Binuclear　copper(II)　complexes　containing　ferrocenyl　Cu-2　(dmaf)(2)　(CH3COO)(4)　(I)　and　Cu-2　(dmaf)(2)　(C6H5COO)(4)　(II)　[dmaf　=　(dimethylamino-methyl)ferrocene]　were　synthesized　at　room　temperature.　Their　chemical　constitutions　were　measured　semiquantitatively　by　scanning　electrical　mirror　(SEM),　and　their　cell　parameters　were　determined　by　X-ray　diffraction,　which　show　that　the　two　complexes　have　similar　crystal　structure.　The　studies　on　IR,　far　IR,　solid　electronic　spectrum　of　diffuse　reflection,　and　cyclic　voltammetry　(CV)　indicate　that　the　two　compounds　have　an　UV　absorption　peak　in　234-269　nm　and　245-280　nm,　respectively,　and　in　the　visible　range　there　is　a　d-d　transition　wide　region.　The　CV　curves　indicate　that　the　oxidation-reduction　potentials　of　the　two　compounds　are　0.53,　0.37　and　0.62,　0.36　V,　respectively.