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学者姓名：温娜
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Abstract ：
When the AlCl3/toluene system is employed as a catalyst, the vulcanized rubber obtained from the dodecanedioic acid (DA)-based vulcanization of epoxidized natural rubber (ENR) can be effectively decrosslinked at 160 degrees C over a period of 18 h. The reclaimed rubber can subsequently be revulcanized using DA, thereby demonstrating favorable recyclability and mechanical properties (tensile strength is 2.5 MPa, elongation at break is 91.6% and the rate of degradation is 100%). During the reaction process, AlCl3 coordinates with the carbonyl oxygen atoms within the cross-linking network, facilitating a nucleophilic substitution reaction between water (as the nucleophile) and ester groups. This reaction leads to the formation of hydroxyl groups, some of which undergo dehydration to form carbon-carbon double bonds. Through comprehensive characterization of the reclaimed rubber and model compounds, the plausible decrosslinking mechanism of the vulcanizate was elucidated.
Keyword ：
Cross-linking Cross-linking Epoxidized natural rubber Epoxidized natural rubber Model compounds Model compounds Recycle Recycle Sulfur-free vulcanization Sulfur-free vulcanization
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| GB/T 7714 | Chen, Bingshen , Ke, Jinhuang , Lin, Tengfei et al. Chemical Recovery and Decrosslinking Mechanism of Dodecanedioic Acid-Cured Epoxidized Natural Rubber [J]. | CHEMISTRYSELECT , 2025 , 10 (24) . |
| MLA | Chen, Bingshen et al. "Chemical Recovery and Decrosslinking Mechanism of Dodecanedioic Acid-Cured Epoxidized Natural Rubber" . | CHEMISTRYSELECT 10 . 24 (2025) . |
| APA | Chen, Bingshen , Ke, Jinhuang , Lin, Tengfei , Wen, Na , Gao, Min , Zhao, Chunlin et al. Chemical Recovery and Decrosslinking Mechanism of Dodecanedioic Acid-Cured Epoxidized Natural Rubber . | CHEMISTRYSELECT , 2025 , 10 (24) . |
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Postoperative abdominal adhesions are the most common complication following abdominopelvic surgery, posing a significant burden on patients, clinicians, and society. However, current physical barriers often involve a tradeoff between preventing these adhesions and inhibiting inflammation. Herein, a one-stone-two-birds strategy is presented to address this challenge through an injectable intertwined hydrogel containing sulfobetaine, modified aminocaproic acid (A6ACA), and ZnO nanoparticles (PSA-ZnO hydrogel). This intertwined network is stabilized by multiple intermolecular coordination bonds, including hydrogen bonds and electrostatic interactions—enabling facile injection and resistance to abdominal creep stress. Experimental results demonstrate that PSA-ZnO hydrogel fully reduce the severity of peritoneal adhesions in treated rats at both 7- and 14-days post-surgery, outperforming commercially available hyaluronic acid (HA) gel due to its superior antifouling, antibacterial (> 95% clearance of E. coli and S. aureus,), hemostatic (55 s), and wound healing properties (IL-6 and TNF-α decreased and VEGF increased). Unlike conventional barriers, PSA-ZnO prevents foreign body formation by inhibiting blood clot organization and pathologic fibrin accumulation at wound sites. This integrated approach offers a clinically translatable solution for complete prevention of postoperative adhesions and inflammation, with the potential to improve patient outcomes and reduce healthcare burdens. © 2025 The Author(s). Advanced Science published by Wiley-VCH GmbH.
Keyword ：
antifouling antifouling hydrogel hydrogel multifunctional multifunctional prevent abdominal adhesions prevent abdominal adhesions zwitterionic zwitterionic
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| GB/T 7714 | Wen, N. , Jiang, Y. , Song, Y. et al. An Injectable Zwitterionic Hydrogels with Multiple Intermolecular Interactions for Effective Prevention of Abdominal Adhesions [J]. | Advanced Science , 2025 . |
| MLA | Wen, N. et al. "An Injectable Zwitterionic Hydrogels with Multiple Intermolecular Interactions for Effective Prevention of Abdominal Adhesions" . | Advanced Science (2025) . |
| APA | Wen, N. , Jiang, Y. , Song, Y. , Yang, J. , Long, J. , Wang, Y. et al. An Injectable Zwitterionic Hydrogels with Multiple Intermolecular Interactions for Effective Prevention of Abdominal Adhesions . | Advanced Science , 2025 . |
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The persistent threats posed by toxic chemical warfare agents (CWAs) such as mustard gas (bis(2-chloroethyl) sulfide, HD) and bacterial contaminants demand the development of innovative, sustainable mitigation strategies. Photocatalytic processes that generate reactive oxygen species (ROS) offer a promising dual-functional approach for both chemical detoxification and antibacterial defense. In this study, two structurally analogous covalent organic frameworks (COFs), BPY-COF and BD-COF, are synthesized using benzotrithiophene as the donor unit paired with bipyridine and biphenyl, respectively. These COFs exhibit high crystallinity, broad-spectrum light absorption, and efficient charge carrier transport, with BPY-COF demonstrating superior performance due to the incorporation of heteroatoms. BPY-COF achieved ultrafast detoxification of the mustard gas simulant 2-chloroethyl ethyl sulfide (CEES) with a half-life of 35 min and 100% selectivity for 2-chloroethyl sulfoxide (CEESO) under white LED light, outperforming BD-COF. Additionally, electrospun composite fibers containing 40 wt.% BPY-COF maintained comparable CEES degradation rates and exhibited over 99% antibacterial efficiency against Escherichia coli and Bacillus subtilis within 60 min. These findings highlight the potential of BPY-COF as a multifunctional photocatalyst for integrated applications in chemical detoxification and antibacterial defense, addressing critical challenges in public health and safety.
Keyword ：
antibacterial antibacterial charge transfer charge transfer covalent organic frameworks covalent organic frameworks photocatalytic degradation photocatalytic degradation
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| GB/T 7714 | Zhu, Yongchao , Qin, Liyang , Yang, Mingyuan et al. Dual-Functional Benzotrithiophene-Based Covalent Organic Frameworks for Photocatalytic Detoxification of Mustard Gas Simulants and Antibacterial Defense [J]. | SMALL , 2025 , 21 (12) . |
| MLA | Zhu, Yongchao et al. "Dual-Functional Benzotrithiophene-Based Covalent Organic Frameworks for Photocatalytic Detoxification of Mustard Gas Simulants and Antibacterial Defense" . | SMALL 21 . 12 (2025) . |
| APA | Zhu, Yongchao , Qin, Liyang , Yang, Mingyuan , Shi, Zhicheng , Chen, Hongxuan , Wen, Na et al. Dual-Functional Benzotrithiophene-Based Covalent Organic Frameworks for Photocatalytic Detoxification of Mustard Gas Simulants and Antibacterial Defense . | SMALL , 2025 , 21 (12) . |
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Metal-nitrogen co-doped composite (M-N-C) carbon materials exhibit outstanding catalytic performance in oxygen reduction reactions (ORR), making them promising candidates to replace commercial Pt/C catalysts. However, it remains a challenge to achieve a rational design that ensures a uniform dispersion of the metal active centers in the nitrogen-doped carbon materials and an effective construction of the M-N active sites to enhance the ORR performance. This research introduces an innovative in situ pyrolysis technique utilizing the guanine biomolecule in conjunction with ZIF-67. This approach not only circumvents the pitfalls of structural disintegration and cobalt center agglomeration but also creates an abundance of anchoring sites conducive to the atomic dispersion of cobalt. Consequently, this method fosters the synthesis of Co-N and pyridinic-N active sites, which are pivotal for catalytic activity. The G-Co@NC-800 catalyst demonstrates exceptional ORR catalytic prowess, with a half-wave potential of 0.83 V (vs RHE) and a current density of -5.1 mAcm-2, coupled with remarkable stability and methanol tolerance in alkaline media. These attributes surpass those of commercial Pt/C catalysts, underscoring the superiority of this novel catalyst. This pioneering approach promotes the rational design of uniformly dispersed Co nanoparticles and the extensive construction of Co-N sites. Metal-nitrogen co-doped carbon materials are synthesized via a simple and facile in-situ pyrolysis strategy from biomolecules guanine with ZIF-67.The guanine transferred into 2D carbon nanosheets and nanotubes after pyrolysis, which inhibits the structural collapse and Co centers agglomeration of ZIF-67 during pyrolysis.The guanine provides anchoring sites for the Co nanoparticles (Co-Nx).The uniformly dispersed Co nanoparticles, as well as the widely constructed Co-Nx, provide a large number of active centers for catalytic activity of ORR in alkaline conditions.
Keyword ：
electrocatalyst electrocatalyst guanine guanine metal-organic frameworks metal-organic frameworks nitrogen doped carbon materials nitrogen doped carbon materials oxygen reduction reaction oxygen reduction reaction
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| GB/T 7714 | Zhu, Yongchao , Yang, Weibo , Yang, Mingyuan et al. In Situ Fabrication of Nitrogen Co-Doped Carbon Materials from Biomolecule Guanine for Enhanced Oxygen Electrocatalysis [J]. | ECS JOURNAL OF SOLID STATE SCIENCE AND TECHNOLOGY , 2025 , 14 (4) . |
| MLA | Zhu, Yongchao et al. "In Situ Fabrication of Nitrogen Co-Doped Carbon Materials from Biomolecule Guanine for Enhanced Oxygen Electrocatalysis" . | ECS JOURNAL OF SOLID STATE SCIENCE AND TECHNOLOGY 14 . 4 (2025) . |
| APA | Zhu, Yongchao , Yang, Weibo , Yang, Mingyuan , Zhang, Liang , Mao, Aijiao , Lin, Yihui et al. In Situ Fabrication of Nitrogen Co-Doped Carbon Materials from Biomolecule Guanine for Enhanced Oxygen Electrocatalysis . | ECS JOURNAL OF SOLID STATE SCIENCE AND TECHNOLOGY , 2025 , 14 (4) . |
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This work proposes a sigma-pi hyperconjugation strategy to establish interlayer charge transport channels (CTC) in supramolecular organic nanostructures. A series of ullazine-based molecular semiconductors were designed and synthesized successfully by engineering end groups to demonstrate the sigma-pi hyperconjugation that unlocks the quantum confinement of photogenerated charges in pi-conjugated planes. Ullazine grafted with tert-butyl (U-t-Bu) showed a J-cross-stacking model in which the cross-stacked U-t-Bu molecular pair smoothly glides along the elongated dimension, forming a Z-schemed interlayer CTC by sigma-pi hyperconjugations between C-H sigma-bonds of tert-butyl end group and pi-bonds of ullazines in adjacent layers along the stacking dimension. Consequently, upon photoexcitation of ullazine-based supramolecular nanoaggregates in aqueous solution, the formed Frenkel excitons are dissociated to charge-separated excitons by the interlayer charge separation channels, undergoing an ultrafast charge transfer within 0.58 ps and an ultrafast charge separation within 0.67 ps. The Z-schemed charge separation between adjacent layers leads to a significantly enhanced hydrogen yield over U-t-Bu/PVP/Pt, with a hydrogen evolution rate of 369.9 mu molg-1h-1 and an apparent quantum yield of 1.46% at 420 nm. It is 3.8-fold larger than that of ullazine modified with methoxy (U-OMe), without the sigma-pi hyperconjugation.
Keyword ：
exciton dynamics exciton dynamics HER HER hyperconjugation effect hyperconjugation effect photocatalysis photocatalysis supramolecule supramolecule
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| GB/T 7714 | Yang, Qin , Li, Wanqing , Wang, Ying et al. σ-π Hyperconjugation Unlocks Interlayer Charge Separation of Ullazine-Based Supramolecular Nanostructures for Photocatalytic Hydrogen Evolution [J]. | ACS CATALYSIS , 2025 , 15 (4) : 3267-3275 . |
| MLA | Yang, Qin et al. "σ-π Hyperconjugation Unlocks Interlayer Charge Separation of Ullazine-Based Supramolecular Nanostructures for Photocatalytic Hydrogen Evolution" . | ACS CATALYSIS 15 . 4 (2025) : 3267-3275 . |
| APA | Yang, Qin , Li, Wanqing , Wang, Ying , Zhuang, Yan , Wu, Shuhong , Wang, Shuo et al. σ-π Hyperconjugation Unlocks Interlayer Charge Separation of Ullazine-Based Supramolecular Nanostructures for Photocatalytic Hydrogen Evolution . | ACS CATALYSIS , 2025 , 15 (4) , 3267-3275 . |
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Two-way shape memory polymers (2W-SMPs), which can transition between two distinct temporary shapes, have garnered significant attention from researchers. This study successfully developed thermadapt 2W-SMPs using syndiotactic 1,2-polybutadiene (SPB) by leveraging dynamic covalent crosslinking techniques. Initially, m-chloroperbenzoic acid (m-CPBA) was employed for the epoxidation of SPB. Cysteine (Cys) was subsequently introduced to form a dynamic covalent bond of beta-hydroxy ester via the reaction between the epoxy groups on SPB and the carboxyl groups of Cys. The sulfhydryl groups of Cys can undergo oxidative coupling to form disulfide bonds, thereby establishing two distinct types of dynamic covalent bonds within the material and lowering its topological rearrangement temperature. Through the exchange reactions of these dynamic covalent bonds at elevated temperatures, the resulting material exhibits enhanced mechanical properties and can be reshaped in the solid state. This work provides a viable method for preparing recyclable thermally adaptive 2W-SMPs under stress-free conditions, thereby enriching the research landscape in the field of shape memory materials.
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| GB/T 7714 | Chen, Bingshen , Xia, Biao , Liao, Shijie et al. Dynamic covalent networks enable thermadapt two-way shape memory behavior in syndiotactic 1,2-polybutadiene-based recyclable polymers [J]. | JOURNAL OF MATERIALS SCIENCE , 2025 , 60 (28) : 12172-12185 . |
| MLA | Chen, Bingshen et al. "Dynamic covalent networks enable thermadapt two-way shape memory behavior in syndiotactic 1,2-polybutadiene-based recyclable polymers" . | JOURNAL OF MATERIALS SCIENCE 60 . 28 (2025) : 12172-12185 . |
| APA | Chen, Bingshen , Xia, Biao , Liao, Shijie , Zeng, Daiwei , Lin, Tengfei , Wen, Na et al. Dynamic covalent networks enable thermadapt two-way shape memory behavior in syndiotactic 1,2-polybutadiene-based recyclable polymers . | JOURNAL OF MATERIALS SCIENCE , 2025 , 60 (28) , 12172-12185 . |
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As advanced optical storage materials, fluorescent hydrogels still face significant challenges in achieving multi-stimulus responsiveness and broad spectral tunability. This study presents a novel aggregation-induced emission (AIE)-active hydrogel system with dual fluorescence emission characteristics, synthesized via a facile one-pot approach. Through controlled freeze-thaw processing cycles, tetrakis(4-hydroxyphenyl)ethylene (TPE-4OH) and tetrakis(4-aminophenyl)ethylene (TPE-4NH2) were successfully incorporated into the three-dimensional polymer matrix. The developed system demonstrates programmable fluorescence modulation through three distinct stimulus-response mechanisms: solvent composition (DMSO/H2O), pH variation (HCl/NaOH), and ion coordination (Fe3(+)/EDTA). Notably, these stimuli enable precise individual or synergistic control over both fluorescence intensity and chromatic characteristics of the hydrogel system. Furthermore, fluorescence modulation precision was enhanced through proportional control of the dual fluorophores, enabling tunable ion recognition sensitivity and a spectral shift from blue to green emission. The integrated multi-stimulus responsiveness and reversible emission characteristics confer dual functionality to this hydrogel system: serving as a patterned substrate fabrication platform while demonstrating promising applicability in multidimensional encryption technologies, analyte-specific sensing probes, and smart optical devices.Graphical abstractMultistimuli-responsive hydrogel system with color changing capabilities.
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| GB/T 7714 | Zeng, Daiwei , Li, Zhou , Su, Yue et al. Dual AIEgen-synergized multistimuli-responsive hydrogels for programmable optical information storage [J]. | JOURNAL OF MATERIALS SCIENCE , 2025 , 60 (34) : 15098-15112 . |
| MLA | Zeng, Daiwei et al. "Dual AIEgen-synergized multistimuli-responsive hydrogels for programmable optical information storage" . | JOURNAL OF MATERIALS SCIENCE 60 . 34 (2025) : 15098-15112 . |
| APA | Zeng, Daiwei , Li, Zhou , Su, Yue , Liu, Chen-chen , Li, Fang , Chen, Jianxing et al. Dual AIEgen-synergized multistimuli-responsive hydrogels for programmable optical information storage . | JOURNAL OF MATERIALS SCIENCE , 2025 , 60 (34) , 15098-15112 . |
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The bioluminescence mechanisms of deep-sea organisms provide innovative ideas for biomimetic design. To meet the detection needs in low-light deep-sea environments, the development of soft robots with high-brightness luminescence is crucial for long-term in situ observation. Directly incorporating high-performance fluorescent molecules into hydrogel matrices presents challenges: fluorescent molecules tend to dissociate in physically crosslinked systems, and complex aqueous environments may lead to instability in the material structure. These issues limit the fluorescence stability and service life of underwater devices. Inspired by the behaviors of marine organisms, this study proposes a biomimetic soft actuator with high fluorescence intensity. The actuator adopts a bilayer hydrogel structure, where the luminescent layer (PT4B-N), covalently crosslinked with fluorescent molecules, achieves a high photoluminescence quantum yield (PLQY > 60%), and the pH-responsive driving layer (PNPC) enables motion control (strip-shaped hydrogel: maximum bending angle approximate to 360 degrees, cycle time approximate to 20 min). The experimental results demonstrate that the actuator can realize biological-like synergic fluorescence and shape change (SFSC) behavior.
Keyword ：
aggregation-induced emission aggregation-induced emission biomimetic soft actuator biomimetic soft actuator fluorescent hydrogel fluorescent hydrogel
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| GB/T 7714 | Liao, Shijie , Dong, Gaolei , Han, Bing et al. A Biomimetic Soft Actuator Achieves Efficient Fluorescence via Covalent Cross-Linking [J]. | SMALL , 2025 , 21 (36) . |
| MLA | Liao, Shijie et al. "A Biomimetic Soft Actuator Achieves Efficient Fluorescence via Covalent Cross-Linking" . | SMALL 21 . 36 (2025) . |
| APA | Liao, Shijie , Dong, Gaolei , Han, Bing , Wei, Junwen , Zhang, Yangdong , Guo, Yihao et al. A Biomimetic Soft Actuator Achieves Efficient Fluorescence via Covalent Cross-Linking . | SMALL , 2025 , 21 (36) . |
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稀土上转换纳米粒子(UCNPs)因其具有毒性小、化学稳定性好和背景荧光低等优点被用于构建荧光纳米传感器.通过溶剂热法制备核壳UCNPs,采用柠檬酸钠对其进行表面配体交换得到水溶性核壳UCNPs(Cit-CS-UCNPs),以Cit-CS-UCNPs作为荧光传感器的能量供体,二氧化锰(MnO2)纳米片作为荧光传感器的能量受体,采用荧光共振能量转移(FRET)机理,构建了一种用于食品添加剂二氧化氢(H2O2)和叔丁基对苯二酚(TBHQ)检测的荧光纳米传感器(Cit-CS-UCNPs-MnO2).通过扫描电镜(SEM)、荧光光谱和紫外可见吸收光谱(UV-Vis)等分析测试手段对制备的纳米材料的形貌结构和性能进行表征.考察了猝灭剂浓度、孵育温度及孵育时间等实验条件对荧光传感体系检测性能的影响.荧光光谱和UV-Vis实验结果表明,Cit-CS-UCNPs最大发射峰位于654 nm,Cit-CS-UCNPs与MnO2结合后,核壳UCNPs发生荧光猝灭,当存在H2O2时,Cit-CS-UCNPs的荧光恢复,说明在此波段H2O2与MnO2纳米片发生氧化还原反应,MnO2纳米片被还原成Mn2+,逐渐从Cit-CS-UCNPs的表面解离下来;存在TBHQ时,Cit-CS-UCNPs-MnO2与TBHQ体系峰位与TBHQ偏移到253 nm,为TBHQ与MnO2纳米片发生氧化还原反应,使得Cit-CS-UCNPs-MnO2体系中FRET效应减弱,荧光强度回升.SEM结果表明,MnO2纳米片均匀包覆在Cit-CS-UCNPs的周围,在水中仍可保持良好的分散性,表明MnO2纳米片修饰到Cit-CS-UCNPs表面.对猝灭剂高锰酸钾(KMnO4)的浓度进行了优化.结果表明,当KMnO4浓度为10 mol·L-1时,猝灭效率可达90％.对检测条件进行优化,结果表明H2O2的检测孵育时间为25 min时,MnO2和H2O2之间氧化还原反应基本完全,Cit-CS-UCNPs-MnO2荧光恢复值最大;TBHQ的检测孵育时间为30 min.在最佳实验条件下,Cit-CS-UCNPs-MnO2 的荧光强度变化比率与 H2O2 浓度(0～1 000 μmol·L-1)及 TBHQ 浓度(0～0.6 mmol·L-1)分别具有良好的线性关系.保持最佳实验条件,选取食品中存在的代表性金属离子(如K+、Na+、Ca2+和Mg2+)和常见的食品添加剂苯甲酸(BA)、D-葡萄糖(Glu)、山梨酸钾(PS)、蔗糖(Suc)、纳他霉素(Nat)和肌醇(Ino)作为研究对象进行选择性测试,发现与H2O2相比,Cit-CS-UCNPs-MnO2对其他添加物质没有强烈的反应,传感器整体荧光信号波动不大,因此Cit-CS-UCNPs-MnO2对H2O2和TBHQ可进行特异性检测.
Keyword ：
上转换纳米粒子 上转换纳米粒子 核壳结构 核壳结构 荧光纳米传感器 荧光纳米传感器
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| GB/T 7714 | 张璇 , 王雅森 , 温娜 et al. 基于稀土上转换纳米粒子传感器的构建及其在食品添加剂检测中的应用 [J]. | 光谱学与光谱分析 , 2024 , 44 (9) : 2459-2466 . |
| MLA | 张璇 et al. "基于稀土上转换纳米粒子传感器的构建及其在食品添加剂检测中的应用" . | 光谱学与光谱分析 44 . 9 (2024) : 2459-2466 . |
| APA | 张璇 , 王雅森 , 温娜 , 吕海霞 , 李宝铭 . 基于稀土上转换纳米粒子传感器的构建及其在食品添加剂检测中的应用 . | 光谱学与光谱分析 , 2024 , 44 (9) , 2459-2466 . |
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Wound dressings play a critical role in the wound healing process; however, conventional dressings often address singular functions, lacking versatility in meeting diverse wound healing requirements. Herein, dual-network, multifunctional hydrogels (PSA/CS-GA) have been designed and synthesized through a one-pot approach. The in vitro and in vivo experiments demonstrate that the optimized hydrogels have exceptional antifouling properties, potent antibacterial effects and rapid hemostatic capabilities. Notably, in a full-thickness rat wound model, the hydrogel group displays a remarkable wound healing rate exceeding 95% on day 10, surpassing both the control group and the commercial 3M group. Furthermore, the hydrogels exert an anti-inflammatory effect by reducing inflammatory factors interleukin 6 (IL-6) and tumor necrosis factor-alpha (TNF-alpha), enhance the release of the vascular endothelial growth factor (VEGF) to promote blood vessel proliferation, and augment collagen deposition in the wound, thus effectively accelerating wound healing in vivo. These innovative hydrogels present a novel and highly effective approach to wound healing. Dual network multifunctional hydrogels are developed using a one-pot synthesis approach. The in vitro and in vivo experiments demonstrate that these hydrogels have exceptional antifouling properties, potent antibacterial effects and rapid hemostatic capabilities.
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| GB/T 7714 | Jiang, Hongzhi , Huang, Xueping , Yang, Jiachao et al. Dual network composite hydrogels with robust antibacterial and antifouling capabilities for efficient wound healing [J]. | JOURNAL OF MATERIALS CHEMISTRY B , 2024 , 12 (20) : 4909-4921 . |
| MLA | Jiang, Hongzhi et al. "Dual network composite hydrogels with robust antibacterial and antifouling capabilities for efficient wound healing" . | JOURNAL OF MATERIALS CHEMISTRY B 12 . 20 (2024) : 4909-4921 . |
| APA | Jiang, Hongzhi , Huang, Xueping , Yang, Jiachao , Yu, Xunbin , Yang, Weibo , Song, Yunhao et al. Dual network composite hydrogels with robust antibacterial and antifouling capabilities for efficient wound healing . | JOURNAL OF MATERIALS CHEMISTRY B , 2024 , 12 (20) , 4909-4921 . |
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