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学者姓名：李浩宏
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Purpose: To investigate the inhibition of Streptococcus mutans (S.mutans) and its biofilm by AgBr-nanoparticles (NP) @CTMAB (cetyltrimethyl-ammonium bromide) and evaluate the changes in Polymethyl methacrylate (PMMA)'s surface roughness (Ra), microhardness, and flexural strength during prolonged immersion in AgBr-NP@CTMAB for application in the denture cleaning industry. Patients and Methods: The antibacterial activity of AgBr-NP@CTMAB against S.mutans was measured colony formation assay, OD600 and laser confocal microscopy. Changes in the specimens' values for surface roughness, microhardness, and flexural strength (MPa) were measured after immersion solutions for 180 or 360 days. Results: The AgBr-NP@CTMAB solution exhibited a robust antibacterial effect on planktonic S. mutans, with a minimum bactericidal concentration of 5 mu g/mL. The 10 mu g/mL AgBr-NP@CTMAB solution efficiently inhibited S. mutans biofilm formation. (2) No significant difference in surface roughness after immersion in AgBr-NP@CTMAB (10 mu g/mL and 20 mu g/mL) comparing with distilled water (P > 0.05) and Polident had significantly higher than distilled water (P < 0.05). There was a significant decrease in the surface hardness of the PMMA specimens that were immersed in the Polident compared with those in distilled water (P < 0.05). While, no significant differences in surface hardness after immersion in the AgBr-NP@CTMAB (P > 0.05). The result of flexural strength suggested that there was no statistically significant difference (P < 0.05) between AgBr-NP@CTMAB as well as Polident and water. Conclusion: AgBrNP@CTMAB can efficiently inhibit the growth of plankton S.mutans and biofilm formation, without affecting the flexural strength, microhardness, or surface roughness of PMMA. Therefore, AgBrNP@CTMAB holds promise as a new denture cleaning agent.
Keyword ：
AgBr-NP@CTMAB AgBr-NP@CTMAB biofilm biofilm denture cleanser denture cleanser polymethyl methacrylate polymethyl methacrylate S.mutans S.mutans
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| GB/T 7714 | Huang, Jing-Jing , Jia, Lin , Zhang, Qiao-Jun et al. Anti-Microbial Effect of AgBr-NP@CTMAB on Streptococcus Mutans and Assessment of Surface Roughness Hardness and Flexural Strength of PMMA [J]. | INTERNATIONAL JOURNAL OF NANOMEDICINE , 2024 , 19 : 1273-1285 . |
| MLA | Huang, Jing-Jing et al. "Anti-Microbial Effect of AgBr-NP@CTMAB on Streptococcus Mutans and Assessment of Surface Roughness Hardness and Flexural Strength of PMMA" . | INTERNATIONAL JOURNAL OF NANOMEDICINE 19 (2024) : 1273-1285 . |
| APA | Huang, Jing-Jing , Jia, Lin , Zhang, Qiao-Jun , Li, Hao-Hong , Zheng, Da-Li , Zheng, Ming . Anti-Microbial Effect of AgBr-NP@CTMAB on Streptococcus Mutans and Assessment of Surface Roughness Hardness and Flexural Strength of PMMA . | INTERNATIONAL JOURNAL OF NANOMEDICINE , 2024 , 19 , 1273-1285 . |
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The development of green memorizers with distinct mechanism is significant. In this work, renewable polyphenol ellagic acid (EA) and environmentally friendly calcium were used to construct a unique 3D interpenetrated bio-metal-organic framework (BioMOF), i.e. {[Ca2(EA)3(4H2O)]2H2O}n. Its high chemical stability stems from the twofold interpenetrated (6,3) bi-layers and versatile strong pi-pi stacking interactions. The memorizer FTO/{[Ca2(EA)3(4H2O)]2H2O}n/Ag exhibits good bipolar resistive switching performance with an ON/OFF ratio of 5.40 x 103 and a tolerant temperature of 300 degrees C. In particular, the local conjugated EA ligand and strong pi-pi stacking interactions in the interpenetrated 3D network are responsible for a carrier trapping/de-trapping process, rendering the excellent binary resistive switching performance. This work demonstrates a new way for the construction of green electrons by adopting renewable natural products as organic linkers. Natural product ellagic acid was used to construct a stable 3D BioMOF with twofold interpenetrated (6,3) bi-layers, which was fabricated as a biomemorizer with an ON/OFF ratio of 5.40 x 103 bearing a high working temperature of 300 degrees C.
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| GB/T 7714 | Liu, Ting-Bo , Deng, Jing-Wen , Li, Yi et al. Stable calcium ellagate metal-organic frameworks as high-performance green memorizers bearing high working temperatures [J]. | INORGANIC CHEMISTRY FRONTIERS , 2024 , 11 (10) : 3056-3062 . |
| MLA | Liu, Ting-Bo et al. "Stable calcium ellagate metal-organic frameworks as high-performance green memorizers bearing high working temperatures" . | INORGANIC CHEMISTRY FRONTIERS 11 . 10 (2024) : 3056-3062 . |
| APA | Liu, Ting-Bo , Deng, Jing-Wen , Li, Yi , Fu, Hai-Ying , Shi, Liang-Wen , Lin, Shi-Ying et al. Stable calcium ellagate metal-organic frameworks as high-performance green memorizers bearing high working temperatures . | INORGANIC CHEMISTRY FRONTIERS , 2024 , 11 (10) , 3056-3062 . |
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Dehydroxylation of biomass-based platform molecules is critical for obtaining building blocks for use in the chemical industry. Acid catalytic dehydration has provided a feasible route. However, simultaneously pursuing high product-selective and ultra-stable catalysts for the dehydroxylation of polyols remains an open challenge. In this study, a strategy for in-situ Bronsted acid sites (BAS) with chemo-adsorption selectivity is proposed. The construction of defect sites B[3] and P[4] species has been proved to be a prerequisite for the dynamic acid site formation at hydrothermal conditions. The BPO4 catalyst with in-situ BAS can achieve the high selectivity of acrolein (similar to 80%) and robust stability of catalyst (over 425 h) using glycerol dehydration as a model reaction. In addition, in-situ BAS is highly selective for secondary hydroxyl groups and has been extended to other substrate applications. This catalytic strategy provides a green, efficient, and economical approach for converting biomassderived polyols to high-value-added chemicals.
Keyword ：
Acrolein Acrolein Biomass Biomass Dehydration Dehydration Glycerol Glycerol In -situ Br onsted acid In -situ Br onsted acid
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| GB/T 7714 | Su, Chenxin , Zhou, Shouquan , Wu, Shaoyun et al. Highly efficient dehydration of polyols: In-situ Brempty setnsted acid from boron phosphate catalyst [J]. | CHEMICAL ENGINEERING JOURNAL , 2024 , 483 . |
| MLA | Su, Chenxin et al. "Highly efficient dehydration of polyols: In-situ Brempty setnsted acid from boron phosphate catalyst" . | CHEMICAL ENGINEERING JOURNAL 483 (2024) . |
| APA | Su, Chenxin , Zhou, Shouquan , Wu, Shaoyun , Gao, Mingbin , Zhang, Weiling , Ma, Zhuang et al. Highly efficient dehydration of polyols: In-situ Brempty setnsted acid from boron phosphate catalyst . | CHEMICAL ENGINEERING JOURNAL , 2024 , 483 . |
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Background: Drug-resistant microbes pose a global health concern, requiring the urgent development of effective antibacterial agents and strategies in clinical practice. Therefore, there is an urgent need to explore novel antibacterial materials to effectively eliminate bacteria. The synthesis of quaternary phosphonium salt in haloargentate systems, wherein the phosphorus atom is represented in a cationic form, is a possible strategy for the development of antibacterial materials.Methods: Using (triphenyl)phosphonium-based quaternary phosphorus salts with different spacer lengths (n=2, 4, 6) as a template, we designed three kinds of quaternary phosphorus salts as effective antibacterial agents against drug-resistant bacteria.Results: The synthesized quaternary phosphorus salt of (1,4-DBTPP)Br2 effectively prevented the formation of the bacterial biofilms, and degraded bacterial membranes and cell walls by promoting the production of reactive oxygen species, which exhibited effective therapeutic effects in a rat model of a superficial wound infected with methicillin-resistant Staphylococcus aureus. Conclusion: The quaternary phosphorus salt (1,4-DBTPP)Br2 demonstrated hemocompatibility and low toxicity, revealing its potential in the treatment of clinical infections.
Keyword ：
antibacterial antibacterial biocompatible biocompatible quaternary phosphorus salts quaternary phosphorus salts reactive oxygen species reactive oxygen species wound infection therapy wound infection therapy
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| GB/T 7714 | Shi, Liang-Wen , Zhuang, Quan-Quan , Wang, Tai-Qin et al. Synthetic Antibacterial Quaternary Phosphorus Salts Promote Methicillin-Resistant Staphylococcus aureus-Infected Wound Healing [J]. | INTERNATIONAL JOURNAL OF NANOMEDICINE , 2023 , 18 : 1145-1158 . |
| MLA | Shi, Liang-Wen et al. "Synthetic Antibacterial Quaternary Phosphorus Salts Promote Methicillin-Resistant Staphylococcus aureus-Infected Wound Healing" . | INTERNATIONAL JOURNAL OF NANOMEDICINE 18 (2023) : 1145-1158 . |
| APA | Shi, Liang-Wen , Zhuang, Quan-Quan , Wang, Tai-Qin , Jiang, Xian-Dong , Liu, Yue , Deng, Jing-Wen et al. Synthetic Antibacterial Quaternary Phosphorus Salts Promote Methicillin-Resistant Staphylococcus aureus-Infected Wound Healing . | INTERNATIONAL JOURNAL OF NANOMEDICINE , 2023 , 18 , 1145-1158 . |
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By introducing Cu(II) ions as additional connecting nodes to construct stable heterometallic uranyl-organic frameworks (UOFs) with thiophene-2,5-dicarboxylic acid (H2TDC) and N-donor auxiliary ligands, three new uranyl complexes, namely, [Cu(phen)(UO2)(TDC)2] (1), [Cu(phen-NO2)(2)(UO2)(TDC)(2)].3H(2)O (2), and [Cu(phen-NH2)(H2O)(2)(UO2)(TDC)(2)].4H(2)O (3) (phen = 1,10-phenanthroline) have been successfully synthesized by hy-drothermal reaction. Complex 1 exhibits a rare three-dimensional (3D) network structure of cds topology con-nected by UO2, Cu(phen), and TDC units. Both complexes 2 and 3 feature similar one-dimensional chain structures based on UO2, TDC, Cu(Phen-NO2)2 and UO2, TDC, Cu(phen-NH2)(H2O)(2) respectively. The N-donor auxiliary ligands play a key role in determining their structural dimensionalities and bandgaps formation. Among the three uranyl complexes, phen with a smaller size than its derivatives, phen-NO2 and phen-NH2, was found to be favorable for constructing 3D UOFs. Moreover, complexes with both phen-NO2 and phen-NH2 showed varying degrees of redshift on optical spectra. The UV-Visible diffuse-reflectance spectra, analyzed with Tauc's fitting in considering Urbach tailing, revealed an indirect bandgap of 2.94 eV, an indirect bandgap of 2.67 eV, and a direct bandgap of 2.45 eV for 1, 2 and 3, respectively. Moreover, thermogravimetric analyses indicate that 3D anhy-drous uranyl complex 1 possessed a robust structure and excellent thermal stability above 250 celcius.
Keyword ：
5-dicarboxylic acid 5-dicarboxylic acid Heterometallic Heterometallic Tauc's analysis Tauc's analysis Thiophene-2 Thiophene-2 Uranyl-organic frameworks Uranyl-organic frameworks
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| GB/T 7714 | Wu, Hong-Yan , Gao, Qiao-Wei , Li, Hao-Hong et al. Constructing stable uranyl-copper(II) bimetallic organic frameworks using rigid thiophenedicarboxylic acid [J]. | POLYHEDRON , 2023 , 243 . |
| MLA | Wu, Hong-Yan et al. "Constructing stable uranyl-copper(II) bimetallic organic frameworks using rigid thiophenedicarboxylic acid" . | POLYHEDRON 243 (2023) . |
| APA | Wu, Hong-Yan , Gao, Qiao-Wei , Li, Hao-Hong , Lai, Wen-Zhong , Hu, Ting , Zhang, Jian-Han . Constructing stable uranyl-copper(II) bimetallic organic frameworks using rigid thiophenedicarboxylic acid . | POLYHEDRON , 2023 , 243 . |
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Two new heterometallic uranyl-organic frameworks (UOFs), [Cd(phen)(2)(H2O)(2)][(UO2)(2)(BDC)(3)]center dot 2H(2)O (1) and [Ni(phen)(3)][(UO2)(2)(BDC)(3)]center dot 2H(2)O (2), were obtained under hydrothermal conditions. Both crystal structures were characterized by single-crystal X-ray diffraction analyses and the results indicate that both complexes feature a similar 2D honeycomb framework that is connected by rigid benzenedicarboxylate (BDC) ligands and uranyl units. BDC works as a linker to bridge neighboring UO22+ units, where UO22+ is tris-chelated. Different guest molecules guided the stacking of 2D layers and lead into their 3D supramolecular crystal structures with different space groups. As a result, 1 crystallized in a polar space group Cc, whereas 2 belongs to a chiral space group P6(1)22. Thermogravimetric measurements were performed to study their thermal stability. UV-visible diffuse reflectance spectroscopy measurements indicate an experimental optical bandgap of 3.87 eV and 3.63 eV, respectively, for 1 and 2. Luminescent studies of both samples show strong green light emissions.
Keyword ：
crystal structure crystal structure Heterometallic Heterometallic luminescence luminescence uranyl complexes uranyl complexes
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| GB/T 7714 | Wu, Hong-Yan , Luo, Ju-Xiang , Li, Hao-Hong et al. Guest molecular guided syntheses of 2-dimensional uranyl complexes with rigid benzenedicarboxylate ligands [J]. | JOURNAL OF COORDINATION CHEMISTRY , 2023 , 76 (2) : 292-306 . |
| MLA | Wu, Hong-Yan et al. "Guest molecular guided syntheses of 2-dimensional uranyl complexes with rigid benzenedicarboxylate ligands" . | JOURNAL OF COORDINATION CHEMISTRY 76 . 2 (2023) : 292-306 . |
| APA | Wu, Hong-Yan , Luo, Ju-Xiang , Li, Hao-Hong , Zhang, Jian-Han . Guest molecular guided syntheses of 2-dimensional uranyl complexes with rigid benzenedicarboxylate ligands . | JOURNAL OF COORDINATION CHEMISTRY , 2023 , 76 (2) , 292-306 . |
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The aspect ratio modulation in the alcoholysis process is highly significant for the production of high-quality sucralose. In this work, antisolvent crystallization (ASC) accompanied by preferred orientation was first adopted in the sucralose separation, based on which simultaneous modulations on aspect ratio, solubility, and stability have been realized. In detail, after the alcoholysis process in methanol, four antisolvents bearing different functional groups were used in ASC, i.e., isopentanol (IPN), isovaleraldehyde (IVD), isovaleric acid (IVA), and isobutyl propionate (IBP). To our interest, when IVA was used as the antisolvent, the highest separation efficiency (49.33%), fastest crystallizing rate (5.64%/h), lowest aspect ratio (1.55), and solubility (9.28 wt %) and good thermal stability (131.65 degrees C) of sucralose were achieved. Single crystal structures of sucralose using different antisolvents have been determined. Sucralose using IVA as the antisolvent exhibits the greatest molecular distortion and strongest intermolecular C-HCl hydrogen bonds; thus, the preferred growth along {002}/{011} directions has occurred and accounted for its lower aspect ratio, worse solubility, and better stability. The strongest methanolIVA interactions due to the presence of a carboxyl group can accelerate the formation of the emulsion, resulting in the fastest crystallizing rate. The antisolvent screening and the discovery about relative mechanisms will provide a theoretical guide for the production of high-quality sucralose.
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| GB/T 7714 | Xu, Qiaoyan , Lv, Zhoulin , Chen, Xiaoping et al. Aspect Ratio Modulation of Sucralose through {002}/{011} Preferred Orientation in Antisolvent Crystallization [J]. | ACS OMEGA , 2023 , 8 (44) : 41145-41155 . |
| MLA | Xu, Qiaoyan et al. "Aspect Ratio Modulation of Sucralose through {002}/{011} Preferred Orientation in Antisolvent Crystallization" . | ACS OMEGA 8 . 44 (2023) : 41145-41155 . |
| APA | Xu, Qiaoyan , Lv, Zhoulin , Chen, Xiaoping , Li, Shaoheng , Huang, Changqi , Chen, Jingjing et al. Aspect Ratio Modulation of Sucralose through {002}/{011} Preferred Orientation in Antisolvent Crystallization . | ACS OMEGA , 2023 , 8 (44) , 41145-41155 . |
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The exploration of novel photo/thermal-responsive nonvolatile memorizers will be beneficial for energysaving memories. Herein, new < 110 > -oriented perovskites using single template melamine, i.e. , [(MLAIH 2 )(Pb X 4 )] n ( X = Br ( alpha- 1 ), Cl ( alpha- 2 ), MLAI = melamine) have been prepared and their structures upon irradiation of visible light have been investigated. They have been fabricated as nonvolatile memory devices with structures of ITO/[(MLAI-H 2 )(Pb X 4 )] n /PMMA/Ag (device- 1 : X = Br, device- 2 : X = Cl), which can exhibit unique visible light-triggered binary nonvolatile memory performances. Interestingly, the silent or working status can be monitored by visible chromisms. Furthermore, the light-triggered binary resistive switching mechanisms of these ITO/[(MLAI-H 2 )(Pb X 4 )] n /PMMA/Ag memory devices have been clarified in terms of EPR, fluorescence, and single-crystal structural analysis. The presence of light-activated traps in < 110 > -oriented [(MLAI-H 2 )(Pb X 4 )] n perovskites are dominated in the appearance of light-triggered resistive switching behaviors, based on which the inverted internal electrical fields can be established. According to the structural analysis, the more distorted Pb X 6 octahedra, higher corrugated < 110 > -oriented perovskite sheets, and more condensed organic-inorganic packing in Br-containing perovskite are beneficial for the stabilization of light-activated traps, which lead to the better resistive switching behavior of device- 1 . This work can pave a new avenue for the establishment of novel energy-saving nonvolatile memorizers used in aerospace or military industries.(c) 2023 Published by Elsevier B.V. on behalf of Chinese Chemical Society and Institute of Materia Medica, Chinese Academy of Medical Sciences.
Keyword ：
110-Oriented lead halide perovskite 110-Oriented lead halide perovskite Light-triggered memory Light-triggered memory Nonvolatile memorizer Nonvolatile memorizer Photochromisms Photochromisms Photo-responsive structural evolution Photo-responsive structural evolution
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| GB/T 7714 | Song, Kaiyue , Zhou, Panke , Zong, Lulu et al. The visible light-triggered nonvolatile memory performances in melamine-decorated 110-oriented lead halide perovskites: A photo-responsive structural evolution insight [J]. | CHINESE CHEMICAL LETTERS , 2023 , 34 (3) . |
| MLA | Song, Kaiyue et al. "The visible light-triggered nonvolatile memory performances in melamine-decorated 110-oriented lead halide perovskites: A photo-responsive structural evolution insight" . | CHINESE CHEMICAL LETTERS 34 . 3 (2023) . |
| APA | Song, Kaiyue , Zhou, Panke , Zong, Lulu , Yang, Zhencong , Li, Haohong , Chen, Zhirong . The visible light-triggered nonvolatile memory performances in melamine-decorated 110-oriented lead halide perovskites: A photo-responsive structural evolution insight . | CHINESE CHEMICAL LETTERS , 2023 , 34 (3) . |
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Polysulfide-based multilevel memorizers are promising as novel memorizers, in which the occurrence of S-n(2-) relaxation is key for their multilevel memory. However, the effects of crystal packing and the side group of organic ligands on S-n(2-) relaxation are still ambiguous. In this work, ionic [Zn(S-6)(2)Zn-2(Bipy)(2)SO4 (1), Zn(S-6)(2)Zn(Pmbipy)(3) (2)] and neutral [ZnS6(Ombipy) (3), ZnS6(Phen)(2) (4)] Zn/polysulfide/organic complexes with different packing modes and structures of organic ligands have been synthesized and were fabricated as memory devices. In both ionic and neutral Zn complexes, the S-6(2-) relaxation will be blocked by steric hindrances due to the packing of counter-cations and hydrogen-bond restrictions. Consequently, only the binary memory performances can be seen in FTO/1/Ag, FTO/2/Ag, and FTO/4/Ag, which originate from the more condensed packing of conjugated ligands upon electrical stimulus. Interestingly, FTO/3/Ag illustrates the unique thermally triggered reversible binary-ternary switchable memory performance. In detail, after introducing a methyl group on the 6 '-position of bipyridine in ZnS6(Ombipy) (3), the ring-to-chain relaxation of S-6(2-) anions at room temperature will be inhibited, but it can happen at a higher temperature of 120 degrees C, which has been verified by elongated S-S lengths and the strengthened C-HS hydrogen bond upon heating. The rules drawn in this work will provide a useful guide for the design of stimulus-responsive memorizers that can be applied in special industries such as automobile, oil, and gas industries.
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| GB/T 7714 | Lin, Xiaoli , Zhou, Panke , Gao, Yiqun et al. Implementation of Thermal-Triggered Binary-Ternary Switchable Memory Performance in Zn/polysulfide/organic Complex-Based Memorizers by Finely Modulating the S6 2- Relaxation [J]. | INORGANIC CHEMISTRY , 2023 , 63 (1) : 775-783 . |
| MLA | Lin, Xiaoli et al. "Implementation of Thermal-Triggered Binary-Ternary Switchable Memory Performance in Zn/polysulfide/organic Complex-Based Memorizers by Finely Modulating the S6 2- Relaxation" . | INORGANIC CHEMISTRY 63 . 1 (2023) : 775-783 . |
| APA | Lin, Xiaoli , Zhou, Panke , Gao, Yiqun , Li, Tao , Chen, Xiong , Li, Haohong et al. Implementation of Thermal-Triggered Binary-Ternary Switchable Memory Performance in Zn/polysulfide/organic Complex-Based Memorizers by Finely Modulating the S6 2- Relaxation . | INORGANIC CHEMISTRY , 2023 , 63 (1) , 775-783 . |
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The low ternary yield and expensive organic active materials hinder the potential industrialization of organic multi-level resistive memories. Here, facile melamine (M)-cyanuric acid (C) hydrogen-bonded organic frame-work (M -C HOF) was firstly fabricated as a new type of ternary memorizer. In the M -C HOF, the robust graphite-like planar 2D sheet along ab-plane containing a rosette motif is constructed from nine hydrogen bonds among M and C, and the 2D sheets are stacked into a 3D network through strong pi-pi stacking interactions. The FTO/M-C/Ag device exhibits a typical ternary memory performance with considerable OFF/ON1/ON2 current ratio of 1:103.1:104.6, relatively low set voltages (1.14 and 1.70 V), good reliability, and high ternary device yield of 74 %. The ternary resistive switching behavior could be ascribed to the filled traps in 2D layer (for ON1 state) and the carriers flowing in 3D network (for ON2 state), which have been verified by quenched fluorescence of isolated M and C, increased (201) lattice plane distance upon external voltages. Besides, this ternary memorizer has superior thermal stability (300 degrees C) and irradiative tolerance. This attempt of HOF-based ternary memorizer presents a new choice for efficient and facial multi-level resistive material.
Keyword ：
Hydrogen-bonded organic framework Hydrogen-bonded organic framework Memorizers in harsh environment Memorizers in harsh environment Ternary resistive memorizer Ternary resistive memorizer Ternary resistive switching mechanism Ternary resistive switching mechanism
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| GB/T 7714 | Song, Kaiyue , Yang, Hailong , Chen, Binjun et al. The facile implementing ternary resistive memory in graphite-like melamine-cyanuric acid hydrogen-bonded organic framework with high ternary yield and environmental tolerance [J]. | APPLIED SURFACE SCIENCE , 2023 , 608 . |
| MLA | Song, Kaiyue et al. "The facile implementing ternary resistive memory in graphite-like melamine-cyanuric acid hydrogen-bonded organic framework with high ternary yield and environmental tolerance" . | APPLIED SURFACE SCIENCE 608 (2023) . |
| APA | Song, Kaiyue , Yang, Hailong , Chen, Binjun , Lin, Xiaoli , Liu, Yue , Liu, Yuanzheng et al. The facile implementing ternary resistive memory in graphite-like melamine-cyanuric acid hydrogen-bonded organic framework with high ternary yield and environmental tolerance . | APPLIED SURFACE SCIENCE , 2023 , 608 . |
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