Low-temperature and template-free synthesis of ZnIn2S 4 microspheres - Details

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Abstract：

Porous　ZnIn2S4　microspheres　have　been　successfully　synthesized　by　means　of　a　facile　thermal　solution　method　at　353　K.　This　method　was　a　simple　route　that　involved　low　temperature,　no　templates,　no　catalysts,　no　surfactants,　or　organic　solvents.　Scanning　electron　microscopy,　transmission　electron　microscopy,　high-resolution　transmission　electron　microscopy,　X-ray　diffraction,　energy-dispersive　X-ray　spectroscopy,　X-ray　photoelectron　spectroscopy,　nitrogen　sorption　analysis,　and　a　UV-vis　spectrophotometer　were　used　to　characterize　the　products.　The　results　demonstrated　that　the　microspheres,　which　were　composed　of　many　ZnIn2S4　single　crystal　nanosheets,　underwent　the　Oswald　ripening　and　self-assembly　processes.　A　morphology　formation　mechanism　has　been　proposed　and　discussed.　The　porous　ZnIn2S4　product　showed　an　enhancing　visible-light　photocatalytic　activity　for　methyl　orange　degradation.　The　as-grown　architectures　may　have　potential　applications　in　solar　energy　conversion,　environmental　remediation,　and　advanced　optical/electric　nanodevices.　©　2008　American　Chemical　Society.

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[ 1 ] [Chen, Z.]Research Institute of Photocatalysis, State Key Laboratory Breeding Base of Photocatalysis, Fuzhou University, Fuzhou, 350002, China
[ 2 ] [Li, D.]Research Institute of Photocatalysis, State Key Laboratory Breeding Base of Photocatalysis, Fuzhou University, Fuzhou, 350002, China
[ 3 ] [Zhang, W.]Research Institute of Photocatalysis, State Key Laboratory Breeding Base of Photocatalysis, Fuzhou University, Fuzhou, 350002, China
[ 4 ] [Chen, C.]Research Institute of Photocatalysis, State Key Laboratory Breeding Base of Photocatalysis, Fuzhou University, Fuzhou, 350002, China
[ 5 ] [Li, W.]Research Institute of Photocatalysis, State Key Laboratory Breeding Base of Photocatalysis, Fuzhou University, Fuzhou, 350002, China
[ 6 ] [Sun, M.]Research Institute of Photocatalysis, State Key Laboratory Breeding Base of Photocatalysis, Fuzhou University, Fuzhou, 350002, China
[ 7 ] [He, Y.]Research Institute of Photocatalysis, State Key Laboratory Breeding Base of Photocatalysis, Fuzhou University, Fuzhou, 350002, China
[ 8 ] [Fu, X.]Research Institute of Photocatalysis, State Key Laboratory Breeding Base of Photocatalysis, Fuzhou University, Fuzhou, 350002, China

Reprint 's Address：

[Li, D.]Research Institute of Photocatalysis, State Key Laboratory Breeding Base of Photocatalysis, Fuzhou University, Fuzhou, 350002, China

Email：

dzli@fzu.edu.cn

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Source ：

Inorganic Chemistry

ISSN： 0020-1669

Year： 2008

Issue： 21

Volume： 47

Page： 9766-9772

4 . 1 4 7

JCR@2008

4 . 3 0 0

JCR@2023

JCR Journal Grade：1

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WoS CC Cited Count： 0

SCOPUS Cited Count： 183

ESI Highly Cited Papers on the List： 0 Unfold All

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Chinese Cited Count：

30 Days PV： 2

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