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Abstract：
The hydrothermal reaction of V2O5, Cu(CH3COO)2 · H2O, TMAOH and 1,2-diaminopropane gave a novel three-dimensional framework material, {[Cu(1,2-pn)2]4[V18O42(H 2O)]}n · 8nH2O, which was constructed from the mixed-valence {V18O42(H2O)} clusters interconnected through {Cu(1,2-pn)2} complex groups. {[Cu(1,2-pn)2]4[V18O42(H 2O)]}n · 8nH2O was characterized by IR, TGA and single-crystal X-ray diffraction. It crystallizes in tetragonal space group P4/nnc with a=1.510 7(2) nm, c= 1.864 5(4) nm, Dc=2.028 g/cm3, Z=2, R1=0.063 1, wR2=0.153 8.
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Chemical Journal of Chinese Universities
ISSN： 0251-0790
Year： 2002
Issue： 4
Volume： 23
Page： 536-537
0 . 8 3
JCR@2002
0 . 7 0 0
JCR@2023
JCR Journal Grade：2
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ESI Highly Cited Papers on the List： 0 Unfold All
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30 Days PV： 0
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