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author:

陈天文 (陈天文.) [1] (Scholars:陈天文)

Indexed by:

CQVIP PKU CSCD

Abstract:

探讨了采用液相色谱-电喷雾串联质谱法检测小鼠前列腺中芥子碱硫氰酸盐的方法. 流动相为V(乙腈)∶V(0.5%乙酸)=20∶80, 色谱柱为Zorbax XDB-C18 (150 mm×4.6 mm i.d., 5 μm), 流速为0.6 mL/min. 芥子碱硫氰酸盐的准分子离子和二级碎片离子分别为m/z 304和m/z 251, 方法的检出限为0.7 μg/L, 线性范围为2.7~80.5 μg/L, r为0.9934, 相对标准偏差为7.5%~12.9%, 样品的回收率为81.2%~102.5%.

Keyword:

前列腺 液相色谱-电喷雾离子阱质谱 芥子碱

Community:

  • [ 1 ] [陈天文]福州大学

Reprint 's Address:

  • 陈天文

Email:

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Source :

分析试验室

ISSN: 1000-0720

CN: 11-2017/TF

Year: 2008

Issue: 5

Volume: 27

Page: 115-117

Cited Count:

WoS CC Cited Count:

SCOPUS Cited Count:

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count: -1

Chinese Cited Count:

30 Days PV: 2

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