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学者姓名：陈崇启
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Abstract ：
Ammonia is a carbon-free energy carrier with 17.6 wt% hydrogen content. The design of an efficient and compact ammonia decomposition reactor based on low-temperature catalysts is the key to realizing industrial hydrogen production from ammonia. In this work, a multiscale model was developed by bridging the particle-scale characteristics of catalysts and reactor performances, to fully comprehend the ammonia decomposition process. The effects of catalyst porosity and pore diameters on the reactor size, precious metal loading, and the profile of temperature and heat flux were systematically evaluated. An improved reactor design was further proposed by applying the segmented reactor packed with two-stage egg-shell-type low-temperature catalysts, which decreased the precious metal usage by 61.6% and the temperature drop by 42.9 K. This segmentation strategy balanced the reaction rate and heat flux, indicating a significant potential in highly efficient, economical, and reliable hydrogen production from ammonia.
Keyword ：
ammonia decomposition ammonia decomposition catalyst micro-structure catalyst micro-structure hydrogen production hydrogen production multiscale model multiscale model precious metal reduction precious metal reduction
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| GB/T 7714 | Zhang, Lixuan , Wu, Yifan , Huang, Wenshi et al. Multiscale modeling of a low-temperature NH3 decomposition reactor for precious metal reduction and temperature control [J]. | AICHE JOURNAL , 2025 . |
| MLA | Zhang, Lixuan et al. "Multiscale modeling of a low-temperature NH3 decomposition reactor for precious metal reduction and temperature control" . | AICHE JOURNAL (2025) . |
| APA | Zhang, Lixuan , Wu, Yifan , Huang, Wenshi , Lin, Li , Wang, Luqiang , Wu, Zeyun et al. Multiscale modeling of a low-temperature NH3 decomposition reactor for precious metal reduction and temperature control . | AICHE JOURNAL , 2025 . |
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Ammonia decomposition is a promising approach for on-site hydrogen generation for fuel cells, and the development of a cost-effective and efficient catalyst is highly desired. In this study, a series of NixMg75-xAl25 hydrotalcite-like compounds (HTlc) with different Ni contents were synthesized by co-precipitation, followed by calcination and reduction treatments. Influences of Ni content and ammonia reduction on the catalytic performance for ammonia decomposition were investigated. The characterization results of the as-prepared samples showed that HTlc was decomposed into Mg(Ni, Al)O solid solution by calcination, which displayed a strong interaction between Ni species and support, while upon reduction with ammonia at 750 degrees C, well-dispersed Ni metal nanoparticles with an average crystallite size range of 5.9-7.7 nm were formed. No nitrogen oxides (NOx) were produced during the NH3 reduction process as indicated by mass spectrometry analysis, and the catalyst reduced with ammonia showed comparable activity with that reduced with hydrogen, suggesting that ammonia can be used as a reductant gas. The catalyst activity increased with the increase of Ni content and reduction temperature. Among the catalysts, the Ni20Mg55Al25 catalyst reduced with ammonia at 750 degrees C showed the best activity, which afforded 98% ammonia conversion at 600 degrees C at a space velocity of 30000 mLg(cat)(-1)h(-1), and no evident deactivation was observed during a 100 h test, demonstrating good activity, stability, and sintering resistance.
Keyword ：
ammonia decomposition ammonia decomposition hydrogen production hydrogen production hydrotalcite-like compound hydrotalcite-like compound nickel catalyst nickel catalyst
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| GB/T 7714 | Lian, Minli , Su, Jiaxin , Huang, Hongyang et al. Supported Ni Catalysts from Ni-Mg-Al Hydrotalcite-like Compounds: Preparation and Catalytic Performance for Ammonia Decomposition [J]. | JOURNAL OF INORGANIC MATERIALS , 2025 , 40 (1) : 53-60 . |
| MLA | Lian, Minli et al. "Supported Ni Catalysts from Ni-Mg-Al Hydrotalcite-like Compounds: Preparation and Catalytic Performance for Ammonia Decomposition" . | JOURNAL OF INORGANIC MATERIALS 40 . 1 (2025) : 53-60 . |
| APA | Lian, Minli , Su, Jiaxin , Huang, Hongyang , Ji, Yuyin , Deng, Haifan , Zhang, Tong et al. Supported Ni Catalysts from Ni-Mg-Al Hydrotalcite-like Compounds: Preparation and Catalytic Performance for Ammonia Decomposition . | JOURNAL OF INORGANIC MATERIALS , 2025 , 40 (1) , 53-60 . |
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An effective B-site doping strategy through heterovalent ions was developed to synthesize a series of pyrochlore Pr2Zr1.95X0.05O7+delta (PZX, X = Mn, Sc, Sn, Nb, Mo, Al, Ga, In) for the direct ammonia solid oxide fuel cell (DA-SOFC) cathode. To guide the design of efficient cathodes for DA-SOFC, we explore the relationships between the ionic radius/valence of dopant and electrochemical performance. In view of the energy matching and interaction between the dopant and the host lattice, the substitution of trivalent Sc3+ with similar ionic radius for tetravalent Zr4+ can greatly improve the oxygen reduction reaction activity of Pr2Zr2O7 due to the reduced bond energy of 48f-oxygen ions in octahedral [ZrO6] units. As a result, the anode-supported single cell Ni-YSZ|YSZ|PZSc-60YSZ yields an output power density of 0.44 and 1.45 Wcm(-2) at 600 and 800 degrees C with ammonia fuel, outperforming PZX (X = Mn, Sn, Nb, Mo, Al, Ga, In) and common La0.8Sr0.2MnO3 (LSM)-based DA-SOFC. The detailed characterizations are employed to gain insight into the structure-activity relationship and reaction mechanism.
Keyword ：
Direct ammonia solid oxide fuel cell Direct ammonia solid oxide fuel cell Distribution of relaxation time Distribution of relaxation time Pyrochlore Pyrochlore Structural distortion Structural distortion
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| GB/T 7714 | Fang, Huihuang , Yang, Shiqing , Ye, Weijie et al. Mechanism insight into enhanced oxygen reduction reaction over heterovalent ion incorporated pyrochlore Pr2Zr2O7 for direct ammonia solid oxide fuel cells [J]. | CHEMICAL ENGINEERING SCIENCE , 2024 , 290 . |
| MLA | Fang, Huihuang et al. "Mechanism insight into enhanced oxygen reduction reaction over heterovalent ion incorporated pyrochlore Pr2Zr2O7 for direct ammonia solid oxide fuel cells" . | CHEMICAL ENGINEERING SCIENCE 290 (2024) . |
| APA | Fang, Huihuang , Yang, Shiqing , Ye, Weijie , Zhong, Fulan , Luo, Yu , Wang, Shaorong et al. Mechanism insight into enhanced oxygen reduction reaction over heterovalent ion incorporated pyrochlore Pr2Zr2O7 for direct ammonia solid oxide fuel cells . | CHEMICAL ENGINEERING SCIENCE , 2024 , 290 . |
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Molybdate-intercalated magnesium–aluminum hydrotalcite-like compounds (HTlc) were synthesized by anion-exchange and used as precursor to prepare supported molybdenum nitride catalyst for ammonia decomposition. The as-synthesized precursors and the derived mixed metal oxides and nitride catalysts were characterized by ICP, XRD, Raman spectroscopy, XPS, H2-TPR, and HAADF-STEM-EDX. The characterizations indicated that molybdate was well intercalated into the HTlc interlayer as MoO42– and the Mo content was tunable by altering the intercalation degree of molybdate. Upon calcination, molybdena was dominantly presented as isolated tetrahedrally coordinated MoOx species. Upon nitridation with ammonia at 700 ºC, highly dispersed and composition-uniform molybdenum nitride (Mo2±xN) was formed. The Mo0.5Mg3Al nitride catalyst showed good activity for ammonia decomposition, providing nearly full conversion of ammonia at 625 ºC under a space velocity of 5,000 mL gcat–1 h–1. The optimal catalyst also exhibited high catalytic stability during 100 h operation at 625 ºC, and no obvious aggregation took place, attributable to the strong metal–support interaction between molybdenum nitride and Mg–Al mixed oxide. It is suggested that the hydrotalcite-derived Mg–Al mixed oxide supported highly dispersed Mo2±xN species was active and stable for ammonia decomposition. © 2024 Elsevier B.V.
Keyword ：
Alumina Alumina Aluminum nitride Aluminum nitride Aluminum oxide Aluminum oxide Ammonia Ammonia Catalyst activity Catalyst activity Hydrogen production Hydrogen production Magnesium compounds Magnesium compounds Molybdenum oxide Molybdenum oxide Nitrides Nitrides
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| GB/T 7714 | Wei, Xiaofeng , Su, Jiaxin , Xie, Guanbao et al. Supported highly dispersed molybdenum nitride derived from molybdate-intercalated Mg‒Al hydrotalcite-like compounds as a catalyst for ammonia decomposition [J]. | Molecular Catalysis , 2024 , 562 . |
| MLA | Wei, Xiaofeng et al. "Supported highly dispersed molybdenum nitride derived from molybdate-intercalated Mg‒Al hydrotalcite-like compounds as a catalyst for ammonia decomposition" . | Molecular Catalysis 562 (2024) . |
| APA | Wei, Xiaofeng , Su, Jiaxin , Xie, Guanbao , Lian, Minli , Huang, Hongyang , Chen, Chongqi et al. Supported highly dispersed molybdenum nitride derived from molybdate-intercalated Mg‒Al hydrotalcite-like compounds as a catalyst for ammonia decomposition . | Molecular Catalysis , 2024 , 562 . |
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Ammonia decomposition for onsite hydrogen production has been regarded as an important reaction which links to efficient hydrogen storage, transport and utilization. However, it still remains challenging to develop efficient catalysts with robust stability for ammonia decomposition. Herein, an integrated strategy was employed to synthesize Ru/SiO2@N-CS via wrapping a thin layer of N-doped carbon onto the SiO2 sphere, following the anchor of Ru nanoparticles (NPs) onto the support. The obtained Ru/SiO2@N-CS (Ru loading: 1 wt%) shows a promising performance for ammonia decomposition, reaching 94.5 % at 550 °C with a gas hourly space velocity (GHSV) of 30 000 mL gcat-1h−1. The combination of the SiO2 as the core prevents the degradation of N-doped carbon layers and then enhance the durability of the catalysts, remaining stable after 50 h at evaluated temperatures. Adequate characterizations were used to illustrate the effect of microchemical environment on ammonia decomposition activity of Ru/SiO2@N-CS catalyst under different calcination atmosphere and the correlation between structure and performance. © 2024 Elsevier B.V.
Keyword ：
Ammonia decomposition Ammonia decomposition N-doped carbon N-doped carbon Ruthenium Ruthenium SiO2 SiO2 Stability Stability
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| GB/T 7714 | Huang, Y. , Ren, H. , Fang, H. et al. Ru nanoparticles embedded in Ru/SiO2@N-CS for boosting hydrogen production via ammonia decomposition with robust lifespan [J]. | Applied Surface Science , 2024 , 669 . |
| MLA | Huang, Y. et al. "Ru nanoparticles embedded in Ru/SiO2@N-CS for boosting hydrogen production via ammonia decomposition with robust lifespan" . | Applied Surface Science 669 (2024) . |
| APA | Huang, Y. , Ren, H. , Fang, H. , Ouyang, D. , Chen, C. , Luo, Y. et al. Ru nanoparticles embedded in Ru/SiO2@N-CS for boosting hydrogen production via ammonia decomposition with robust lifespan . | Applied Surface Science , 2024 , 669 . |
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The ammonia decomposition for the production of carbon-free hydrogen has triggered great attention yet still remains challenging due to its sluggish kinetics, posting the importance of precise design of efficient catalysts for ammonia decomposition under low temperatures. Constructing the metal-support interaction and interface is one of the most important strategies for promoting catalysts. In this work, by coating ceria onto the Ni nanoparticles (NPs), we discover that the Ni-CeO2 interfaces create an exceptional effect to enhance the catalytic decomposition of ammonia by over 10 folds, compared with the pristine Ni. The kinetic analysis demonstrates that the recombinative N2 desorption is the rate-determining step (RDS) and the Ni-CeO2 interface greatly increases the RDS. Based on these understandings, a strategy to fabricate the Ni/CeO2 catalyst with abundant Ni-Ce-O interfaces via one-pot sol-gel method was employed (hereafter denoted to s-Ni/CeO2). The s-Ni/CeO2 catalyst shows a high activity for ammonia decomposition, achieving a H2 formation rate of 10.5 mmol gcat-1 min-1 at 550 degrees C. Combined with a series of characterizations, the relationship between the catalyst structure and the performance was investigated for further understanding the effect of metal-oxide interfaces.
Keyword ：
Ammonia decomposition Ammonia decomposition Cerium oxide Cerium oxide Metal -oxide interfaces Metal -oxide interfaces Metal-support interaction Metal-support interaction Nickel Nickel
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| GB/T 7714 | Chen, Jiangping , Ren, Hongju , Wu, Kai et al. Boosting hydrogen production of ammonia decomposition via the construction of metal-oxide interfaces [J]. | CHINESE JOURNAL OF STRUCTURAL CHEMISTRY , 2024 , 43 (2) . |
| MLA | Chen, Jiangping et al. "Boosting hydrogen production of ammonia decomposition via the construction of metal-oxide interfaces" . | CHINESE JOURNAL OF STRUCTURAL CHEMISTRY 43 . 2 (2024) . |
| APA | Chen, Jiangping , Ren, Hongju , Wu, Kai , Fang, Huihuang , Chen, Chongqi , Lin, Li et al. Boosting hydrogen production of ammonia decomposition via the construction of metal-oxide interfaces . | CHINESE JOURNAL OF STRUCTURAL CHEMISTRY , 2024 , 43 (2) . |
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【目的】在“双碳”背景下，氨作为无碳富氢的能源载体，体积能量密度高、易液化存储，具有广阔的发展前景。然而复杂的储运环境增加了液氨储罐和管道腐蚀的风险，因此，研究复杂输送环境下液氨腐蚀问题是“氨-氢”能源基础设施制造和安全服役的关键。【方法】通过综述液氨腐蚀的研究进展，探讨了不同环境、不同材料的氨腐蚀行为和应力腐蚀开裂机制。同时，总结了相关氨腐蚀检测方法和具体防护措施，并展望了未来氨腐蚀研究的发展方向。【结果】氧气、碳氧化合物、硫化物及氯化物的混入对氨腐蚀有促进作用，而水杂质对氨腐蚀的影响具有两面性；应力能够引起液氨应力腐蚀开裂，不同材料的应力腐蚀敏感性从大到小依次为铜及其合金、高强钢、碳钢。【结论】基于国内对液氨腐蚀行为机理尚不明确、氨腐蚀防护措施有待完善等问题，提出以下建议：(1)采用实验研究、仿真模拟等方法，探究多杂质关联作用下不同材质的液氨腐蚀行为和内在腐蚀机理；(2)需结合液氨管道实际输送环境及材料失效特征，开展管线钢及焊材-液氨临界失效边界检验与腐蚀风险评价；(3)从液氨储罐及管道的设计、选材、制造、使用等多个角度，结合多种腐蚀防腐措施，形成完善的液氨储运系统腐蚀控制、防护及评价标准体系。（图5，表2，参77）
Keyword ：
应力腐蚀 应力腐蚀 液氨储运 液氨储运 环境腐蚀 环境腐蚀 腐蚀检测 腐蚀检测 防护技术 防护技术
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| GB/T 7714 | 李加庆 , 冯智雨 , 梁辉龙 et al. 复杂输送环境下液氨腐蚀行为及防护技术研究进展 [J]. | 油气储运 , 2024 , 43 (02) : 121-133,162 . |
| MLA | 李加庆 et al. "复杂输送环境下液氨腐蚀行为及防护技术研究进展" . | 油气储运 43 . 02 (2024) : 121-133,162 . |
| APA | 李加庆 , 冯智雨 , 梁辉龙 , 尹鹏博 , 滕霖 , 陈崇启 et al. 复杂输送环境下液氨腐蚀行为及防护技术研究进展 . | 油气储运 , 2024 , 43 (02) , 121-133,162 . |
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Developing efficient and robust catalysts for hydrogen production by ammonia decomposition is of importance towards the "zero-carbon" economy. Herein, a series of B-site Ni- and Co-doped A-site-deficient SrTiO3 perovskite (Sr0.9Ti0.8Ni0.1Co0.1O3-delta, STNC) with the in situ exsolution of NiCo nano-alloys were fabricated under reducing atmosphere. The Ni-Co/STO (SrTiO3) catalyst derived from STNC shows much higher activity for ammonia decomposition than those Ni and Ni-Co based catalysts fabricated by impregnation. The STNC derived sample can produce 32.6 mmol gcat-1 & sdot;min- 1 hydrogen at 600 degrees C, 2.2 and 1.9 fold higher than those of Ni/STO and Ni-Co/STO. Furthermore, the synthesis methods including the Pechini, hydrothermal and ball milling methods were investigated for the preparation of the exsoluted Ni-Co catalysts toward ammonia decomposition. The STNC-HT catalyst by hydrothermaldemonstrated an excellent performance and reached 70% and a near equilibrium conversion of ammonia under 600 and 650 degrees C with a WHSV of 30,000 mL gcat between structure and performance was further studied by a series of characterizations. In addition, the STNC-HT catalyst was employed in the direct ammonia solid oxide fuel cells, in which the performance is closely related to the ammonia decomposition activity, and shows a satisfying power density of 99.3 mW cm- 2. Generally, we identified an approach to engineer catalysts with enhanced activity for the ammonia utilization as energy vectors in our work.
Keyword ：
Ammonia decomposition Ammonia decomposition Hydrogen Hydrogen In-situ exsolution In-situ exsolution Ni-Co alloy Ni-Co alloy Perovskite Perovskite Synthesis method Synthesis method
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| GB/T 7714 | Ren, Hongju , Zhi, Guo , Chen, Chongqi et al. In situ exsolution of Ni-Co alloys from A-site-deficient perovskite for efficient ammonia decomposition [J]. | INTERNATIONAL JOURNAL OF HYDROGEN ENERGY , 2024 , 96 : 385-395 . |
| MLA | Ren, Hongju et al. "In situ exsolution of Ni-Co alloys from A-site-deficient perovskite for efficient ammonia decomposition" . | INTERNATIONAL JOURNAL OF HYDROGEN ENERGY 96 (2024) : 385-395 . |
| APA | Ren, Hongju , Zhi, Guo , Chen, Chongqi , Fang, Huihuang , Lin, Zhihong , Lin, Li et al. In situ exsolution of Ni-Co alloys from A-site-deficient perovskite for efficient ammonia decomposition . | INTERNATIONAL JOURNAL OF HYDROGEN ENERGY , 2024 , 96 , 385-395 . |
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Low-temperature direct ammonia fuel cell via ammonia oxidation reaction (AOR) is one of the most attractive ways for ammonia utilization. The Pt-Ir alloyed catalysts have been proven greatly efficient in AOR to overcome the sluggish kinetics and complex multi-electron processes; however, it still remains challenging for further improvement because of the complexity of alloyed types and unclear fundamental understanding. Herein, we systematically fabricated a series of PtxIry/XC-72 catalysts via tuning the Pt/Ir compositions and these catalysts demonstrate significant composition-dependent behaviours in AOR, whereas the Pt favours increasing current densities and the Ir facilitates reducing onset potentials. Importantly, the actual surface Pt/Ir atomic configuration is totally different with the classic view for homogeneous alloys by combining catalytic and characteristic analyses. The Pt prefers to be segregated on the topmost surface. Then the quantified correlations between current density/onset potential and Pt composition in Pt - Ir nanoparticles (NPs) were further established and discussed. The onset potential of AOR is significantly reduced by Ir incorporation while it is insensitive to Ir contents. Accordingly, the well-studied Pt5Ir5/XC-72 catalyst was further employed in an alkaline exchange membrane fuel cell, exhibiting a peak power density (230.0 mW cm-2). Our work provides insights into the effect of Pt/Ir compositions on AOR, with the goal of catalysts engineering for AOR and ammonia fuel cells.
Keyword ：
Ammonia oxidation reaction Ammonia oxidation reaction Bimetallic alloys Bimetallic alloys Direct ammonia fuel cells Direct ammonia fuel cells Iridium Iridium Platinum Platinum
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| GB/T 7714 | Fang, Huihuang , Liao, Chen , Cai, Quanying et al. Tuning surficial atomic configuration of Pt-Ir catalysts for efficient ammonia oxidation and low-temperature direct ammonia fuel cells [J]. | CHEMICAL ENGINEERING SCIENCE , 2023 , 280 . |
| MLA | Fang, Huihuang et al. "Tuning surficial atomic configuration of Pt-Ir catalysts for efficient ammonia oxidation and low-temperature direct ammonia fuel cells" . | CHEMICAL ENGINEERING SCIENCE 280 (2023) . |
| APA | Fang, Huihuang , Liao, Chen , Cai, Quanying , Zhong, Fulan , Lin, Li , Chen, Chongqi et al. Tuning surficial atomic configuration of Pt-Ir catalysts for efficient ammonia oxidation and low-temperature direct ammonia fuel cells . | CHEMICAL ENGINEERING SCIENCE , 2023 , 280 . |
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Pyrochlore oxide A(2)B(2)O(7) is a potential anode catalyst of ammonia-fed solid oxide fuel cell (SOFC) due to its unique and open structure that can make some oxygen ions flow to occupy the hole position to form Frankel defect. Herein, various rare-earth ions with different radius are selected as the A site to construct defective pyrochlore oxide RE2Zr1.95Ni0.05O7+delta (REZN, RE = La, Pr, Nd, Sm, Gd, LZN/PZN/NZN/SZN/GZN) to gain insights into oxygen vacancies that can be the diffusion and adsorption active site for ammonia. In the n-type semiconductor REZN, the degree of crystal ordering decreases with the decrease of the radius of rare-earth RE3+ ions. Among them, GZN exhibits the most negative conduction band and the smallest band gap, making it easier to overcome the energy potential barrier and facilitate the movement of carriers. As a result, the conductivity of GZN is about 25 times higher than that of LZN. The average TEC value of GZN is 10.40 x 10(-6) K-1, which matches that of electrolyte YSZ (10.50 x 10(-6) K-1). The maximum power density of ammonia-fed SOFC supported by YSZ electrolyte based on GZN anode is 128.63 mW center dot cm(-2) at 800 degrees C, which is 2.3 times higher than that of NiO-based SOFC. The single cell based on GZN anode can be run continuously for 100 h at 800 degrees C without significant degradation. The preliminary results suggest that GZN oxide is promising to be a candidate catalyst for ammonia-fed SOFC anode.
Keyword ：
Ammonia-fed solid oxide fuel cell Ammonia-fed solid oxide fuel cell Ammonia oxidation Ammonia oxidation Electrochemical performance Electrochemical performance Geometry distortion Geometry distortion RE2Zr1.95Ni0.05O7+delta anode RE2Zr1.95Ni0.05O7+delta anode
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| GB/T 7714 | Zhong, Fulan , Wang, Xinmin , Wang, Lei et al. Tuning geometry distortion of pyrochlore RE2Zr1.95Ni0.05O7+delta anodes with rich oxygen vacancies for ammonia-fed solid oxide fuel cell [J]. | SEPARATION AND PURIFICATION TECHNOLOGY , 2023 , 312 . |
| MLA | Zhong, Fulan et al. "Tuning geometry distortion of pyrochlore RE2Zr1.95Ni0.05O7+delta anodes with rich oxygen vacancies for ammonia-fed solid oxide fuel cell" . | SEPARATION AND PURIFICATION TECHNOLOGY 312 (2023) . |
| APA | Zhong, Fulan , Wang, Xinmin , Wang, Lei , Fang, Huihuang , Luo, Yu , Chen, Chongqi et al. Tuning geometry distortion of pyrochlore RE2Zr1.95Ni0.05O7+delta anodes with rich oxygen vacancies for ammonia-fed solid oxide fuel cell . | SEPARATION AND PURIFICATION TECHNOLOGY , 2023 , 312 . |
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