Photoredox Catalytic Two-Component Radical β-Fluoro-Fluorosulfonamidation Reaction of Styrenes - Details

author：

Huang, Y. (Huang, Y..) ^[1] | Huang, J. (Huang, J..) ^[2] | Wang, P. (Wang, P..) ^[3] | Liao, S. (Liao, S..) ^[4]

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Abstract：

In　this　study,　a　visible-light-mediated　two-component　β-fluoro-fluorosulfonamidation　reaction　of　styrenes　is　demonstrated.　The　bench-stable　reagent,　N-fluorosulfamoyl-pyridinium　tetrafluoroborate　can　be　used　as　a　photoredox-active　nitrogen-centered　radical　precursor　and　also　as　the　fluoride　source.　This　transformation　can　convert　a　series　of　styrenes　to　functional　group-enriched　products,　including　substrates　with　electron-donating　or　withdrawing　groups,　as　well　as　di-　and　tri-substituents　on　the　CC　double　bond.　©　2025　Wiley-VCH　GmbH.

Keyword：

fluorination fluorosulfamidation photoredox catalysis radical reactions sulfamoyl fluorides

Community：

[ 1 ] [Huang Y.]Key Laboratory of Molecule Synthesis and Function Discovery (Fujian Province University), College of Chemistry, Fuzhou University, Fuzhou, 350108, China
[ 2 ] [Huang Y.]State Key Laboratory of Physical Chemistry of Solid Surfaces, Xiamen University, Xiamen, 361005, China
[ 3 ] [Huang J.]Key Laboratory of Molecule Synthesis and Function Discovery (Fujian Province University), College of Chemistry, Fuzhou University, Fuzhou, 350108, China
[ 4 ] [Huang J.]State Key Laboratory of Physical Chemistry of Solid Surfaces, Xiamen University, Xiamen, 361005, China
[ 5 ] [Wang P.]Key Laboratory of Green and Precise Synthetic Chemistry and Application, Ministry of Education, College of Chemistry and Materials Science, Huaibei Normal University, Anhui, Huaibei, 235000, China
[ 6 ] [Liao S.]State Key Laboratory of Physical Chemistry of Solid Surfaces, Xiamen University, Xiamen, 361005, China

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Related Keywords：

Photoredox Catalytic Two-Component Radical β-Fluoro-Fluorosulfonamidation Reaction of Styrenes
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Source ：

European Journal of Organic Chemistry

ISSN： 1434-193X

Year： 2025

Issue： 22

Volume： 28

2 . 5 0 0

JCR@2023

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ESI Highly Cited Papers on the List： 0 Unfold All

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30 Days PV： 2

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