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学者姓名：李宝铭
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Abstract ：
Acid orange 7 doped poly(3,4-ethylenedioxythiophene)/molybdenum disulfide/reduced graphene oxide (MoS2-RGO@AO7-PEDOT) composite is prepared via a facile two-step approach, where the first step is the molybdenum disulfide (MoS2) nanosheets dispersing on reduced graphene oxide (RGO) evenly using a hydrothermal method, and the second step involves the stable coating of acid orange 7 (AO7) doped poly(3,4-ethylenedioxythiophene) (PEDOT) on the MoS2-RGO surface through chemical oxidation method with AO7 acting as a guide and connector. At a mass ratio of 4:1 between 3,4-ethylenedioxythiophene (EDOT) and MoS2-RGO, MoS2-RGO is coated by AO7 doped PEDOT, and the composite shows a discontinuous lamellar structure without agglomeration of PEDOT, which provides a significant interface between the composite and the electrolyte in favor of increasing the contact area. The large contact area is beneficial for active substances to participate in the redox reaction for charge storage and improving the ion transport efficiency of the electrolyte, which would lead to enhanced electrochemical performance. The composite's specific capacitance in 1 mol L-1 sulfuric acid (H2SO4) is 233 F g-1, which surpasses that of PEDOT by 101%, and the composite retains an impressive 70.6% of its initial specific capacitance after 10,000 cycles. In addition, a flexible all-solid-state supercapacitor is created to investigate its practical application, where H2SO4/polyvinyl alcohol is utilized as the ionic electrolyte and spacer. The supercapacitor demonstrates a maximum energy density of 7.2 Wh kg-1 at a power density of 600 W kg-1, and it maintains 3.52 Wh kg-1 even under high-power density of 4800 W kg-1.
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| GB/T 7714 | Wang, Yasen , Jiang, Junhui , Li, Baoming . Acid orange 7 doped poly(3,4-ethylenedioxythiophene)/molybdenum disulfide/reduced graphene oxide composite as an electrode material for flexible all-solid-state supercapacitors [J]. | JOURNAL OF MATERIALS SCIENCE , 2024 , 59 (5) : 2055-2069 . |
| MLA | Wang, Yasen 等. "Acid orange 7 doped poly(3,4-ethylenedioxythiophene)/molybdenum disulfide/reduced graphene oxide composite as an electrode material for flexible all-solid-state supercapacitors" . | JOURNAL OF MATERIALS SCIENCE 59 . 5 (2024) : 2055-2069 . |
| APA | Wang, Yasen , Jiang, Junhui , Li, Baoming . Acid orange 7 doped poly(3,4-ethylenedioxythiophene)/molybdenum disulfide/reduced graphene oxide composite as an electrode material for flexible all-solid-state supercapacitors . | JOURNAL OF MATERIALS SCIENCE , 2024 , 59 (5) , 2055-2069 . |
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本发明公开了一种抗湿滑改性热塑性聚氨酯及其制备方法和应用，属于热塑性聚氨酯抗湿滑改性技术领域。所述抗湿滑改性热塑性聚氨酯是以热塑性聚氨酯为基体，以非硫化溴化丁基橡胶为抗湿滑改性剂，以γ‑氨丙基三乙氧基硅烷为相容剂，以硬脂酸锌为热稳定剂，以棕榈油为增塑软化剂，经熔融共混制备而成。本发明制得的抗湿滑改性热塑性聚氨酯具有较高的干、湿摩擦系数、较大的拉伸强度和断裂伸长率、较低的硬度，主要用于制作运动鞋、安全鞋的鞋底，具有显著的经济价值与社会效益。
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| GB/T 7714 | 李宝铭 , 林海峰 , 陶涛 et al. 一种抗湿滑改性热塑性聚氨酯及其制备方法和应用 : CN202210461947.7[P]. | 2022-04-29 00:00:00 . |
| MLA | 李宝铭 et al. "一种抗湿滑改性热塑性聚氨酯及其制备方法和应用" : CN202210461947.7. | 2022-04-29 00:00:00 . |
| APA | 李宝铭 , 林海峰 , 陶涛 , 熊雷 . 一种抗湿滑改性热塑性聚氨酯及其制备方法和应用 : CN202210461947.7. | 2022-04-29 00:00:00 . |
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本发明公开了一种基于核壳结构上转换纳米粒子检测叔丁基对苯二酚的方法，属于食品添加剂的检测技术领域。所述检测方法是先利用表面配体交换反应制备柠檬酸钠修饰核壳结构上转换纳米粒子，再通过超声作用制备二氧化锰纳米片修饰核壳结构上转换纳米粒子，最后，绘制“荧光强度变化比率‑叔丁基对苯二酚浓度”标准工作曲线，建立线性工作方程。本发明检测方法能够实现对水溶液中食品添加剂叔丁基对苯二酚的检测，且具有线性检测范围宽、检测限低、灵敏度高等优势，在食品和环境领域具有广泛的应用前景。
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| GB/T 7714 | 李宝铭 , 林莹莹 , 邢益锋 et al. 基于核壳结构上转换纳米粒子检测叔丁基对苯二酚的方法 : CN202111395473.2[P]. | 2021-11-23 00:00:00 . |
| MLA | 李宝铭 et al. "基于核壳结构上转换纳米粒子检测叔丁基对苯二酚的方法" : CN202111395473.2. | 2021-11-23 00:00:00 . |
| APA | 李宝铭 , 林莹莹 , 邢益锋 , 吕海霞 . 基于核壳结构上转换纳米粒子检测叔丁基对苯二酚的方法 : CN202111395473.2. | 2021-11-23 00:00:00 . |
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本发明公开了一种高韧性耐热聚乳酸复合材料及其制备方法，属于聚乳酸改性技术领域。所述高韧性耐热聚乳酸复合材料是以聚乳酸为基体，蒙脱土接枝丙交酯为填充剂，聚对苯二甲酸丁二酸丁二酯为增韧剂，以熔融接枝法制备的甲基丙烯酸缩水甘油酯和甲基丙烯酸丁酯共接枝聚乳酸为相容剂，癸二酸二苯基二酰肼为成核剂，经熔融共混制备而成。本发明制得的聚乳酸复合材料具有较低的原料成本、较高的韧性和热变形温度以及可完全生物降解性，适用于医疗、服饰、汽车、食品包装等领域，具有显著的经济价值与社会效益。
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| GB/T 7714 | 李宝铭 , 陶涛 , 林海峰 et al. 一种高韧性耐热聚乳酸复合材料及其制备方法 : CN202211428488.9[P]. | 2022-11-15 00:00:00 . |
| MLA | 李宝铭 et al. "一种高韧性耐热聚乳酸复合材料及其制备方法" : CN202211428488.9. | 2022-11-15 00:00:00 . |
| APA | 李宝铭 , 陶涛 , 林海峰 , 熊雷 . 一种高韧性耐热聚乳酸复合材料及其制备方法 : CN202211428488.9. | 2022-11-15 00:00:00 . |
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本发明公开了一种非反应性增容PLA/PBAT复合材料及其制备方法，属于高分子复合材料的制备技术领域。所述复合材料是以聚乳酸为原料，以聚己二酸对苯二甲酸丁二酯为增韧剂，以固相接枝法制得的聚乳酸接枝新癸酸缩水甘油酯为增容剂，经熔融共混制备而成。本发明制得的复合材料具有较高的拉伸强度、较优异的韧性、较低的熔体黏度和可完全生物降解性，主要用于医疗、服饰、汽车、食品包装领域，具有显著的经济价值与社会效益。
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| GB/T 7714 | 李宝铭 , 吴康迪 , 王静 et al. 一种非反应性增容PLA/PBAT复合材料及其制备方法 : CN202211212070.4[P]. | 2022-09-30 00:00:00 . |
| MLA | 李宝铭 et al. "一种非反应性增容PLA/PBAT复合材料及其制备方法" : CN202211212070.4. | 2022-09-30 00:00:00 . |
| APA | 李宝铭 , 吴康迪 , 王静 , 张璇 . 一种非反应性增容PLA/PBAT复合材料及其制备方法 : CN202211212070.4. | 2022-09-30 00:00:00 . |
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Congo red doped poly (3,4-ethylene dioxythiophene)/graphene oxide (GO/CR-PEDOT) composite was prepared by simple chemical oxidation method, where Congo red doped poly (3,4-ethylene dioxythiophene) (CR-PEDOT) evenly and stably coated on the surface of graphene oxide (GO) under the guidance and connection of congo red (CR), respectively. Therefore, GO with a large specific surface area could bring into full play its function as a supporting skeleton to decrease the degree of volume expansion and shrinkage of GO/CR-PEDOT composite in charge/discharge process and improve its specific capacitance and cycle stability. The results showed that the maximum specific capacitance of GO/CR-PEDOT composite was up to 227 F/g when the feeding mass ratio of GO to 3,4-ethylene dioxythiophene was 1:1, which was 110% higher than that of poly (3,4-ethylene dioxythiophene) (PEDOT), and the capacitance retention was 92.3 % after 10,000 cycles. Furthermore, a model of asymmetric supercapacitor was fabricated by using GO/CR-PEDOT composite as positive material, activated carbon as negative material and 1 mol/L Na2SO4 as electrolyte, which exhibited that the energy density was as high as 14.4 Wh/kg when the power density was 996 W/kg and still achieved 9.11 Wh/kg at a high power density of 7999 W/kg. (C) 2021 Elsevier Ltd. All rights reserved.
Keyword ：
Asymmetric supercapacitor Asymmetric supercapacitor Congo red Congo red Graphene oxide Graphene oxide Poly (3,4-ethylene dioxythiophene) Poly (3,4-ethylene dioxythiophene)
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| GB/T 7714 | Du, Yuanyuan , Cao, Dingfa , Li, Baoming et al. Stable conge red doped poly (3,4-ethylene dioxythiophene)/graphene oxide composite as electrode material for high-performance asymmetric supercapacitors [J]. | ELECTROCHIMICA ACTA , 2021 , 395 . |
| MLA | Du, Yuanyuan et al. "Stable conge red doped poly (3,4-ethylene dioxythiophene)/graphene oxide composite as electrode material for high-performance asymmetric supercapacitors" . | ELECTROCHIMICA ACTA 395 (2021) . |
| APA | Du, Yuanyuan , Cao, Dingfa , Li, Baoming , Lu, Haixia , Shen, Yu . Stable conge red doped poly (3,4-ethylene dioxythiophene)/graphene oxide composite as electrode material for high-performance asymmetric supercapacitors . | ELECTROCHIMICA ACTA , 2021 , 395 . |
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Reduced graphene oxide nanofiber (rGONF) modified by anthraquinone-1,5-disulfonate (AQDS) (AQDS-rGONF) was prepared by one-step hydrothermal reaction, and nanocilia-like polyaniline (PANI) grew uniformly on the surface of rGONF under the guidance of AQDS as a starting point of polymerization to fabricate successfully PANI/AQDS-rGONF composite. The results showed that PANI/AQDS-rGONF composite had a larger specific capacitance of 511 F/g than PANI/rGONF composite of 360 F/g or PANI of 312 F/g at a current density of 8 mA/cm(2), and a greater electrochemical stability with the specific capacitance retention of 82.4% than PANI/rGONF of 63.2% or PANI of 52.2% after 2000 cycles, which were closely related to the synergistic effects of special nanocilia-like structure, large specific surface area, rGONF as a supporting skeleton and AQDS as a "bridge". In addition, an asymmetric supercapacitor based on PANI/AQDS-rGONF composite as cathode was assembled, which exhibited a high energy density of 17.9 Wh/kg at a power density of 907 W/kg.
Keyword ：
AQDS-guided growth AQDS-guided growth Asymmetric supercapacitor Asymmetric supercapacitor Cathode material Cathode material Graphene nanofiber Graphene nanofiber Nanocilia-like polyaniline Nanocilia-like polyaniline
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| GB/T 7714 | Du, Yuanyuan , Wang, Xiaobing , Li, Baoming et al. AQDS-guided growth of nanocilia-like polyaniline on graphene nanofiber as cathode material for high-performance asymmetric supercapacitors [J]. | SYNTHETIC METALS , 2021 , 272 . |
| MLA | Du, Yuanyuan et al. "AQDS-guided growth of nanocilia-like polyaniline on graphene nanofiber as cathode material for high-performance asymmetric supercapacitors" . | SYNTHETIC METALS 272 (2021) . |
| APA | Du, Yuanyuan , Wang, Xiaobing , Li, Baoming , Lu, Haixia , Shen, Yu . AQDS-guided growth of nanocilia-like polyaniline on graphene nanofiber as cathode material for high-performance asymmetric supercapacitors . | SYNTHETIC METALS , 2021 , 272 . |
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本发明公开了一种聚苯胺/二硫化镍/石墨烯纳米纤维复合材料及其制备方法，属于超级电容器电极材料制备技术领域。所述复合材料是以苯胺为单体，以水热法制备的石墨烯纳米纤维负载二硫化镍为支撑骨架，以过硫酸铵为氧化剂，在超声作用下，经化学氧化反应制备而成。本发明制备的复合材料具有高的比电容和优异的电化学循环稳定性，主要用于制作超级电容器的电极，具有显著的经济价值和社会效益。
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| GB/T 7714 | 李宝铭 , 付新峰 , 吴章浩 . 一种聚苯胺/二硫化镍/石墨烯纳米纤维复合材料及其制备方法 : CN202011088409.5[P]. | 2020-10-13 . |
| MLA | 李宝铭 et al. "一种聚苯胺/二硫化镍/石墨烯纳米纤维复合材料及其制备方法" : CN202011088409.5. | 2020-10-13 . |
| APA | 李宝铭 , 付新峰 , 吴章浩 . 一种聚苯胺/二硫化镍/石墨烯纳米纤维复合材料及其制备方法 : CN202011088409.5. | 2020-10-13 . |
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本发明公开了一种聚3, 4‑乙撑二氧噻吩/石墨毡柔性电极材料的制备方法，属于超级电容器用电极材料的制备技术领域。所述电极材料是以3, 4‑乙撑二氧噻吩作为单体，以十二烷基硫酸钠作为表面活性剂，以橙黄Ⅱ作为掺杂剂，以过硫酸铵作为氧化剂，利用化学氧化法在石墨毡上聚合而成。本发明制得的电极材料具有较高的比电容和较优异的循环稳定性，主要用于制作超级电容器的柔性电极，具有显著的经济价值与社会效益。
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| GB/T 7714 | 李宝铭 , 林莹莹 , 江俊辉 . 一种聚3, 4-乙撑二氧噻吩/石墨毡柔性电极材料的制备方法 : CN202011088630.0[P]. | 2020-10-13 . |
| MLA | 李宝铭 et al. "一种聚3, 4-乙撑二氧噻吩/石墨毡柔性电极材料的制备方法" : CN202011088630.0. | 2020-10-13 . |
| APA | 李宝铭 , 林莹莹 , 江俊辉 . 一种聚3, 4-乙撑二氧噻吩/石墨毡柔性电极材料的制备方法 : CN202011088630.0. | 2020-10-13 . |
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Functionalized graphene oxide (GO) nanocomposites including GO-Fe and GO-Fe-P were prepared and used as a curing additive for a one-component room temperature-curable epoxy adhesive (OCRTCEA). The results showed that the functionalized GO nanocomposites were conducive to accelerating the curing reaction of OCRTCEA with a moisture-activated ketimine as a latent curing agent, and when OCRTCEA containing 1 wt% GO-Fe-P was exposed to air at room temperature for 24 h, its lap shear strength reached 11.2 MPa, which was 144% higher than that of pure OCRTCEA under the same test conditions. Furthermore, the storage stability of OCRTCEA containing 1 wt% GO-Fe-P was similar with that of pure OCRTCEA over 60 days of storage. The enhanced curing reaction activity of OCRTCEA might be due to the role of curing accelerator of GO nanocomposites, the enhanced polarity of OCRTCEA because of the addition of GO nanocomposites, and the special morphology of GO nanocomposites.
Keyword ：
Durability Durability Epoxides Epoxides Mechanical properties of adhesives Mechanical properties of adhesives Nanofillers Nanofillers
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| GB/T 7714 | Li, Baoming , Wang, Xiaoli , Bai, Mengdi et al. Improvement of curing reaction activity of one-component room temperature-curable epoxy adhesive by the addition of functionalized graphene oxide [J]. | INTERNATIONAL JOURNAL OF ADHESION AND ADHESIVES , 2020 , 98 . |
| MLA | Li, Baoming et al. "Improvement of curing reaction activity of one-component room temperature-curable epoxy adhesive by the addition of functionalized graphene oxide" . | INTERNATIONAL JOURNAL OF ADHESION AND ADHESIVES 98 (2020) . |
| APA | Li, Baoming , Wang, Xiaoli , Bai, Mengdi , Shen, Yu . Improvement of curing reaction activity of one-component room temperature-curable epoxy adhesive by the addition of functionalized graphene oxide . | INTERNATIONAL JOURNAL OF ADHESION AND ADHESIVES , 2020 , 98 . |
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