Radical Oxyazidation of Alkenes in Pure Water - Details

author：

Cui, Jinfeng (Cui, Jinfeng.) ^[1] | Zhou, Huan (Zhou, Huan.) ^[2] | Li, Yajun (Li, Yajun.) ^[3] | Bao, Hongli (Bao, Hongli.) ^[4]

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Abstract：

Compared　to　universal　radical　difunctionalizations　of　alkenes　that　are　performed　with　organic　solvents,　such　reactions　with　water　as　the　sole　solvent　are　rarely　reported.　Concerning　the　global　consensus　on　environmental　issues,　we　have　developed　herein　a　method　for　the　radical　oxyazidation　of　alkenes　in　pure　water.　This　reaction　allows　the　construction　of　C　N　and　C　O　bonds　in　a　one-pot　process.　Styrenes,　1,3-dienes,　and　unactivated　alkenes　react　smoothly　under　mild　and　environmentally　benign　conditions　to　afford　a　wide　scope　of　functionalized　azides　in　excellent　yields　and　selectivities.　©　2022　Georg　Thieme　Verlag.　All　rights　reserved.

Keyword：

Copper Olefins Styrene

Community：

[ 1 ] [Cui, Jinfeng]College of Chemistry, Fuzhou University, Fuzhou, Fujian; 350108, China
[ 2 ] [Cui, Jinfeng]Key Laboratory of Coal to Ethylene Glycol and Its Related Technology, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou; 350002, China
[ 3 ] [Zhou, Huan]Key Laboratory of Coal to Ethylene Glycol and Its Related Technology, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou; 350002, China
[ 4 ] [Li, Yajun]Key Laboratory of Coal to Ethylene Glycol and Its Related Technology, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou; 350002, China
[ 5 ] [Bao, Hongli]Key Laboratory of Coal to Ethylene Glycol and Its Related Technology, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou; 350002, China
[ 6 ] [Bao, Hongli]University of Chinese Academy of Sciences, Beijing; 100049, China

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Source ：

Synthesis (Germany)

ISSN： 0039-7881

Year： 2022

Issue： 14

Volume： 54

Page： 3262-3270

2 . 6

JCR@2022

2 . 2 0 0

JCR@2023

ESI HC Threshold：74

JCR Journal Grade：2

CAS Journal Grade：3

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ESI Highly Cited Papers on the List： 0 Unfold All

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30 Days PV： 2

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