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author:

Cheng, Q. (Cheng, Q..) [1] | Yang, F. (Yang, F..) [2] | Li, J. (Li, J..) [3] | Lu, S. (Lu, S..) [4] | Lan, J. (Lan, J..) [5] | Jiang, J. (Jiang, J..) [6]

Indexed by:

Scopus PKU CSCD

Abstract:

A method to analyze the volatile components in Minnan oolong tea was developed based on headspace solid phase microextraction (HS-SPME) coupled with comprehensive two dimensional gas chromatography-time of flight mass spectrometry (GC×GC-TOF MS). Volatile compounds of 48 oolong tea samples with different qualities and production seasons from five varieties (Tieguanyin, Huangjingui, Benshan, Maoxie and Meizhan) were extracted by HS-SPME and analyzed by GC×GC-TOF MS. More than 2000 peaks were obtained from each sample, and 51 common compounds were tentatively identified by comparison with the standard mass spectrum databases, retention indices and structure spectra. The projection score of the common compounds obtained from principal component analysis (PCA) had presented a straightforward classification trend for different oolong tea varieties. In addition, 9 compounds which had significant impact on the classification were selected by stepwise discriminate analysis, and used as variables to establish four discriminated functions by Fisher' s discriminate analysis (FDA). The accuracy for the recognition of 48 samples was 97.9%. The results had demonstrated the feasibility of the method to be used to discriminate the oolong tea varieties.

Keyword:

Comprehensive two-dimensional gas chromatography-time of flight mass spectrometry (GC×GC-TOF MS); Fisher's discriminate analysis; Headspace solid phase microextraction (HS-SPME); Minnan oolong tea; Principal component analysis (PCA); Volatile components

Community:

  • [ 1 ] [Cheng, Q.]Key Laboratory of Analysis and Detection for Food Safety of Ministry of Education, Fujian Provincial Key Laboratory of Analysis and Detection Technology for Food Safety, Department of Chemistry of Fuzhou University, Fuzhou, 350108, China
  • [ 2 ] [Yang, F.]Inspection and Quarantine Technical Center of Fujian Entry-Exit Inspection and Quarantine Bureau, Key Laboratory of Inspection and Quarantine of Fujian, Fuzhou, 350001, China
  • [ 3 ] [Li, J.]Inspection and Quarantine Technical Center of Fujian Entry-Exit Inspection and Quarantine Bureau, Key Laboratory of Inspection and Quarantine of Fujian, Fuzhou, 350001, China
  • [ 4 ] [Lu, S.]Inspection and Quarantine Technical Center of Fujian Entry-Exit Inspection and Quarantine Bureau, Key Laboratory of Inspection and Quarantine of Fujian, Fuzhou, 350001, China
  • [ 5 ] [Lan, J.]Inspection and Quarantine Technical Center of Fujian Entry-Exit Inspection and Quarantine Bureau, Key Laboratory of Inspection and Quarantine of Fujian, Fuzhou, 350001, China
  • [ 6 ] [Jiang, J.]Inspection and Quarantine Technical Center of Fujian Entry-Exit Inspection and Quarantine Bureau, Key Laboratory of Inspection and Quarantine of Fujian, Fuzhou, 350001, China

Reprint 's Address:

  • [Yang, F.]Inspection and Quarantine Technical Center of Fujian Entry-Exit Inspection and Quarantine Bureau, Key Laboratory of Inspection and Quarantine of FujianChina

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Source :

Chinese Journal of Chromatography (Se Pu)

ISSN: 1000-8713

CN: 21-1185/O6

Year: 2015

Issue: 2

Volume: 33

Page: 174-181

1 . 2 0 0

JCR@2023

Cited Count:

WoS CC Cited Count: 0

SCOPUS Cited Count: 4

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 4

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