Palladium-Catalyzed Direct C-H Carbonylation of Free Primary Benzylamines: A Synthesis of Benzolactams - Details

author：

Zhang, C. (Zhang, C..) ^[1] | Ding, Y. (Ding, Y..) ^[2] | Gao, Y. (Gao, Y..) ^[3] | Li, S. (Li, S..) ^[4] | Li, G. (Li, G..) ^[5]

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Abstract：

A　protocol　for　palladium-catalyzed　C-H　carbonylation　of　readily　available　free　primary　benzylamines　using　NH2　as　the　chelating　group　under　an　atmospheric　pressure　of　CO　has　been　achieved,　providing　a　general,　atom-　and　step-economic　approach　to　benzolactams,　an　important　structural　motif　found　in　many　biologically　active　compounds.　Application　of　this　new　method　is　also　exemplified　in　the　concise　syntheses　of　two　bioactive　molecules.　©　Copyright　2018　American　Chemical　Society.

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[ 1 ] [Zhang, C.]College of Chemistry, Fuzhou University, Fuzhou, Fujian, 350002, China
[ 2 ] [Zhang, C.]Key Laboratory of Coal to Ethylene Glycol and Its Related Technology, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou, Fujian, 350002, China
[ 3 ] [Ding, Y.]Key Laboratory of Coal to Ethylene Glycol and Its Related Technology, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou, Fujian, 350002, China
[ 4 ] [Gao, Y.]Key Laboratory of Coal to Ethylene Glycol and Its Related Technology, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou, Fujian, 350002, China
[ 5 ] [Li, S.]Key Laboratory of Coal to Ethylene Glycol and Its Related Technology, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou, Fujian, 350002, China
[ 6 ] [Li, G.]Key Laboratory of Coal to Ethylene Glycol and Its Related Technology, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou, Fujian, 350002, China

Reprint 's Address：

[Li, S.]Key Laboratory of Coal to Ethylene Glycol and Its Related Technology, Fujian Institute of Research on the Structure of Matter, Chinese Academy of SciencesChina

Email：

sdli@fjirsm.ac.cn

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Source ：

Organic Letters

ISSN： 1523-7060

Year： 2018

Issue： 9

Volume： 20

Page： 2595-2598

6 . 5 5 5

JCR@2018

4 . 9 0 0

JCR@2023

ESI HC Threshold：209

JCR Journal Grade：1

CAS Journal Grade：1

Cited Count：

WoS CC Cited Count：

SCOPUS Cited Count： 60

ESI Highly Cited Papers on the List： 0 Unfold All

WanFang Cited Count：

Chinese Cited Count：

30 Days PV： 3

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