Study of the grafting reaction of SnMe4 on the surface of ZSM-5 zeolite - Details

author：

Zheng, Y. (Zheng, Y..) ^[1] | Wang, X.-X. (Wang, X.-X..) ^[2] | Li, Z.-H. (Li, Z.-H..) ^[3] | Fu, X.-Z. (Fu, X.-Z..) ^[4] | Wei, K.-M. (Wei, K.-M..) ^[5]

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Abstract：

The　grafting　reaction　of　tetramethyltin　on　the　surface　of　ZSM-5　zeolite　(Si:　A1　=　55.0)　was　studied　under　vacuum　conditions,　and　the　chemical　compositions,　structure　and　properties　of　the　resulting　solid　were　characterized　by　in　situ　FTIR,　ICP,　XRD,　XPS,　UV-vis　DRS,　temperature　programmed　decomposition　(TPD)　and　N2　adsorption.　The　results　show　that　the　reaction　occurs　on　the　surface　of　ZSM-5　zeolite　at　223　K　without　destroying　the　zeolite　framework.　The　BET　surface　area　and　the　pore　volume　of　the　zeolite　decrease　and　the　surface　properties　change;　however,　the　microporous　structure　is　retained　during　the　reaction　and　post　treatment.　Copyright　©　2006　John　Wiley　&　Sons,　Ltd.

Keyword：

Grafting reaction; Surface organometallic chemistry; Tetramethyltin; ZSM-5 zeolite

Community：

[ 1 ] [Zheng, Y.]Research Institute of Photocatalysis, Fuzhou University, Fuzhou 350002, China
[ 2 ] [Zheng, Y.]College of Chemistry and Materials Science, Fujian Normal University, Fuzhou 350007, China
[ 3 ] [Wang, X.-X.]Research Institute of Photocatalysis, Fuzhou University, Fuzhou 350002, China
[ 4 ] [Li, Z.-H.]Research Institute of Photocatalysis, Fuzhou University, Fuzhou 350002, China
[ 5 ] [Fu, X.-Z.]Research Institute of Photocatalysis, Fuzhou University, Fuzhou 350002, China
[ 6 ] [Wei, K.-M.]Research Institute of Photocatalysis, Fuzhou University, Fuzhou 350002, China

Reprint 's Address：

[Wang, X.-X.]Research Institute of Photocatalysis, Fuzhou University, Fuzhou 350002, China

Email：

xwang@fzu.edu.cn

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Source ：

Applied Organometallic Chemistry

ISSN： 0268-2605

Year： 2006

Issue： 12

Volume： 20

Page： 874-879

1 . 2 3 3

JCR@2006

3 . 7 0 0

JCR@2023

JCR Journal Grade：2

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SCOPUS Cited Count： 2

ESI Highly Cited Papers on the List： 0 Unfold All

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30 Days PV： 0

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