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author:

Lu, Lijun (Lu, Lijun.) [1] | Xiong, Wenming (Xiong, Wenming.) [2] | Li, Xiaojing (Li, Xiaojing.) [3] | Lv, Shuiyuan (Lv, Shuiyuan.) [4] | Tang, Xi (Tang, Xi.) [5] | Chen, Minshi (Chen, Minshi.) [6] | Zou, Zhexiang (Zou, Zhexiang.) [7] | Lin, Zhenyu (Lin, Zhenyu.) [8] | Qiu, Bin (Qiu, Bin.) [9] | Chen, Guonan (Chen, Guonan.) [10]

Indexed by:

EI

Abstract:

A method based on reversed-phase liquid chromatography-tandem mass spectrometry (LC/MS/MS) coupled with solid phase extraction (SPE) was developed and validated for qualitative and quantitative detection of eight parabens in four types of food simulant sample, including distilled water, 3% acetic acid, 10% ethanol and olive oil. The detection limits of the eight parabens after the SPE procedure were in the range of 0.005-0.010 μg L-1 in distilled water, 0.006-0.015 μg L-1 in 3% acetic acid, 0.005-0.017 μg L-1 in 10% ethanol and 0.2-0.6 μg L-1 in olive oil. The relative standard deviations (RSDs) were in the range of 1.90-8.48% for distilled water, 1.01-3.73% for 3% acetic acid, 5.78-12.97% for 10% ethanol and 0.29-5.40% for olive oil. The proposed method was applied to assess the migration of parabens from real antibacterial plastic packaging samples with satisfactory results. This journal is © the Partner Organisations 2014.

Keyword:

Acetic acid Electrospray ionization Ethanol Liquid chromatography Mass spectrometry Olive oil Parabens pH Phase separation

Community:

  • [ 1 ] [Lu, Lijun]Ministry of Education Key Laboratory of Analysis and Detection Technology for Food Safety, Department of Chemistry, Fuzhou University, Fuzhou 350002, China
  • [ 2 ] [Xiong, Wenming]Ministry of Education Key Laboratory of Analysis and Detection Technology for Food Safety, Department of Chemistry, Fuzhou University, Fuzhou 350002, China
  • [ 3 ] [Li, Xiaojing]Technical Centre of Fujian Entry-Exit Inspection and Quarantine Bureau, Fuzhou 350001, China
  • [ 4 ] [Lv, Shuiyuan]Technical Centre of Fujian Entry-Exit Inspection and Quarantine Bureau, Fuzhou 350001, China
  • [ 5 ] [Tang, Xi]Technical Centre of Fujian Entry-Exit Inspection and Quarantine Bureau, Fuzhou 350001, China
  • [ 6 ] [Chen, Minshi]Technical Centre of Fujian Entry-Exit Inspection and Quarantine Bureau, Fuzhou 350001, China
  • [ 7 ] [Zou, Zhexiang]Technical Centre of Fujian Entry-Exit Inspection and Quarantine Bureau, Fuzhou 350001, China
  • [ 8 ] [Lin, Zhenyu]Ministry of Education Key Laboratory of Analysis and Detection Technology for Food Safety, Department of Chemistry, Fuzhou University, Fuzhou 350002, China
  • [ 9 ] [Qiu, Bin]Ministry of Education Key Laboratory of Analysis and Detection Technology for Food Safety, Department of Chemistry, Fuzhou University, Fuzhou 350002, China
  • [ 10 ] [Chen, Guonan]Ministry of Education Key Laboratory of Analysis and Detection Technology for Food Safety, Department of Chemistry, Fuzhou University, Fuzhou 350002, China

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Source :

Analytical Methods

ISSN: 1759-9660

Year: 2014

Issue: 7

Volume: 6

Page: 2096-2101

1 . 8 2 1

JCR@2014

2 . 7 0 0

JCR@2023

ESI HC Threshold:268

JCR Journal Grade:2

CAS Journal Grade:3

Cited Count:

WoS CC Cited Count:

SCOPUS Cited Count:

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 0

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