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学者姓名：李小娟
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Abstract ：
Developing the transition metal catalysts with high reactivity for the sulfate radical (SO4 -center dot) based advanced oxidation processes (SR-AOPs) has been attracting numerous attentions. To improve the peroxymonosulfate (PMS) activation process mediated by Co-based catalysts, a vanadium-cobalt bimetallic catalyst (V@CoO) was fabricated by modification vanadium through a simple solvothermal method. The pollutants degradation experiments showed that the obtained V@CoO exhibited much higher performance on PMS activation (5.55-8.33 times larger of apparent rate constants) than pure CoO, and the V@CoO/PMS system could quickly degrade various organic contaminants within 5 min under the attack of both radicals (SO4 -center dot and O2-center dot) and non-radicals (1O2). The density functional theory (DFT) calculations and electrochemical tests revealed that the enhancing mechanism of V modification involved four aspects: (i) promoting the PMS adsorption on the surface of V@CoO; (ii) enhancing the electron transfer efficiency between V@CoO and PMS; (iii) activating PMS with V3+ and V4+ species; (iv) accelerating the circulation of Co2+ and Co3+, leading to the promotion on the production of reactive oxygen species (ROS). Furthermore, the V@CoO/PMS system also exhibited satisfactory stability in a broad pH range and good efficiency in the presence of co-existing components (HCO3-, NO3-, PO43- , Cl- and HA) in water. This study will provide new insights to designing high-performance, environment-friendly bimetal catalysts and some basis for the remediation of organic contaminants with SR-AOPs.
Keyword ：
Co-based catalyst Co-based catalyst Degradation Degradation Organic pollutants Organic pollutants Peroxymonosulfate activation Peroxymonosulfate activation V modification V modification
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| GB/T 7714 | Jiang, Yanting , Weng, Xin , Hu, Yihui et al. Enhanced peroxymonosulfate (PMS) activation process mediated by vanadium modified CoO catalyst for rapid degradation of organic pollutants: Insights into the role of V [J]. | JOURNAL OF ENVIRONMENTAL CHEMICAL ENGINEERING , 2024 , 12 (2) . |
| MLA | Jiang, Yanting et al. "Enhanced peroxymonosulfate (PMS) activation process mediated by vanadium modified CoO catalyst for rapid degradation of organic pollutants: Insights into the role of V" . | JOURNAL OF ENVIRONMENTAL CHEMICAL ENGINEERING 12 . 2 (2024) . |
| APA | Jiang, Yanting , Weng, Xin , Hu, Yihui , Lv, Yuancai , Yu, Zhendong , Liu, Yifan et al. Enhanced peroxymonosulfate (PMS) activation process mediated by vanadium modified CoO catalyst for rapid degradation of organic pollutants: Insights into the role of V . | JOURNAL OF ENVIRONMENTAL CHEMICAL ENGINEERING , 2024 , 12 (2) . |
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Developing adsorbents with high performance and long service life for effective extracting the trace organochlorine pesticides (OCPs) from real water is attracting numerous attentions. Herein, a self-standing covalent organic framework (COF-TpPa) membrane with fiber morphology was successfully synthesized by using electrospun nanofiber membranes as template and employed as solid-phase microextraction (SPME) coating for ultra-high sensitivity extraction and analysis of trace OCPs in water. The as-synthesized COF-TpPa membrane exhibited a high specific surface area (800.83 m(2) g(-1)), stable nanofibrous structure, and excellent chemical and thermal stability. Based on the COF-TpPa membrane, a new SPME analytical method in conjunction with gas chromatography-mass spectrometry (GC-MS) was established. This proposed method possessed favorable linearity in concentration of 0.05-2000 ng L-1, high sensitivity with enrichment factors ranging from 2175 to 5846, low limits of detection (0.001-0.150 ng L-1), satisfactory precision (RSD < 10 %), and excellent repeatability (>150 cycles), which was better than most of the reported works. Additionally, the density functional theory (DFT) calculations and XPS results demonstrated that the outstanding enrichment performance of the COF-TpPa membrane was owing to synergistic effect of pi-pi stacking effects, high specific surface area and hydrogen bonding. This work will expect to extend the applications of COF membrane to captures trace organic pollutants in complex environmental water, as well as offer a multiscale interpretation for the design of effective adsorbents.
Keyword ：
Covalent organic framework nanofibrous Covalent organic framework nanofibrous Direct immersion solid-phase microextraction Direct immersion solid-phase microextraction Gas chromatography-mass spectrometry Gas chromatography-mass spectrometry membrane membrane Organochlorine pesticides Organochlorine pesticides
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| GB/T 7714 | Lin, Chunxiang , Weng, Yufang , Lin, Yule et al. Porous covalent organic framework nanofibrous membrane for excellent enrichment and ultra-high sensitivity detection of trace organochlorine pesticides in water [J]. | JOURNAL OF CHROMATOGRAPHY A , 2024 , 1721 . |
| MLA | Lin, Chunxiang et al. "Porous covalent organic framework nanofibrous membrane for excellent enrichment and ultra-high sensitivity detection of trace organochlorine pesticides in water" . | JOURNAL OF CHROMATOGRAPHY A 1721 (2024) . |
| APA | Lin, Chunxiang , Weng, Yufang , Lin, Yule , Liu, Yifan , Li, Xiaojuan , Lv, Yuancai et al. Porous covalent organic framework nanofibrous membrane for excellent enrichment and ultra-high sensitivity detection of trace organochlorine pesticides in water . | JOURNAL OF CHROMATOGRAPHY A , 2024 , 1721 . |
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Detecting trace endocrine disruptors in water is crucial for evaluating the water quality. In this work, a innovative modified polyacrylonitrile@cyanuric chloride-triphenylphosphine nanofiber membrane (PAN@CC-TPS) was prepared by in situ growing triazine porous organic polymers on the polyacrylonitrile (PAN) nanofibers, and used in the dispersive solid phase extraction (DSPE) to enrich trace nitrobenzene phenols (NPs) in water. The resluted PAN@CC-TPS nanofiber membrane consisted of numerous PAN nanofibers cover with CC-TPS solid spheres (similar to 2.50 mu m) and owned abundant functional groups, excellent enrichment performance and good stability. In addition, the method based on PAN@CC-TPS displayed outstanding capacity in detecting the trace nitrobenzene phenols, with 0.50-1.00 mu g/L of the quantification, 0.10-0.80 mu g/L of the detection limit, 85.35-113.55 % of the recovery efficiency, and 98.08-103.02 of the enrichment factor, which was comparable to most materials. Meanwhile, when PAN@CC-TPS was adopted in the real water samples (sea water and river water), the high enrichment factors and recovery percentages strongly confirmed the feasibility of PAN@CC-TPS for enriching and detecting the trace NPs. Besides, the related mechanism of extracting NPs on PAN@CC-TPS mainly involved the synergistic effect of hydrogen bonding, pi-pi stacking and hydrophobic effect.
Keyword ：
Adsorption Adsorption Dispersive solid phase extraction Dispersive solid phase extraction Enrichment Enrichment Nanofiber membrane Nanofiber membrane Nitro-phenol Nitro-phenol Triazine Triazine
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| GB/T 7714 | Weng, Xin , Liu, Shuting , Huang, Jian et al. Efficient dispersive solid phase extraction of trace nitrophenol pollutants in water with triazine porous organic polymer modified nanofiber membrane [J]. | JOURNAL OF CHROMATOGRAPHY A , 2024 , 1717 . |
| MLA | Weng, Xin et al. "Efficient dispersive solid phase extraction of trace nitrophenol pollutants in water with triazine porous organic polymer modified nanofiber membrane" . | JOURNAL OF CHROMATOGRAPHY A 1717 (2024) . |
| APA | Weng, Xin , Liu, Shuting , Huang, Jian , Lv, Yuancai , Liu, Yifan , Li, Xiaojuan et al. Efficient dispersive solid phase extraction of trace nitrophenol pollutants in water with triazine porous organic polymer modified nanofiber membrane . | JOURNAL OF CHROMATOGRAPHY A , 2024 , 1717 . |
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A boron and iron co-doped biochar (B-Fe/biochar) from Masson pine bark was fabricated and used to activate peroxydisulfate (PDS) for the degradation of guaiacol (GL). The roles of the dopants and the contribution of the radical and non-radical oxidations were investigated. The results showed that the doping of boron and iron significantly improved the catalytic activity of the biochar catalyst with a GL removal efficiency of 98.30% within 30 min. The degradation of the GL mainly occurred through the generation of hydroxyl radicals (center dot OHs) and electron transfer on the biochar surface, and a non-radical degradation pathway dominated by direct electron transfer was proposed. Recycling the B-Fe/biochar showed low metal leaching from the catalyst and satisfactory long-term stability and reusability, providing potential insights into the use of metal and non-metal co-doped biochar catalysts for PDS activation.
Keyword ：
B/Fe co-doping B/Fe co-doping biochar biochar Masson pine bark Masson pine bark peroxydisulfate activation peroxydisulfate activation
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| GB/T 7714 | Huang, Jian , Zhu, Yu , Bian, Huiyang et al. Insights into Enhanced Peroxydisulfate Activation with B and Fe Co-Doped Biochar from Bark for the Rapid Degradation of Guaiacol [J]. | MOLECULES , 2023 , 28 (22) . |
| MLA | Huang, Jian et al. "Insights into Enhanced Peroxydisulfate Activation with B and Fe Co-Doped Biochar from Bark for the Rapid Degradation of Guaiacol" . | MOLECULES 28 . 22 (2023) . |
| APA | Huang, Jian , Zhu, Yu , Bian, Huiyang , Song, Liang , Liu, Yifan , Lv, Yuancai et al. Insights into Enhanced Peroxydisulfate Activation with B and Fe Co-Doped Biochar from Bark for the Rapid Degradation of Guaiacol . | MOLECULES , 2023 , 28 (22) . |
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As the cheap and efficient catalysts, the iron-based catalysts have been considered as one of the most promising catalysts for peroxydisulfate (PDS) activation and the development of high-performance iron-based catalysts are attracting growing attentions. In this work, a magnetic Fe-based catalysts (Fe/NC-1000) was obtained by using Fe modified ZIF-8 as the precursor and used to activate the PDS for the degradation of perfluorooctane sulphonate (PFOS). Morphology and structure analysis showed that the resulted Fe/NC-1000 catalyst was displayed porous spheres (40-60 nm) and mainly composed of Fe0, FeNx and carbon. When Fe/NC-1000 was employed to activate the PDS (0.1 g/L of catalyst dosage, 0.5 g/L of PDS dosage and at initial pH of 4.6), the Fe/NC-1000/PDS system exhibited excellent efficiency (97.9 & PLUSMN; 0.1) % for PFOS (10 mg/L) degradation within 30 min. The quenching tests and EPR results revealed that the Fe/NC-1000/PDS system degraded PFOS primarily through singlet oxygen (1O2) evolution and electron-transfer process. Besides, based on the degradation byproducts determined by LC-MS-MS, the PFOS first occurred de-sulfonation to form PFOA, and then the resulted PFOA underwent stepwise defluorination in the Fe/NC-1000/PDS system. Density Functional Theory (DFT) calculations and electrochemistry tests strongly confirmed that Fe/NC-1000 exhibited high electron transfer efficiency, resulting in promoted performance on activating PDS. Importantly, the results of Ecological Structure-Activity Relationship (ECOSAR) analysis showed that the intermediates were lowly toxic during the PFOS degradation, manifesting a green process for PFOS removal. This study would provide more understandings for the persulfate activation process mediated by Fe-based catalysts for Perfluorinated alkyl substances (PFAS) elimination.
Keyword ：
Degradation Degradation Fe-based catalyst Fe-based catalyst MOFs MOFs Perfluorooctane sulphonate Perfluorooctane sulphonate Peroxydisulfate activation Peroxydisulfate activation
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| GB/T 7714 | Jiang, Yanting , Hu, Yihui , Yu, Zhendong et al. Rapid PFOS mineralization with peroxydisulfate activation process mediated by N modified Fe-based catalyst [J]. | ECOTOXICOLOGY AND ENVIRONMENTAL SAFETY , 2023 , 263 . |
| MLA | Jiang, Yanting et al. "Rapid PFOS mineralization with peroxydisulfate activation process mediated by N modified Fe-based catalyst" . | ECOTOXICOLOGY AND ENVIRONMENTAL SAFETY 263 (2023) . |
| APA | Jiang, Yanting , Hu, Yihui , Yu, Zhendong , Lv, Yuancai , Liu, Yifan , Li, Xiaojuan et al. Rapid PFOS mineralization with peroxydisulfate activation process mediated by N modified Fe-based catalyst . | ECOTOXICOLOGY AND ENVIRONMENTAL SAFETY , 2023 , 263 . |
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In this study, the boron-doped iron-carbon composite (Fe@B/C-2) was prepared via a simple solvothermal and secondary calcination process by using iron metal-organic frameworks (Fe-MOFs) as precursor. The obtained Fe@B/C-2 possessed abundant active sites and low iron ion leaching, and exhibited excellent performance on peroxydisulfate (PDS) activation for efficient PFOS (10 mg/L) degradation (94 %) in 60 min, with 0.2 g/L of catalyst dosage, 1.0 g/L of PDS dosage and at 5.0 of initial pH. The radical scavenging and electron paramagnetic resonance (EPR) tests demonstrated that SO4 & sdot;- and & sdot;OH were the primary active species during PFOS elimination. Under the attack of these species, PFOS was first transformed into PFOA, followed by a sequential defluorination process, and lastly mineralized into CO2 and F. Notably, DFT results revealed that Fe species,-BC3/-BC2O structures on the carbon matrix performed crucial roles in PDS activation. The extraordinary catalytic activity of Fe@B/C-2 was attributable to the synergistic effects of Fe nanoparticles and the B-doped on carbon matrix. The doped B not only could activate the inert carbon skeleton and provided more catalytic centers, but also could accelerate the electron transfer efficiency, leading to a boost in PDS decomposition.
Keyword ：
Degradation Degradation Fe -based catalyst Fe -based catalyst Perfluorooctane sulfonic acid Perfluorooctane sulfonic acid Peroxydisulfate activation Peroxydisulfate activation
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| GB/T 7714 | Jiang, Yanting , Yu, Zhendong , Lv, Yuancai et al. Insights to PFOS elimination with peroxydisulfate activation mediated by boron modified Fe/C catalysts: Enhancing mechanism of boron and PFOS degradation pathway [J]. | JOURNAL OF COLLOID AND INTERFACE SCIENCE , 2023 , 652 : 1743-1755 . |
| MLA | Jiang, Yanting et al. "Insights to PFOS elimination with peroxydisulfate activation mediated by boron modified Fe/C catalysts: Enhancing mechanism of boron and PFOS degradation pathway" . | JOURNAL OF COLLOID AND INTERFACE SCIENCE 652 (2023) : 1743-1755 . |
| APA | Jiang, Yanting , Yu, Zhendong , Lv, Yuancai , Li, Xiaojuan , Lin, Chunxiang , Ye, Xiaoxia et al. Insights to PFOS elimination with peroxydisulfate activation mediated by boron modified Fe/C catalysts: Enhancing mechanism of boron and PFOS degradation pathway . | JOURNAL OF COLLOID AND INTERFACE SCIENCE , 2023 , 652 , 1743-1755 . |
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Heteroatomic co-doped carbon materials have broad application prospect in the field of persulfate-based advanced oxidation processes. In this paper, nitrogen and chlorine co-doped ZIF-8 derived porous carbon materials (NClC) were synthesized by a two-step pyrolysis method, as follows: 1.5 g ZIF-8 was transferred to a quartz boat, calcined for 6 h at 800. with a heating rate of 5 degrees C/min in a N-2 atmosphere, and cool naturally to room temperature; the black carbon material obtained was further treated with 0.5 mol/L HCl for 24 h to remove the residual Zn and then dried in a 60 degrees C oven to acquire N-doped porous carbon (NC); subsequently, 1.2 g NH4Cl was uniformly dissolved in 20 mL ultrapure water, and 0.15 g of the synthesized NC was added; after stirring and reaction for 5 h, the mixture was placed in a 60. oven to dry overnight; the dried sample was ground to a uniform powder and then calcined for 2 h at 700, 800, 900 or 1000 degrees C in a N-2 atmosphere to obtain NClCX, in which the "X" represents the secondary calcination temperature (degrees C). Additionally, NC900 was obtained by calcination of NC at 900. in the same way without any modification. The composition and structure of all carbon materials were characterized by field emission scanning electron microscope (FESEM), transmission electron microscope (TEM), X-ray diffraction (XRD), Raman, BET and X-ray photoelectron spectroscopy (XPS). Phenol was employed as a targeted contaminant to explore the performance of NClCX on PMS activation, and the results showed NClC900 exhibited excellent catalytic performance with 97.7% of phenol and 72.4% of total organic carbon (TOC) removal in 30 min. NClC900/PMS system presented excellent acid-base tolerance and anti-interference ability, which can effectively remove phenol over a broad pH range (pH=3 similar to 9) or under the interference of various anions (NO3-, Cl-, H2PO4-, HCO3-) and humic acid (HA). Moreover, the NClC900/PMS system performed outstanding feasibility in the removal of dyes, antibiotics, phenols, pesticide and purification of actual contaminated water samples. Cyclic experiments showed that NClC900 had good stability and could remove 72.1% of phenol after repeated use for 4 times. Quenching experiments, electron paramagnetic resonance and electrochemical analysis indicated that O-1(2) and surface-bound SO4 center dot- were the main active species for phenol degradation, and the graphite N, C-Cl of NClC900 were the key active sites for generating of O-1(2) and surface-bound SO4 center dot-.
Keyword ：
co-doped co-doped metal-organic frameworks metal-organic frameworks peroxymonosulfate peroxymonosulfate singlet oxygen singlet oxygen surface-bound radical surface-bound radical
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| GB/T 7714 | Li, Xiaojuan , Ye, Ziyu , Xie, Shuhan et al. Study on Performance and Mechanism of Phenol Degradation through Peroxymonosulfate Activation by Nitrogen/Chlorine Co-doped [J]. | ACTA CHIMICA SINICA , 2022 , 80 (9) : 1238-1249 . |
| MLA | Li, Xiaojuan et al. "Study on Performance and Mechanism of Phenol Degradation through Peroxymonosulfate Activation by Nitrogen/Chlorine Co-doped" . | ACTA CHIMICA SINICA 80 . 9 (2022) : 1238-1249 . |
| APA | Li, Xiaojuan , Ye, Ziyu , Xie, Shuhan , Wang, Yongjing , Wang, Yonghao , Lv, Yuancai et al. Study on Performance and Mechanism of Phenol Degradation through Peroxymonosulfate Activation by Nitrogen/Chlorine Co-doped . | ACTA CHIMICA SINICA , 2022 , 80 (9) , 1238-1249 . |
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A series of boron and nitrogen co-doped hierarchical porous carbon materials (BNC) were prepared via a facile one-step calcination process, and the catalytic performance of BNC on PMS activation for phenol removal was investigated. BNC-1 exhibited the optimal catalytic performance with a phenol degradation efficiency of 99.6% within 30 min. B, N co-doping strategy improved the specific surface areas (SSA) and total pore volumes (TPV) of carbon catalysts, providing them with abundant active sites, among which graphitic N and BC(3 )were identified as critical catalytic sites for PMS activation. Quenching tests, electron paramagnetic resonance (EPR) and electrochemical experiments demonstrated that singlet oxygen (O-1(2)) was the dominant active species while surface -bound sulfate radical (SO4 center dot-) played an inferior role in the BNC-1/PMS/Phenol system, and the role of hydroxyl radical (center dot OH), superoxide radical (O-2(center dot-)) and surface electron transport cannot be ignored either. The coexistence of radical and non-radical oxidation processes made BNC-1/PMS system have excellent acid-base tolerance (pH=3-11), anti-interference ability and pollutant mineralization performance (68.3% of TOC removal within 30 min). This study presented a high-efficiency and environment-friendly B, N co-doped metal-free catalyst for pollutants degradation via PMS activation and provided an in-depth research for the mechanism of PMS activation by BNC.
Keyword ：
Boron and nitrogen co -doped Boron and nitrogen co -doped Metal -organic frameworks Metal -organic frameworks Peroxymonosulfate Peroxymonosulfate Phenol Phenol Singlet oxygen Singlet oxygen
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| GB/T 7714 | Li, Xiaojuan , Ye, Ziyu , Xie, Shuhan et al. Insight into the performance and mechanism of peroxymonosulfate activation by B, N co-doped hierarchical porous carbon for phenol degradation [J]. | JOURNAL OF ENVIRONMENTAL CHEMICAL ENGINEERING , 2022 , 10 (5) . |
| MLA | Li, Xiaojuan et al. "Insight into the performance and mechanism of peroxymonosulfate activation by B, N co-doped hierarchical porous carbon for phenol degradation" . | JOURNAL OF ENVIRONMENTAL CHEMICAL ENGINEERING 10 . 5 (2022) . |
| APA | Li, Xiaojuan , Ye, Ziyu , Xie, Shuhan , Li, Hongyan , Lv, Yuancai , Wang, Yongjing et al. Insight into the performance and mechanism of peroxymonosulfate activation by B, N co-doped hierarchical porous carbon for phenol degradation . | JOURNAL OF ENVIRONMENTAL CHEMICAL ENGINEERING , 2022 , 10 (5) . |
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杂原子共掺杂碳材料在过硫酸盐活化领域具有广阔的应用前景.本工作通过两步煅烧法合成了氮氯共掺杂ZIF-8衍生多孔碳材料(NClC),并以苯酚为目标污染物,考察其活化过一硫酸盐(PMS)的催化性能,结果表明,30 min内,0.04 g/L NClC900活化0.3 g/L PMS可去除水中97.7%的苯酚(50 mg/L),且总有机碳去除率可达72.4%;NClC900/PMS体系具备优异的酸碱耐受性(pH=3～9)和抗干扰能力,无机阴离子和腐植酸对其影响较小,且该体系还可有效去除水中的染料、抗生素、酚类及农药等有机污染物;循环实验结果表明,NClC900在重复使用4次后其苯酚去除率可达72.1...
Keyword ：
共掺杂 共掺杂 单线态氧 单线态氧 表面结合自由基 表面结合自由基 过一硫酸盐 过一硫酸盐 金属有机骨架材料 金属有机骨架材料
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| GB/T 7714 | 李小娟 , 叶梓瑜 , 谢书涵 et al. 氮氯共掺杂多孔碳活化过一硫酸盐降解苯酚的性能及机理研究 [J]. | 化学学报 , 2022 , 80 (09) : 1238-1249 . |
| MLA | 李小娟 et al. "氮氯共掺杂多孔碳活化过一硫酸盐降解苯酚的性能及机理研究" . | 化学学报 80 . 09 (2022) : 1238-1249 . |
| APA | 李小娟 , 叶梓瑜 , 谢书涵 , 王永净 , 王永好 , 吕源财 et al. 氮氯共掺杂多孔碳活化过一硫酸盐降解苯酚的性能及机理研究 . | 化学学报 , 2022 , 80 (09) , 1238-1249 . |
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碳材料因其比表面积高、吸附性能佳,并且能克服加热、紫外光照射、超声等传统活化方式能耗高、金属催化材料产生二次污染的弊端而在活化过硫酸盐降解有机污染物应用中具有潜力。杂原子(N、S、B、P等)掺杂不仅能打破碳材料网络惰性、提高电导率,还能增加反应活性位点,是提升碳材料活化过硫酸盐性能的有效途径。本文介绍了碳材料活化过硫酸盐的机理,主要包括自由基途径、单线态氧途径及表面电子传递,并进一步总结了杂原子掺杂碳材料活化过硫酸盐的机理;然后综述了杂原子碳材料的种类、制备方法及其在有机污染物降解中的应用,最后指出了已有研究存在的不足,并提出杂原子掺杂碳材料稳定性及可重复利用性的提升和降解机制的深入探索是未来...
Keyword ：
杂原子掺杂 杂原子掺杂 活化 活化 碳材料 碳材料 自由基 自由基 过硫酸盐 过硫酸盐 降解 降解
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| GB/T 7714 | 李小娟 , 叶兰妹 , 廖凤珍 et al. 杂原子掺杂碳材料活化过硫酸盐技术的研究进展 [J]. | 化工进展 , 2021 , 40 (01) : 273-281 . |
| MLA | 李小娟 et al. "杂原子掺杂碳材料活化过硫酸盐技术的研究进展" . | 化工进展 40 . 01 (2021) : 273-281 . |
| APA | 李小娟 , 叶兰妹 , 廖凤珍 , 叶梓瑜 , 叶礼志 . 杂原子掺杂碳材料活化过硫酸盐技术的研究进展 . | 化工进展 , 2021 , 40 (01) , 273-281 . |
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