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Abstract:
A method based on reversed-phase liquid chromatography-tandem mass spectrometry (LC/MS/MS) coupled with solid phase extraction (SPE) was developed and validated for qualitative and quantitative detection of eight parabens in four types of food simulant sample, including distilled water, 3% acetic acid, 10% ethanol and olive oil. The detection limits of the eight parabens after the SPE procedure were in the range of 0.005-0.010 μg L-1 in distilled water, 0.006-0.015 μg L-1 in 3% acetic acid, 0.005-0.017 μg L-1 in 10% ethanol and 0.2-0.6 μg L-1 in olive oil. The relative standard deviations (RSDs) were in the range of 1.90-8.48% for distilled water, 1.01-3.73% for 3% acetic acid, 5.78-12.97% for 10% ethanol and 0.29-5.40% for olive oil. The proposed method was applied to assess the migration of parabens from real antibacterial plastic packaging samples with satisfactory results. This journal is © the Partner Organisations 2014.
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Analytical Methods
ISSN: 1759-9660
Year: 2014
Issue: 7
Volume: 6
Page: 2096-2101
1 . 8 2 1
JCR@2014
2 . 7 0 0
JCR@2023
ESI HC Threshold:268
JCR Journal Grade:2
CAS Journal Grade:3
Cited Count:
SCOPUS Cited Count: 10
ESI Highly Cited Papers on the List: 0 Unfold All
WanFang Cited Count:
Chinese Cited Count:
30 Days PV: 0
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