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学者姓名：何春娴
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Abstract ：
高校实验室是科技创新和人才培养的摇篮,科学的实验室管理方式能够充分发挥实验室功能,也是提高教学质量,完成实验任务的根本保障。在结合实验室工作实际情况的基础上,借鉴国内外科研院所实验室建设经验,分析了高校实验室管理工作中的问题和不足,从实验室信息化建设、开放实验室建设、实验室安全建设等方面探讨实验室的管理方法和管理模式。以提高实验室管理效率,更好地服务于教学科研工作,为聚力福州大学“双一流”建设提供实验室支持。
Keyword ：
信息化 信息化 实验室安全 实验室安全 实验平台 实验平台 设备共享 设备共享
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| GB/T 7714 | 何春娴 , 陈星伟 , 林珍珍 et al. 高校实验平台管理模式探索 [J]. | 实验室科学 , 2024 , 27 (01) : 182-184,188 . |
| MLA | 何春娴 et al. "高校实验平台管理模式探索" . | 实验室科学 27 . 01 (2024) : 182-184,188 . |
| APA | 何春娴 , 陈星伟 , 林珍珍 , 丁正新 . 高校实验平台管理模式探索 . | 实验室科学 , 2024 , 27 (01) , 182-184,188 . |
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Abstract ：
本发明公开了一种含稀土元素的硫化物光催化剂及其制备方法和应用，采用简单的水热法或溶剂热法制备含稀土元素的硫化物催化剂，并将其应用于光催化CO2还原体系中。本发明的制备方法简单易行、温和低能耗。制得的催化剂具有显著提高光催化CO2还原性能，且产物选择性高的优点，在光催化领域具有较广泛的应用前景，同时也为新型光催化剂的制备提供了新的思路。
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| GB/T 7714 | 丁正新 , 王文静 , 何春娴 et al. 一种含稀土元素的硫化物光催化剂及其制备方法和应用 : CN202210039689.3[P]. | 2022-01-14 00:00:00 . |
| MLA | 丁正新 et al. "一种含稀土元素的硫化物光催化剂及其制备方法和应用" : CN202210039689.3. | 2022-01-14 00:00:00 . |
| APA | 丁正新 , 王文静 , 何春娴 , 魏芬 , 韩世同 , 龙金林 et al. 一种含稀土元素的硫化物光催化剂及其制备方法和应用 : CN202210039689.3. | 2022-01-14 00:00:00 . |
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Abstract ：
建立了高效液相色谱-四极杆-飞行时间质谱(HPLC-Q-TOF MS)法分析宁夏枸杞根皮的主要化学成分.采用 Agilent ZORBAX Extend C18 柱(250 mm×4.6 mm×5 μm),以水(含 10 mmol/L 醋酸铵)-乙腈为流动相进行等度洗脱,流速1.0 mL/min,柱温30℃,进样量5 μL;电喷雾离子源正、负离子模式检测,质量扫描范围m/z 100～300和300～2 000.利用数据转换软件将原始数据转换成mzXML格式,在GNPS上建立分子网络,并运用Cytoscape软件对结果进行可视化解读,结合文献数据推测化合物结构.通过手动检索发现了宁夏枸杞根皮中的21个化合物,与已报道的枸杞根皮中化合物一致.通过分子网络化聚类分析发现11个化合物,为地骨皮中首次报道,其中化合物24和25为新发现的环九肽类化合物.该方法可快速分析宁夏枸杞根皮的化学成分,为其质量控制奠定基础.
Keyword ：
分子网络化 分子网络化 宁夏枸杞根皮 宁夏枸杞根皮 高效液相色谱-四极杆-飞行时间质谱(HPLC-Q-TOF MS) 高效液相色谱-四极杆-飞行时间质谱(HPLC-Q-TOF MS)
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| GB/T 7714 | 何春娴 , 陈靖枝 , 杨静玲 et al. 基于HPLC-Q-TOF MS的网络化技术对宁夏枸杞根皮的化学成分研究 [J]. | 质谱学报 , 2022 , 43 (6) : 792-803 . |
| MLA | 何春娴 et al. "基于HPLC-Q-TOF MS的网络化技术对宁夏枸杞根皮的化学成分研究" . | 质谱学报 43 . 6 (2022) : 792-803 . |
| APA | 何春娴 , 陈靖枝 , 杨静玲 , 李舂龙 , 马晓莉 , 南泽东 et al. 基于HPLC-Q-TOF MS的网络化技术对宁夏枸杞根皮的化学成分研究 . | 质谱学报 , 2022 , 43 (6) , 792-803 . |
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Abstract ：
In the past decades, systematic isolation and structural identification of chemical components from plant material, especially traditional Chinese medicine, have provided a large number of chemical drugs and lead structures for clinic. However, there are still a large number of trace components in traditional Chinese medicine with novel chemical structures and specific pharmacological activities, which need to be further analyzed. With the development of modern analytical technology, the network technology based on tandem mass spectrometry and cluster analysis shows many advantages in trace analysis of complex components. In this paper, a method of high-performance liquid chromatography quadrupole time-of-flight mass spectrometry (HPLC-Q-TOF MS) was developed for the analysis of the main chemical constituents in the root bark of Lycium barbarum L. The aqueous extract sample was separated by methanol aqueous through C18-solid phase extraction, and then the 50% methanol aqueous elution was analyzed using HPLC-Q-TOF MS with C18 column. The ions were monitored in both positive mode and negative mode of ESI with the scanning ranges of m/z 100-300 and 300-2 000. The trace chemical components were analyzed by molecular network technology. The MS data files were converted to the mzXML format and the molecular network was generated on GNPS, then visualized with Cytoscape, and the structures of compounds were predicted based on literature data. Twenty one known compounds in Cortex Lycii were verified by manual analysis technique and eleven new components were firstly identified by molecular networking. It is worth reporting that compound 24 and 25 are different from cyclooctapeptides previously found in the root bark of Lycium chinense (another source of Cortex Lycii), indicating that they can be used as markers for the identification of two species of Cortex Lycii. This work lays a research foundation for promoting the effective application of Lycium barbarum L. root bark. © 2022 Chinese Society for Mass Spectrometry. All rights reserved.
Keyword ：
Cluster analysis Cluster analysis Extraction Extraction High performance liquid chromatography High performance liquid chromatography Inductively coupled plasma Inductively coupled plasma Mass spectrometry Mass spectrometry Medicine Medicine Methanol Methanol Phase separation Phase separation Plants (botany) Plants (botany) Structure (composition) Structure (composition) Trace analysis Trace analysis
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| GB/T 7714 | He, Chun-Xian , Chen, Jing-Zhi , Yang, Jing-Ling et al. Analysis of Chemical Constituents in the Root Bark of Lycium barbarum L. by HPLC-Q-TOF MS Combined with Networking [J]. | Journal of Chinese Mass Spectrometry Society , 2022 , 43 (6) : 792-803 . |
| MLA | He, Chun-Xian et al. "Analysis of Chemical Constituents in the Root Bark of Lycium barbarum L. by HPLC-Q-TOF MS Combined with Networking" . | Journal of Chinese Mass Spectrometry Society 43 . 6 (2022) : 792-803 . |
| APA | He, Chun-Xian , Chen, Jing-Zhi , Yang, Jing-Ling , Li, Chong-Long , Ma, Xiao-Li , Nan, Ze-Dong et al. Analysis of Chemical Constituents in the Root Bark of Lycium barbarum L. by HPLC-Q-TOF MS Combined with Networking . | Journal of Chinese Mass Spectrometry Society , 2022 , 43 (6) , 792-803 . |
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