The　adsorption　of　Ni(II)　in　aqueous　solution　with　ion　exchange　resins　was　investigated,　and　001×14.5　strong　acidic　cation　ion　exchange　resin　showed　the　maximum　capacity　by　the　resin　selection　experiment.　The　adsorption　properties　of　the　selected　001×14.5　resin　for　Ni(II)　were　studied　by　static　experiments.　The　results　indicated　that　the　influence　of　external　diffusion　was　eliminated　when　stirring　speed　was　over　100　r/min,　and　the　best　pH　value　was　7,　and　that　the　percent　removal　of　Ni(II)　increased　as　the　consumption　of　resin.　The　adsorption　behavior　of　001×14.5　for　Ni(II),　which　was　the　favourable　adsorption,　conformed　the　Langmuir　isotherm　equation　well.　The　adsorption　process　corresponded　with　pseudo-second-order　kinetic　model,　the　activation　energy　was　30.9　kJ/mol,　and　the　kinetics　experiments　showed　that　intrapartical　diffusion　was　the　main　rate-controlling　step.　The　desorption　efficiency　of　resin　to　Ni(II)　could　be　over　98%　with　1　mol/L　sulfuric　acid　to　regenerate　the　saturated　resin.