DMSO/SOCl2-Mediated Synthesis of Thiomethylnaphthalenes from Propargyl Alcohols - Details

author：

Wang, Z. (Wang, Z..) ^[1] | Liang, W.-F. (Liang, W.-F..) ^[2] | He, X. (He, X..) ^[3] | Li, J. (Li, J..) ^[4] | Ye, K.-Y. (Ye, K.-Y..) ^[5]

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Abstract：

Herein,　we　reported　the　straightforward　synthesis　of　thiomethylnaphthalenes　via　the　reaction　of　propargyl　alcohols　with　dimethyl　sulfoxide/thionyl　chloride　(DMSO/SOCl2),　which　also　provided　easy　access　to　deuterated　thiomethyl　and　other　thioalkyl　scaffolds　when　deuterated　dimethyl　sulfoxide　and　dialkyl　sulfoxides　were　used,　respectively.　In　addition,　the　thiomethyl　group　can　be　readily　derivatized　to　the　corresponding　sulfoxide,　sulfone,　and　sulfoximine　of　interesting　photophysical　properties.　©　2024　Wiley-VCH　GmbH.

Keyword：

Cyclization Propargyl alcohols Solvatochromism Thiomethylnaphthalenes Transition-metal-free

Community：

[ 1 ] [Wang Z.]Key Laboratory of Molecule Synthesis and Function Discovery (Fujian Province University), College of Chemistry, Fuzhou University, Fuzhou, 350108, China
[ 2 ] [Liang W.-F.]Key Laboratory of Molecule Synthesis and Function Discovery (Fujian Province University), College of Chemistry, Fuzhou University, Fuzhou, 350108, China
[ 3 ] [He X.]Key Laboratory of Molecule Synthesis and Function Discovery (Fujian Province University), College of Chemistry, Fuzhou University, Fuzhou, 350108, China
[ 4 ] [Li J.]Key Laboratory of Molecule Synthesis and Function Discovery (Fujian Province University), College of Chemistry, Fuzhou University, Fuzhou, 350108, China
[ 5 ] [Ye K.-Y.]Key Laboratory of Molecule Synthesis and Function Discovery (Fujian Province University), College of Chemistry, Fuzhou University, Fuzhou, 350108, China
[ 6 ] [Ye K.-Y.]School of Chemistry and Chemical Engineering, Henan Normal University, Xinxiang, 453007, China

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Source ：

Advanced Synthesis and Catalysis

ISSN： 1615-4150

Year： 2024

Issue： 3

Volume： 367

4 . 4 0 0

JCR@2023

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ESI Highly Cited Papers on the List： 0 Unfold All

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