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Abstract：
The title complex Pd(C13H15N2O3)2(C 13H15N2O3))- is the anion of isonitrosoethylacetoacetate-N-benzylimine) crystallizes in the monoclinic system, space group P21/c with a=8. 197(2), b=14. 524(3), c=10. 835(2) Å, β=101. 77(3)°, V = 1262. 8(5) Å3, Dc=1. 580 g/cm3, F(000)=616, Mr=600. 94, μ(MoKα)= 0. 784mm-1, Z=2 and final R=0. 0410 and wR=0. 0962 for 1855 observed reflections [I≥2σ(I)]. The geometry around the palladium atom is a distorted trans PdN4 square plane, the Schiff base ligand C6H5CH2-IEAI- being coordinated through its oximo-nitrogen atom and imino-nitrogen atom.
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CHINESE JOURNAL OF STRUCTURAL CHEMISTRY
ISSN： 0254-5861
CN： 35-1112/TQ
Year： 2000
Issue： 3
Volume： 19
Page： 177-180
5 . 9 0 0
JCR@2023
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