The　widespread　existence　of　antibiotics　in　aquatic　environments　has　gained　much　concern　due　to　their　non　biodegradability　and　eco-toxicity,　which　would　easily　destroy　the　ecological　balance.　In　this　work,　the　synthesized　Mg/Fe　layered　bimetallic　hydroxides　(Mg/Fe　LDHs)　was　first　used　to　adsorb　low　concentration　norfloxacin　(NOR)　antibiotics　in　water.　It　was　found　that　the　LDH　adsorbent　with　a　Mg/Fe　molar　ratio　of　5:1　(MF5:1)　exhibited　superior　adsorption　properties　for　the　removal　of　low　concentration　(20　mg.L-1)　of　Norfloxacin　(NOR).　The　adsorption　capacity　could　reach　to　~　97.07　mg.g(-1)　at　neutral　pH.　Kinetic　fitting　shows　that　it　could　be　well　described　by　Pseudo-second-order　models,　indicating　that　chemical　adsorption　dominants　the　process.　Also,　the　isothermal　adsorption　data　could　be　well　fitted　by　Freundlich　isotherm　model,　which　suggests　a　multilayer　adsorption　process.　The　adsorbent　has　good　properties　of　salt　resistance　with　~　5%　and　30%　decrease　of　removal　efficiencies　in　0.1　mol.L-1　KCl　and　CaCl2　solution,　respectively.　By　contrasting　the　structural　variation　of　the　adsorbent　before　and　after　adsorption,　it　could　be　inferred　that　coordination　and　hydrogen　bonding　rather　than　electrostatic　interaction　might　be　the　main　forces　between　NOR　and　Mg/Fe5:1　nanocrystal.　In　addition,　the　recover　of　the　adsorbent　could　be　easily　achieved　by　pyrolysis　and　rehydration　circle　with　little　decrease　of　adsorption　property.　Our　finding　suggests　that　Mg/Fe　LDHs　can　be　severed　as　a　promising　candidate　for　the　removal　of　antibiotics,　especially　for　the　low　concentrations　of　NOR.