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Abstract:
探讨了采用液相色谱-电喷雾串联质谱法检测小鼠前列腺中芥子碱硫氰酸盐的方法. 流动相为V(乙腈)∶V(0.5%乙酸)=20∶80, 色谱柱为Zorbax XDB-C18 (150 mm×4.6 mm i.d., 5 μm), 流速为0.6 mL/min. 芥子碱硫氰酸盐的准分子离子和二级碎片离子分别为m/z 304和m/z 251, 方法的检出限为0.7 μg/L, 线性范围为2.7~80.5 μg/L, r为0.9934, 相对标准偏差为7.5%~12.9%, 样品的回收率为81.2%~102.5%.
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分析试验室
ISSN: 1000-0720
CN: 11-2017/TF
Year: 2008
Issue: 5
Volume: 27
Page: 115-117
Cited Count:
SCOPUS Cited Count:
ESI Highly Cited Papers on the List: 0 Unfold All
WanFang Cited Count: -1
Chinese Cited Count:
30 Days PV: 2
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