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学者姓名：方圣琼
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Abstract ：
The formidable challenge of membrane fouling and wetting, spurred by the elevated concentration of pollutants in the landfill leachate concentrate during membrane distillation, necessitates substantial costs on membrane cleaning for retaining high separation efficiency. Herein, a durable superhydrophobic poly(vinylidene fluoride) (PVDF) membrane constructed by spray-coating of fluorinated SiO2 nanoparticles was proposed to treat landfill leachate concentrate via membrane distillation. The influence of operational parameters, including transmembrane temperature difference, feed flow rate, and feed salinity, on the membrane distillation performance was explored. Specifically, the increased transmembrane temperature difference and feed flow rate had a strongly positive dependence on the permeation flux during membrane distillation. The superhydrophobic PVDF membrane showed impressive antiwetting and antifouling properties, as indicated by consistently stable superhydrophobicity, obtaining an extremely high rejection of salts and humic substances (>99.99%) over an 8 h membrane distillation for treating landfill leachate concentrate. Furthermore, the tested superhydrophobic PVDF membrane yielded a complete solute removal, resulting in high-quality freshwater production with a 90.13% pure water recovery from landfill leachate concentrate during a 50 h membrane distillation-based concentration procedure with a concentration factor of 10.13. These results manifested the superhydrophobic PVDF membrane as a promising avenue for pure water production from complex waste streams via membrane distillation.
Keyword ：
concentration concentration desalination and purification desalination and purification direct contact membranedistillation direct contact membranedistillation landfill leachate concentrate landfill leachate concentrate superhydrophobic PVDF membrane superhydrophobic PVDF membrane
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| GB/T 7714 | Yu, Fan , Yu, Zijian , Huang, Xuan et al. Effective Membrane Distillation of Landfill Leachate Concentrate Using a Superhydrophobic SiO2/PVDF Membrane for Resource Recovery [J]. | ACS ES&T WATER , 2024 , 4 (4) : 1711-1719 . |
| MLA | Yu, Fan et al. "Effective Membrane Distillation of Landfill Leachate Concentrate Using a Superhydrophobic SiO2/PVDF Membrane for Resource Recovery" . | ACS ES&T WATER 4 . 4 (2024) : 1711-1719 . |
| APA | Yu, Fan , Yu, Zijian , Huang, Xuan , Gu, Ailiang , Du, Jiale , Xie, Shuangling et al. Effective Membrane Distillation of Landfill Leachate Concentrate Using a Superhydrophobic SiO2/PVDF Membrane for Resource Recovery . | ACS ES&T WATER , 2024 , 4 (4) , 1711-1719 . |
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Substantial discharge of industrial oily wastewater calls for an efficient and sustainable treatment for resource recovery. Superwetting membranes offer a feasible approach to fractionate oil species and water from oily wastewater for addressing this technical challenge. In this study, we proposed a useful strategy for constructing a superhydrophilic membrane with superior antibacterial properties through rapid co-deposition of dopamine and 3-aminopropyltriethoxysilane (APTS) initiated by ammonium persulfate on the Cu nanoparticles-loaded porous PVDF substrate. The resultant superhydrophilic membrane yielded an underwater oil contact angle of 163.5(degrees), enabling a fast and robust gravity-driven filtration for various oil-in-water emulsions with a separation efficiency of >99.9 %. Additionally, incorporating of Cu nanoparticles and polydopamine endowed the superhydrophilic membrane with superior antibacterial activity (100 % inhibition efficiency against Escherichia coli), and thereby remarkably enhancing the anti-biofouling performance. This study provides a viable approach to design highperformance membranes for separation of oil-in-water emulsions, with promising applications in the industrial and environmental sectors.
Keyword ：
Antibacteria Antibacteria Cu nanoparticles Cu nanoparticles Mussel-inspired polydopamine coating Mussel-inspired polydopamine coating Oil -in -water emulsions Oil -in -water emulsions Superhydrophilic membrane Superhydrophilic membrane
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| GB/T 7714 | Lin, Yingying , Yu, Fan , Yu, Zijian et al. Mussel-inspired superhydrophilic and antibacterial membranes for effective gravity-driven separation of oil-in-water emulsions [J]. | SEPARATION AND PURIFICATION TECHNOLOGY , 2024 , 341 . |
| MLA | Lin, Yingying et al. "Mussel-inspired superhydrophilic and antibacterial membranes for effective gravity-driven separation of oil-in-water emulsions" . | SEPARATION AND PURIFICATION TECHNOLOGY 341 (2024) . |
| APA | Lin, Yingying , Yu, Fan , Yu, Zijian , Lin, Xiaoyan , Lin, Fang , Liu, Riri et al. Mussel-inspired superhydrophilic and antibacterial membranes for effective gravity-driven separation of oil-in-water emulsions . | SEPARATION AND PURIFICATION TECHNOLOGY , 2024 , 341 . |
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In recent studies, carbon nanotube (CNTs) materials and their composites have demonstrated remarkable catalytic activity in the activation of persulfate (PS), facilitating the efficient degradation of organic pollutants. In this study, a novel Co loaded carbon nanotubes (CoO@CNT) catalyst was prepared to promote PDS activation for the degradation of sulfafurazole (SIZ). Experimental results, the CNT as a carrier effectively reduces the leaching of cobalt ions and improves the electron transport capacity ,whereas the introduced Co effectively activates the PDS, promoting the generation of highly reactive radicals to degrade SIZ. Under optimized conditions (a catalyst dose of 0.2 g/L, a PDS dose of 1 g/L and an initial pH = 9.0), the obtained CoO@CNT demonstrated favorable Fenton-like performance, reaching a degradation efficiency of 95.55% within 30 min. Furthermore, density functional theory (DFT) calculations demonstrate that the introduction of cobalt (Co) accelerates electron transfer, promoting the decomposition of PDS while facilitating the Co 2 + /Co 3 + redox cycling. We further employed the environmental chemistry and risk assessment system (ECOSAR) to evaluate the ecological toxicity of intermediate products, revealing a significant reduction in ecological toxicity associated with this degradation process, thereby confirming its environmental harmlessness. Through batch experiments and studies, we gained a comprehensive understanding of the mechanism and influencing factors of CoO@CNT in the role of SIZ degradation, and provided robust support for evaluating the ecological toxicity of degradation products. This study provides a significant strategy for the development of efficient catalysts incorporating Co for the environmentally friendly degradation of organic pollutants.
Keyword ：
CoO CoO DFT DFT Ecotoxicity Ecotoxicity Persulfate activation Persulfate activation Sulfisoxazole Sulfisoxazole
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| GB/T 7714 | Liu, Qingsong , Zhou, Bin , Zheng, Caihong et al. The CoO-doped carbon nanotubes enhance electronic performance and effectively activate persulfate for the degradation of sulfafurazole [J]. | ENVIRONMENTAL RESEARCH , 2024 , 251 . |
| MLA | Liu, Qingsong et al. "The CoO-doped carbon nanotubes enhance electronic performance and effectively activate persulfate for the degradation of sulfafurazole" . | ENVIRONMENTAL RESEARCH 251 (2024) . |
| APA | Liu, Qingsong , Zhou, Bin , Zheng, Caihong , Wang, Dong , Ge, Yao , Fang, Shengqiong . The CoO-doped carbon nanotubes enhance electronic performance and effectively activate persulfate for the degradation of sulfafurazole . | ENVIRONMENTAL RESEARCH , 2024 , 251 . |
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For the efficient degradation of organic pollutants with the goal of reducing the water environment pollution, we employed an alkaline hydrothermal treatment on primeval g-C3N4 to synthesize a hydroxyl-grafted g-C3N4 (CN-0.5) material, from which we engineered a novel Fenton-like catalyst, known as Cu–CN-0.5. The introduction of numerous hydroxyl functional groups allowed the CN-0.5 substrate to stably fix active copper oxide particles through surface complexation, resulting in a low Cu leaching rate during a Cu–CN-0.5 Fenton-like process. A sequence of characterization techniques and theoretical calculations uncovered that interfacial complexation induced charge redistribution on the Cu–CN-0.5 surface. Specifically, some of the π electrons in the tris-s-triazine units were transferred to the copper oxide particles along the newly formed chemical bonds (C(π)-O-Cu), forming a π-deficient area on the tris-s-triazine plane near the complexation site. In a typical Cu–CN-0.5 Fenton-like process, a stable π-π interaction was established due to the favorable positive-negative match of electrostatic potential between the aromatic pollutants and π-deficient areas, leading to a significant improvement in Cu–CN-0.5's adsorption capacity for aromatic pollutants. Furthermore, pollutants also delivered electrons to the Cu–CN-0.5 Fenton-like system via a “through-space” approach, which suppressed the futile oxidation of H2O2 in reducing the high-valent Cu2+ and significantly improved the generation efficiency of •OH with high oxidative capacity. As expected, Cu–CN-0.5 not only exhibited an efficient Fenton degradation for several typical aromatic organic pollutants, but also demonstrated both a low metal leaching rate (0.12 mg/L) and a H2O2 utilization rate exceeding 80%. The distinctive Fenton degradation mechanism substantiated the potential of the as-prepared material for effective wastewater treatment applications. © 2024
Keyword ：
Alkaline hydrothermal treatment Alkaline hydrothermal treatment Fenton Fenton g-C3N4 g-C3N4 Interfacial regulation Interfacial regulation
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| GB/T 7714 | Zhou, B. , Liu, Q. , Zheng, C. et al. Enhanced Fenton-like catalysis via interfacial regulation of g-C3N4 for efficient aromatic organic pollutant degradation [J]. | Environmental Pollution , 2024 , 356 . |
| MLA | Zhou, B. et al. "Enhanced Fenton-like catalysis via interfacial regulation of g-C3N4 for efficient aromatic organic pollutant degradation" . | Environmental Pollution 356 (2024) . |
| APA | Zhou, B. , Liu, Q. , Zheng, C. , Ge, Y. , Huang, L. , Fu, H. et al. Enhanced Fenton-like catalysis via interfacial regulation of g-C3N4 for efficient aromatic organic pollutant degradation . | Environmental Pollution , 2024 , 356 . |
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Membrane distillation (MD) has been widely used for resource recovery from high-salinity wastewater, due to its superior technical merits of high separation efficiency and potential integration of low-grade heat. Herein, a robust superhydrophobic PVDF membrane prepared by spray-coating of fluorinated silica nanoparticles was employed to treat highly saline dye wastewater by MD. Specifically, impacts of operation conditions, including temperature difference, feed flow-rate, salinity, dye concentration, and dye species, on MD performance of the fabricated superhydrophobic PVDF membrane were comprehensively investigated. The increase of temperature difference and feed flow-rate had a positive effect on the MD flux of the membrane. Conversely, the rise in salinity and dye concentration induced an adverse impact on the MD flux. Furthermore, the superhydrophobic PVDF membrane showed a strong robustness in treating complex streams, as demonstrated by consistently stable MD flux using various dye/NaCl mixed solutions. Due to the robust surface superhydrophobicity, the fabricated PVDF membrane exhibited impressive antiwetting and antifouling properties against highly saline dye wastewater, consistently stable permeation flux, and high dye/salt removal efficiency (>99.99%). Moreover, the superhydrophobic membrane showed a high water recovery (90%) from highly saline dye wastewater with a slight reduction (13.4%) in permeation flux during a 39 h MD filtration. These results signify the promising practicability of the fabricated superhydrophobic PVDF membrane in sustainable management of highly saline dye wastewater via MD. © 2022 American Chemical Society.
Keyword ：
antiwetting and antifouling antiwetting and antifouling desalination desalination highly saline dye wastewater highly saline dye wastewater membrane distillation membrane distillation superhydrophobic membrane superhydrophobic membrane
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| GB/T 7714 | Xie, S. , Du, J. , Huang, X. et al. Water Recovery from Highly Saline Dye Wastewater by Membrane Distillation Using a Superhydrophobic SiO2/PVDF Membrane [J]. | ACS ES and T Water , 2023 , 3 (7) : 1893-1901 . |
| MLA | Xie, S. et al. "Water Recovery from Highly Saline Dye Wastewater by Membrane Distillation Using a Superhydrophobic SiO2/PVDF Membrane" . | ACS ES and T Water 3 . 7 (2023) : 1893-1901 . |
| APA | Xie, S. , Du, J. , Huang, X. , Gu, A. , Fang, S. , Liu, R. et al. Water Recovery from Highly Saline Dye Wastewater by Membrane Distillation Using a Superhydrophobic SiO2/PVDF Membrane . | ACS ES and T Water , 2023 , 3 (7) , 1893-1901 . |
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Conventional membrane processes, e.g., microfiltration and ultrafiltration, suffer from severe permeation flux decline and fouling during the oily wastewater treatment. The superhydrophilic surface decoration provides an important and effective strategy to address this challenge. Herein, a surperhydrophilic/underwater superoleophobic nanocomposite surface with the photocatalytic properties was constructed via one-step facile vacuum-assisted filtration of a g-C3N4 nanosheet/SiO2 nanoparticle dispersion onto a microfiltration membrane substrate. Specifically, with the intercalation of 20 mg.L-1 SiO2 nanoparticles into the g-C3N4 nanosheets, the g-C3N4/SiO2 composite membrane showed the superhydrophilic/underwater superoleophobic properties with an underwater oil contact angle of 170.0 +/- 0.3 degrees. Such a g-C3N4/SiO2 composite membrane yielded a permeation flux of >1290 LMH.bar(-1) with an oil rejection of >99.91% during the vacuum filtration of oil-in-water emulsions. The g-C3N4/SiO2 composite membrane significantly outperformed the pristine microfiltration substrate that had severe fouling caused by oil blockage. Additionally, the g-C3N4/SiO2 composite membrane not only effectively retained the E. coli bacteria through size exclusion effect, but also promoted the inactivation of bacteria via visible-light photocatalysis. Therefore, our membrane has a great promise in practical oily wastewater treatment due to its excellent separation performance and biofouling resistance.
Keyword ：
Bacteria inactivation Bacteria inactivation g-C3N4/SiO2 nanocomposite g-C3N4/SiO2 nanocomposite Oil-in-water emulsion separation Oil-in-water emulsion separation Superhydrophilic membrane Superhydrophilic membrane Visible-light photocatalysis Visible-light photocatalysis
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| GB/T 7714 | Ye, Wenyuan , Chen, Jinjie , Kong, Na et al. Superhydrophilic photocatalytic g-C3N4/SiO2 composite membranes for effective separation of oil-in-water emulsion and bacteria removal [J]. | SEPARATION AND PURIFICATION TECHNOLOGY , 2022 , 290 . |
| MLA | Ye, Wenyuan et al. "Superhydrophilic photocatalytic g-C3N4/SiO2 composite membranes for effective separation of oil-in-water emulsion and bacteria removal" . | SEPARATION AND PURIFICATION TECHNOLOGY 290 (2022) . |
| APA | Ye, Wenyuan , Chen, Jinjie , Kong, Na , Fang, Qingyuan , Hong, Mingqiu , Sun, Yuxiang et al. Superhydrophilic photocatalytic g-C3N4/SiO2 composite membranes for effective separation of oil-in-water emulsion and bacteria removal . | SEPARATION AND PURIFICATION TECHNOLOGY , 2022 , 290 . |
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Removal of copper ions (Cu(II)) efficiently from water is crucial for water environment security. We use sustainable, low-cost, renewable cellulose derivatives (carboxymethylcellulose sodium (CMC-Na)) and polyvinyl alcohol (PVA) as the matrix, and cellulose nanocrystals (CNCs) as the functional addition. The CNC/CMC-Na/PVA hydrogel was prepared by the physical cross-linking method. Static adsorption experiments proved that CNC/CMC-Na/PVA hydrogel has a greater adsorption potential (108 mg/g) towards Cu(II). At the same time, the adsorption of Cu(II) on CNC/CMC-Na/PVA hydrogels is spontaneous and endothermic, and obeys the pseudo-second-order model with intra-particle diffusion. Furthermore, the primary adsorption mechanisms had been electrostatic attraction and surface complexation. Importantly, CNC/CMC-Na/PVA hydrogel has efficient absorbability and preferable reusability in actual water samples. Furthermore, the copper nanoparticles (Cu NPs) adsorbed on the surface of CNC/CMC-Na/PVA hydrogels were reduced with NaBH4 in situ to realize the secondary utilization in CNC/CMC-Na/PVA hydrogels supported by Cu NPs. It is found that the material can be used as a catalyst to efficiently catalyze the conversion of HMF to BHMF (99%). Consequently, we provide insights into the hydrogel preparation that would possibly be promising novel adsorbents for the elimination of heavy-ion from sustainable water purification. [GRAPHICS] .
Keyword ：
Adsorption kinetics Adsorption kinetics Catalyze Catalyze Cellulose nanocrystal Cellulose nanocrystal Copper Copper Hydrogel Hydrogel
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| GB/T 7714 | Wang, Huiqiang , Fang, Shengqiong , Zuo, Miao et al. Removal of copper ions by cellulose nanocrystal-based hydrogel and reduced adsorbents for its catalytic properties [J]. | CELLULOSE , 2022 , 29 (8) : 4525-4537 . |
| MLA | Wang, Huiqiang et al. "Removal of copper ions by cellulose nanocrystal-based hydrogel and reduced adsorbents for its catalytic properties" . | CELLULOSE 29 . 8 (2022) : 4525-4537 . |
| APA | Wang, Huiqiang , Fang, Shengqiong , Zuo, Miao , Li, Zheng , Yu, Xin , Tang, Xing et al. Removal of copper ions by cellulose nanocrystal-based hydrogel and reduced adsorbents for its catalytic properties . | CELLULOSE , 2022 , 29 (8) , 4525-4537 . |
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Recently, highly efficient activation of peroxymonosulfate (PMS) by S-doped cobalt-based catalysts are receiving increased attention. The effect of S is worth exploring since it has a great influence on PMS activation perfor-mance. In this work, dimethyl sulfoxide was adopted as an S source and loaded on bamboo biochar (BB) with Co to form CoS/BBC, which served as an efficient catalyst for PMS activation to degrade sulfamethoxazole (SMX). The experiment results showed that CoS/BBC exhibits an excellent catalytic activity and the SMX (20 mg/L) can be completely degraded under the attack of species of center dot OH, SO4-center dot,1O2 and electron transfer. The SMX degradation conformed to pseudo first-order kinetics with rate constant reaching 0.442 min-1 in 10 min under the optimal conditions (a catalyst dose of 0.02 g/L, a PMS dose of 0.3 g/L and an initial pH = 7.0). The electrochemical experiments and density functional theory (DFT) calculation revealed that the introduction of S can accelerate electron transfer and promote the decomposition of PMS while facilitating Co(III)/Co(II) redox cycling. Furthermore, liquid chromatograph-mass spectrometer (LC-MS) and ecological structure activity relationships (ECOSAR) proved that the degradation process of SMX in CoS/BBC/PMS system has low ecotoxicity and is harmless to the environment. This work provides a new strategy for enhancing electron transfer by S-doped metal materials and the synthesis of efficient catalysts for SMX removal.
Keyword ：
DFT DFT Ecotoxicity Ecotoxicity Peroxymonosulfate activation Peroxymonosulfate activation S -doped S -doped Sulfamethoxazole Sulfamethoxazole
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| GB/T 7714 | Huang, Xiaoyi , Yu, Zhendong , Shi, Yanbiao et al. Highly efficient activation of peroxymonosulfate by Co, S co-doped bamboo biochar for sulfamethoxazole degradation: Insights into the role of S [J]. | JOURNAL OF ENVIRONMENTAL CHEMICAL ENGINEERING , 2022 , 10 (5) . |
| MLA | Huang, Xiaoyi et al. "Highly efficient activation of peroxymonosulfate by Co, S co-doped bamboo biochar for sulfamethoxazole degradation: Insights into the role of S" . | JOURNAL OF ENVIRONMENTAL CHEMICAL ENGINEERING 10 . 5 (2022) . |
| APA | Huang, Xiaoyi , Yu, Zhendong , Shi, Yanbiao , Liu, Qingsong , Fang, Shengqiong . Highly efficient activation of peroxymonosulfate by Co, S co-doped bamboo biochar for sulfamethoxazole degradation: Insights into the role of S . | JOURNAL OF ENVIRONMENTAL CHEMICAL ENGINEERING , 2022 , 10 (5) . |
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Using chicken manure as raw material to prepare activated carbon as a dispersant, a novel biochar-loaded nano-zerovalent iron composite (nZVI@CMBC) was developed and applied to remove hexavalent chromium, i.e., Cr(VI), in wastewater. The dispersion of nano-zerovalent iron (nZVI) particles on the surface of chicken manure-derived biochar (CMBC) successfully inhibited the aggregation of magnetic iron particles and effectively reduced the size of nZVI particles. The results demonstrated that under acidic conditions, the removal efficiency of Cr(VI) by the nZVI@CMBC composite could reach 124.12 mg g(-1). The pseudosecond-order kinetic model had a good agreement with the adsorption kinetics of the nZVI@CMBC composite, implying that the adsorption of Cr(VI) is based on the multi-layer chemical adsorption. Therefore, this study provides a new clue and strategy for removing Cr(VI) in wastewater.
Keyword ：
adsorption adsorption biochar biochar Cr(VI) Cr(VI) nanoscale zerovalent iron nanoscale zerovalent iron reduction reduction
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| GB/T 7714 | Fang, Shengqiong , Huang, Xiaoyi , Xie, Shuangling et al. Removal of Chromium (VI) by a Magnetic Nanoscale Zerovalent Iron-Assisted Chicken Manure-Derived Biochar: Adsorption Behavior and Synergetic Mechanism [J]. | FRONTIERS IN BIOENGINEERING AND BIOTECHNOLOGY , 2022 , 10 . |
| MLA | Fang, Shengqiong et al. "Removal of Chromium (VI) by a Magnetic Nanoscale Zerovalent Iron-Assisted Chicken Manure-Derived Biochar: Adsorption Behavior and Synergetic Mechanism" . | FRONTIERS IN BIOENGINEERING AND BIOTECHNOLOGY 10 (2022) . |
| APA | Fang, Shengqiong , Huang, Xiaoyi , Xie, Shuangling , Du, Jiale , Zhu, Jianlong , Wang, Kai et al. Removal of Chromium (VI) by a Magnetic Nanoscale Zerovalent Iron-Assisted Chicken Manure-Derived Biochar: Adsorption Behavior and Synergetic Mechanism . | FRONTIERS IN BIOENGINEERING AND BIOTECHNOLOGY , 2022 , 10 . |
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Sulfate-radical-based wastewater treatment has re-ceived great interest due to its high-level efficiency. However, the preparation of stable and recyclable nanocatalysts remains a challenge. Herein, a highly efficient catalyst (FeCo/SC) for persulfate activation is successfully synthesized via dispersing S and Fe into carbon skeletons derived from ZIF-67. After the introduction of S, FeCo/SC exhibited excellent catalytic performance. With the action of SO4-center dot, Fe(VI), and 1O2, the degradation efficiency of carbamazepine (CBZ) (10 mg L-1) could be up to 97.9 +/- 2% within 10 min. The results showed that the larger surface area after S doping decreases the electron transfer resistance. The S0/S2- is beneficial for promoting the Fe(III)-to-Fe(II) and Co(III)-to-Co(II) conversion cycle. Moreover, the liquid chromatograph-mass spectrometer (LC-MS), density functional theory (DFT), and ecological structure-activity relationships (ECOSAR) revealed the possible degradation pathway of CBZ, which was a toxicity attenuation process. In consequence, this work offers an innovative scheme for researching the effect of trace S-doped bimetallic oxide nanoparticles on PDS heterogeneous catalytic systems.
Keyword ：
carbamazepine carbamazepine DFT calculation DFT calculation ecotoxicity ecotoxicity peroxydisulfate activation peroxydisulfate activation sulfur sulfur
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| GB/T 7714 | Huang, Xiaoyi , Liu, Qingsong , Zhu, Jianlong et al. Trace Sulfur Accelerated Peroxydisulfate Activation Based on a ZIF-67-Derived Nanostructure for Carbamazepine Degradation [J]. | ACS APPLIED NANO MATERIALS , 2022 . |
| MLA | Huang, Xiaoyi et al. "Trace Sulfur Accelerated Peroxydisulfate Activation Based on a ZIF-67-Derived Nanostructure for Carbamazepine Degradation" . | ACS APPLIED NANO MATERIALS (2022) . |
| APA | Huang, Xiaoyi , Liu, Qingsong , Zhu, Jianlong , Gao, Yanxin , Fang, Shengqiong , Bi, Jinhong . Trace Sulfur Accelerated Peroxydisulfate Activation Based on a ZIF-67-Derived Nanostructure for Carbamazepine Degradation . | ACS APPLIED NANO MATERIALS , 2022 . |
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