Facile synthesis of 1,2-thiobenzonitriles: Via Cu-catalyzed denitrogenative radical coupling reaction - Details

author：

Zhou, Y. (Zhou, Y..) ^[1] | Wang, Y. (Wang, Y..) ^[2] | Lou, Y. (Lou, Y..) ^[3] | Song, Q. (Song, Q..) ^[4]

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Abstract：

A　Cu-catalyzed　synthesis　of　1,2-thiobenzonitriles　via　oxidative　C-N　cleavage　of　3-aminoindazoles　followed　by　radical　coupling　with　thiols　is　developed.　A　diverse　array　of　1,2-thiobenzonitriles　were　obtained　in　good　yields　with　wide　substrate　scope.　Notably,　this　is　the　first　example　of　denitrogenative　radical　coupling　with　3-aminoindazoles.　©　2019　The　Royal　Society　of　Chemistry.

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[ 1 ] [Zhou, Y.]Institute of Next Generation Matter Transformation, College of Chemical Engineering and College of Materials Science Engineering, Huaqiao University, 668 Jimei Blvd, Xiamen Fujian, 361021, China
[ 2 ] [Wang, Y.]Institute of Next Generation Matter Transformation, College of Chemical Engineering and College of Materials Science Engineering, Huaqiao University, 668 Jimei Blvd, Xiamen Fujian, 361021, China
[ 3 ] [Lou, Y.]Collaborative Innovation Center of Yangtze River Delta Region Green Pharmaceuticals, Zhejiang University of Technology, Hangzhou Zhejiang, 310000, China
[ 4 ] [Song, Q.]Institute of Next Generation Matter Transformation, College of Chemical Engineering and College of Materials Science Engineering, Huaqiao University, 668 Jimei Blvd, Xiamen Fujian, 361021, China
[ 5 ] [Song, Q.]Collaborative Innovation Center of Yangtze River Delta Region Green Pharmaceuticals, Zhejiang University of Technology, Hangzhou Zhejiang, 310000, China
[ 6 ] [Song, Q.]Key Laboratory of Molecule Synthesis and Function Discovery, Fujian Province University, College of Chemistry, Fuzhou University, Fuzhou Fujian, 350108, China

Reprint 's Address：

[Song, Q.]Institute of Next Generation Matter Transformation, College of Chemical Engineering and College of Materials Science Engineering, Huaqiao University, 668 Jimei Blvd, China

Email：

qsong@hqu.edu.cn

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Source ：

Chemical Communications

ISSN： 1359-7345

Year： 2019

Issue： 69

Volume： 55

Page： 10265-10268

5 . 9 9 6

JCR@2019

4 . 3 0 0

JCR@2023

ESI HC Threshold：184

JCR Journal Grade：1

CAS Journal Grade：2

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SCOPUS Cited Count：

ESI Highly Cited Papers on the List： 0 Unfold All

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Chinese Cited Count：

30 Days PV： 2

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