physical, XRD, H-2-TPR, and CO-TPD. The results indicated that the addition of 7.5% CeO2 improved the activity of the WGS reaction obviously, and also increased the specific surface area and pore volume of the catalysts. The addition of CeO2 decreases the reduction temperature, enhanced the adsorption and activation of H2O, and improved the adsorption content of CO. Besides, active sites were not changed and the number of active sites on catalysts did not increase obviously.
Keyword ：
bauxite bauxite CeO2 CeO2 impregnated impregnated rare earths rare earths water-gas shift water-gas shift
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| GB/T 7714 | Jiang Lilong , Ye Binghuo , Wei Kemei . Effects of CeO2 on structure and properties of Ni-Mn-K/bauxite catalysts for water-gas shift reaction [J]. | JOURNAL OF RARE EARTHS , 2008 , 26 (3) : 352-356 . |
| MLA | Jiang Lilong et al. "Effects of CeO2 on structure and properties of Ni-Mn-K/bauxite catalysts for water-gas shift reaction" . | JOURNAL OF RARE EARTHS 26 . 3 (2008) : 352-356 . |
| APA | Jiang Lilong , Ye Binghuo , Wei Kemei . Effects of CeO2 on structure and properties of Ni-Mn-K/bauxite catalysts for water-gas shift reaction . | JOURNAL OF RARE EARTHS , 2008 , 26 (3) , 352-356 . |
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Brookite-type TiO2 nanotubes with crystalline multilayer walls have been synthesized for the first time via a simple hydrothermal route.
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| GB/T 7714 | Deng, Qixin , Wei, Mingdeng , Ding, Xiaokun et al. Brookite-type TiO2 nanotubes [J]. | CHEMICAL COMMUNICATIONS , 2008 , (31) : 3657-3659 . |
| MLA | Deng, Qixin et al. "Brookite-type TiO2 nanotubes" . | CHEMICAL COMMUNICATIONS 31 (2008) : 3657-3659 . |
| APA | Deng, Qixin , Wei, Mingdeng , Ding, Xiaokun , Jiang, Lilong , Ye, Binghuo , Wei, Kemei . Brookite-type TiO2 nanotubes . | CHEMICAL COMMUNICATIONS , 2008 , (31) , 3657-3659 . |
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Keyword ：
一氧化碳 一氧化碳 体积比 体积比 侧流试验 侧流试验 催化剂活性 催化剂活性 副反应 副反应 变换工段 变换工段 合成氨厂 合成氨厂 工业在线 工业在线 改性 改性 机械强度 机械强度 永安 永安 热稳定性能 热稳定性能 等体积浸渍法 等体积浸渍法 节能效果 节能效果 装置 装置 试生产 试生产 载体 载体 运行 运行 铝土矿 铝土矿 高温变换催化剂 高温变换催化剂
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| GB/T 7714 | 江莉龙 , 叶炳火 , 魏可镁 et al. 改性铝土矿为载体的Ni-Mn-K一氧化碳高温变换催化剂工业侧流试验 [C] //第五届全国工业催化技术与应用年会论文集(上册) . 2008 . |
| MLA | 江莉龙 et al. "改性铝土矿为载体的Ni-Mn-K一氧化碳高温变换催化剂工业侧流试验" 第五届全国工业催化技术与应用年会论文集(上册) . (2008) . |
| APA | 江莉龙 , 叶炳火 , 魏可镁 , 邢一德 , 张建萍 . 改性铝土矿为载体的Ni-Mn-K一氧化碳高温变换催化剂工业侧流试验 第五届全国工业催化技术与应用年会论文集(上册) . (2008) . |
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