New photocatalyst, Sb2S3, for degradation of methyl orange under visible-light irradiation - Details

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Abstract：

A　novel　visible-light　photocatalyst,　Sb2S3,　was　synthesized　with　a　simple　method.　The　specimen　was　characterized　by　X-ray　diffraction,　transmission　electron　microscopy,　Brunauer-Emmett-Teller　(BET)　surface　area　analysis,　and　UV-vis　diffuse　reflectance　spectroscopy.　The　results　revealed　that　the　as-synthesized　sample　was　orthorhombic　phase　and　consisted　of　rodlike　particles.　It　possessed　a　surface　area　of　15.1　m2·　g-1,　and　the　band　gap　was　about　1.66　eV.　The　photocatalytic　activity　of　Sb2S3　nanorods　was　evaluated　by　the　decomposition　of　methyl　orange　in　aqueous　solution　under　visible-light　irradiation.　The　results　demonstrated　that　the　photodegradation　ratio　of　methyl　orange　was　up　to　97%　after　30　min　of　irradiation,　which　was　much　better　than　that　of　CdS　and　TiO2-xN　x　under　the　same　condition.　Meanwhile,　the　possible　mechanism　of　the　photocatalytic　reaction　had　also　been　studied　by　liquid　chromatography-mass　spectrometry,　and　the　OH　had　been　detected　also　by　terephthalic　acid　photoluminescence　probing　technique.　©　2008　American　Chemical　Society.

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[ 1 ] [Sun, M.]State Key Laboratory Breeding Base of Photocatalysis, College of Chemistry and Chemical Engineering, Fuzhou University, Fuzhou, 350002, China
[ 2 ] [Li, D.]State Key Laboratory Breeding Base of Photocatalysis, College of Chemistry and Chemical Engineering, Fuzhou University, Fuzhou, 350002, China
[ 3 ] [Li, W.]State Key Laboratory Breeding Base of Photocatalysis, College of Chemistry and Chemical Engineering, Fuzhou University, Fuzhou, 350002, China
[ 4 ] [Chen, Y.]State Key Laboratory Breeding Base of Photocatalysis, College of Chemistry and Chemical Engineering, Fuzhou University, Fuzhou, 350002, China
[ 5 ] [Chen, Z.]State Key Laboratory Breeding Base of Photocatalysis, College of Chemistry and Chemical Engineering, Fuzhou University, Fuzhou, 350002, China
[ 6 ] [He, Y.]State Key Laboratory Breeding Base of Photocatalysis, College of Chemistry and Chemical Engineering, Fuzhou University, Fuzhou, 350002, China
[ 7 ] [Fu, X.]State Key Laboratory Breeding Base of Photocatalysis, College of Chemistry and Chemical Engineering, Fuzhou University, Fuzhou, 350002, China

Reprint 's Address：

[Li, D.]State Key Laboratory Breeding Base of Photocatalysis, College of Chemistry and Chemical Engineering, Fuzhou University, Fuzhou, 350002, China

Email：

dzli@fzu.edu.cn

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Journal of Physical Chemistry C

ISSN： 1932-7447

Year： 2008

Issue： 46

Volume： 112

Page： 18076-18081

3 . 3 9 6

JCR@2008

3 . 3 0 0

JCR@2023

JCR Journal Grade：1

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ESI Highly Cited Papers on the List： 0 Unfold All

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30 Days PV： 1

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