Compare Two Methods for Synthesis of Phthalimidomethyl Phthalocyanine Zinc - Details

author：

Peng, Y.-R. (Peng, Y.-R..) ^[1] | Lin, Z.-P. (Lin, Z.-P..) ^[2] | Xue, J.-P. (Xue, J.-P..) ^[3] | Chen, N.-S. (Chen, N.-S..) ^[4] | Huang, J.-L. (Huang, J.-L..) ^[5]

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Abstract：

Molecular　precursors　phthalimidomethyl　phthalic　acid　and　phthalimidomethyl　phthalonitrile　were　synthesized　for　the　first　time　and　both　were　able　to　condensation　to　form　tetra-phthalimidomethyl　phthalocyanine　zinc　through　＂ammomium　molybdate　method＂　and　＂DBU　method　＂respectively.　The　precursors　and　title　compounds　were　characterized　by　element　analysis,　IR,　UV/Vis　as　well　as　NMR.　The　two　synthesis　methods　were　compared,　the　result　indicated　that　using　the　phthalimidomethyl　phthalic　acid　as　precursor　through　the　former　method,　the　product　was　an　isomer　with　C4h　symmetry,　while　using　phthalimidomethyl　phthalonitrile　as　precursor　through　the　latter　method,　the　products　were　a　mixture　of　different　isomers.

Keyword：

Characterization; Phthalocyanine zinc; Synthesis method

Community：

[ 1 ] [Peng, Y.-R.]Institute of Functional Materials, Department of Chemistry, Fuzhou University, Fuzhou 350002, China
[ 2 ] [Peng, Y.-R.]Department of Chemistry, Fujian Normal University, Fuzhou 350007, China
[ 3 ] [Lin, Z.-P.]Institute of Functional Materials, Department of Chemistry, Fuzhou University, Fuzhou 350002, China
[ 4 ] [Xue, J.-P.]Institute of Functional Materials, Department of Chemistry, Fuzhou University, Fuzhou 350002, China
[ 5 ] [Chen, N.-S.]Institute of Functional Materials, Department of Chemistry, Fuzhou University, Fuzhou 350002, China
[ 6 ] [Huang, J.-L.]Institute of Functional Materials, Department of Chemistry, Fuzhou University, Fuzhou 350002, China

Reprint 's Address：

[Huang, J.-L.]Institute of Functional Materials, Department of Chemistry, Fuzhou University, Fuzhou 350002, China

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Source ：

Chinese Journal of Inorganic Chemistry

ISSN： 1001-4861

Year： 2002

Issue： 3

Volume： 18

Page： 324-

0 . 4 9 4

JCR@2002

0 . 8 0 0

JCR@2023

JCR Journal Grade：4

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SCOPUS Cited Count：

ESI Highly Cited Papers on the List： 0 Unfold All

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Chinese Cited Count：

30 Days PV： 3

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